CA2129166A1 - Procede et dispositif pour mesurer des parametres physiques d'echantillons poreux mouillables par des fluides - Google Patents

Procede et dispositif pour mesurer des parametres physiques d'echantillons poreux mouillables par des fluides

Info

Publication number
CA2129166A1
CA2129166A1 CA002129166A CA2129166A CA2129166A1 CA 2129166 A1 CA2129166 A1 CA 2129166A1 CA 002129166 A CA002129166 A CA 002129166A CA 2129166 A CA2129166 A CA 2129166A CA 2129166 A1 CA2129166 A1 CA 2129166A1
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CA
Canada
Prior art keywords
fluid
sample
pressure
wettable
porous
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CA002129166A
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English (en)
Other versions
CA2129166C (fr
Inventor
Roland Lenormand
Annick Eisenzimmer
Gabriel Ringot
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IFP Energies Nouvelles IFPEN
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Individual
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Publication of CA2129166A1 publication Critical patent/CA2129166A1/fr
Application granted granted Critical
Publication of CA2129166C publication Critical patent/CA2129166C/fr
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00—Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08—Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082—Investigating permeability by forcing a fluid through a sample
    • G01N15/0826—Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N29/00—Investigating or analysing materials by the use of ultrasonic, sonic or infrasonic waves; Visualisation of the interior of objects by transmitting ultrasonic or sonic waves through the object
    • G01N29/04—Analysing solids
    • G01N29/07—Analysing solids by measuring propagation velocity or propagation time of acoustic waves
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/024—Mixtures
    • G01N2291/02441—Liquids in porous solids
    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N2291/00—Indexing codes associated with group G01N29/00
    • G01N2291/02—Indexing codes associated with the analysed material
    • G01N2291/028—Material parameters
    • G01N2291/02872—Pressure

Landscapes

  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Health & Medical Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Pathology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Acoustics & Sound (AREA)
  • Fluid Mechanics (AREA)
  • Dispersion Chemistry (AREA)
  • Investigating Or Analyzing Materials By The Use Of Ultrasonic Waves (AREA)
  • Investigating Or Analyzing Materials By The Use Of Electric Means (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)

Abstract

- Le procédé consiste essentiellement à placer un échantillon solide imbibé avec un premier fluide (de l'eau par exemple) dans une enceinte close, d'injecter par des moyens de pression un autre fluide sous pression à une première extrémité de l'enceinte et de balayer l'extrémité opposée par un fluide à basse pression mis en circulation par des moyens de pompage, qui entraîne au dehors le fluide draîné. Le dispositif comporte des moyens de mesure permettant de connaître la pression et la saturation de l'échantillon en au moins un point de sa longueur, la quantité de fluide évacué et la résistivité électrique de l'échantillon. Par une variation progressive des débits injectés, on peut réaliser sans toucher à l'échantillon, des cycles complets de draînages et d'imbibitions avec établissement de courbes de variation de la pression capillaire, et calcul des perméabilités relatives.
- Application notamment à la pétrophysique des roches ou au test de matériaux de construction dans le bâtiment.
CA002129166A 1993-07-29 1994-07-29 Procede et dispositif pour mesurer des parametres physiques d'echantillons poreux mouillables par des fluides Expired - Fee Related CA2129166C (fr)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR9309481A FR2708742B1 (fr) 1993-07-29 1993-07-29 Procédé et dispositiphi pour mesurer des paramètres physiques d'échantillons poreux mouillables par des fluides.
FR93/09481 1993-07-29

Publications (2)

Publication Number Publication Date
CA2129166A1 true CA2129166A1 (fr) 1995-01-30
CA2129166C CA2129166C (fr) 2007-07-10

Family

ID=9449851

Family Applications (1)

Application Number Title Priority Date Filing Date
CA002129166A Expired - Fee Related CA2129166C (fr) 1993-07-29 1994-07-29 Procede et dispositif pour mesurer des parametres physiques d'echantillons poreux mouillables par des fluides

Country Status (5)

Country Link
US (1) US5679885A (fr)
CA (1) CA2129166C (fr)
FR (1) FR2708742B1 (fr)
GB (1) GB2280512B (fr)
NO (1) NO315822B1 (fr)

Families Citing this family (56)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2728344B1 (fr) * 1994-12-19 1997-01-24 Inst Francais Du Petrole Methode et dispositif pour separer et mesurer le volume des differentes phases d'un melange de fluides
AU4460596A (en) * 1995-01-12 1996-07-31 Vladimir Nikolaevich Belonenko Devices for measuring viscosity and for investigating fluid flow through capillary-porous mediums
IT1273968B (it) * 1995-02-24 1997-07-11 Finmeccanica Spa Apparecchiatura per il rilevamento ottico di difetti superficiali in particolare per nastri laminati
FR2731073B1 (fr) * 1995-02-27 1997-04-04 Inst Francais Du Petrole Methode et dispositif pour determiner differents parametres physiques d'echantillons de materiaux poreux, en presence de fluides di- ou triphasiques
FR2734056B1 (fr) * 1995-05-12 1997-06-20 Inst Francais Du Petrole Cellule de mesure a prise de pression multiple
US5731511A (en) * 1995-05-12 1998-03-24 Institut Francais Du Petrole Measuring cell with multiple pressure taps
FR2762681B1 (fr) * 1997-04-29 1999-10-08 Inst Francais Du Petrole Dispositif pour faire des mesures sur un echantillon poreux en presence de fluides, utilisant des membranes semi-permeables resistant a la temperature
FR2781573B1 (fr) * 1998-07-24 2000-08-25 Inst Francais Du Petrole Methode de mesure rapide de l'indice de resistivite d'echantillons solides tels que des roches
US6422063B1 (en) * 1998-08-11 2002-07-23 Ramaswamy C. Anantheswaran Rapid method to experimentally measure the gas permeability of micro-perforated films
FR2785680B1 (fr) * 1998-11-09 2000-12-08 Inst Francais Du Petrole Dispositif pour tester des echantillons de roches a pression et temperature relativement elevees
FR2792678B1 (fr) 1999-04-23 2001-06-15 Inst Francais Du Petrole Procede de recuperation assistee d'hydrocarbures par injection combinee d'une phase aqueuse et de gaz au moins partiellement miscible a l'eau
FR2798734B1 (fr) 1999-09-21 2001-10-12 Inst Francais Du Petrole Methode optimisee pour determiner des parametres physiques d'un echantillon soumis a centrifugation
IT1313693B1 (it) * 1999-11-26 2002-09-09 Eni Spa Procedimento per determinare in continuo l'interazione tra fluidi diperforazione e formazione argillose.
IT1313691B1 (it) * 1999-11-26 2002-09-09 Eni Spa Procedimento per verificare l'efficacia dei fluidi di perforazionenello stabilizzare le pareti di pozzi petroliferi.
AU1939400A (en) * 1999-12-14 2001-12-03 Cristina Crawford Multi-directional permeameter
FR2810736B1 (fr) * 2000-06-23 2002-09-20 Inst Francais Du Petrole Methode pour evaluer des parametres physiques d'un gisement souterrain a partir de debris de roche qui y sont preleves
CA2342119A1 (fr) 2001-03-23 2002-09-23 Universite Du Quebec A Montreal (Uqam) Automatisation du test d'absorption d'eau dans les materiaux poreux
GB2374425A (en) * 2001-04-12 2002-10-16 Nigel Alexander Feetham Porosity measuring device for building materials
FR2836228B1 (fr) * 2002-02-21 2005-08-19 Inst Francais Du Petrole Methode et dispositif pour evaluer des parametres physiques d'un gisement souterrain a partir de debris de roche qui y sont preleves
FR2844355B1 (fr) 2002-09-11 2005-03-25 Inst Francais Du Petrole Methode de mesure de la mouillabilite de roches par resonnance magnetique nucleaire
DE10315391A1 (de) * 2003-04-04 2004-11-04 Federal-Mogul Sealing Systems Gmbh Verfahren und Vorrichtung zur Bestimmung stofflicher Emissionen von Prüflingen
FR2854462B1 (fr) * 2003-04-29 2005-06-24 Inst Francais Du Petrole Methode d'evaluation du facteur de formation d'un gisement souterrain a partir de mesures sur des debris de forage qui y sont preleves
US20040255646A1 (en) * 2003-06-17 2004-12-23 Valeriu Smiricinschi Method for control gas diffusion and bubble formation in liquid porosimetry
FR2874696B1 (fr) * 2004-09-02 2007-03-23 Inst Francais Du Petrole Methode de determination de parametres d'ecoulement multiphasique d'un milieu poreux avec prise en compte de l'heterogeneite locale
DE102005010847B4 (de) * 2005-03-07 2007-08-02 Rea Elektronik Gmbh Vorrichtung zur Messung einer austretenden Flüssigkeit
FR2884923B1 (fr) 2005-04-26 2007-10-19 Inst Francais Du Petrole Methode et dispositif pour evaluer des parametres d'ecoulement et des parametres electriques d'un milieu poreux.
KR100642304B1 (ko) 2005-10-31 2006-11-02 한국지질자원연구원 하중압의 변화에 따른 미고결 시료의 물성측정장치
US7472588B2 (en) * 2007-04-18 2009-01-06 Sorowell Production Services Llc Petrophysical fluid flow property determination
US7567079B2 (en) * 2007-06-08 2009-07-28 University Of New Brunswick Methods suitable for measuring capillary pressure and relative permeability curves of porous rocks
GB0721506D0 (en) * 2007-11-02 2007-12-12 Corpro Systems Ltd Method and apparatus
US9291050B2 (en) * 2008-09-30 2016-03-22 Schlumberger Technology Corporation Determining formation wettability from dielectric measurements
US8201439B2 (en) * 2009-11-02 2012-06-19 Schlumberger Technology Corporation Material wettability characterization and chemical additive evaluation
US8507868B2 (en) * 2011-03-04 2013-08-13 Landmark Graphics Corporation Systems and methods for determining fluid mobility in rock samples
GB2492795B (en) * 2011-07-12 2013-11-20 Schlumberger Holdings Testing imbibition of liquid
CN102636574A (zh) * 2012-04-10 2012-08-15 华侨大学 一种工程用承压渗透式声测探头
DE102012012589A1 (de) 2012-06-19 2013-12-19 Technische Universität Bergakademie Freiberg Kernhalter mit Manteldruckbeaufschlagung
KR101481383B1 (ko) * 2014-02-05 2015-01-14 전남대학교산학협력단 유체주입을 통한 원유생산증진 시스템 및 방법
US9835762B2 (en) 2014-02-06 2017-12-05 Schlumberger Technology Corporation Petrophysical rock characterization
US9417168B2 (en) * 2014-03-10 2016-08-16 Dmar Engineering, Inc. Fatigue testing
US10197490B2 (en) * 2015-06-02 2019-02-05 Dci Corporation Apparatus, method, and system for measuring relative permeability of immiscible fluids
CN104931405B (zh) * 2015-06-16 2017-12-22 南京华研智能科技有限公司 密封渗透装置及采用密封装置的全自动混凝土抗渗仪
US9341558B1 (en) * 2015-08-25 2016-05-17 King Saud University System and method for measuring permeation properties of concrete and porous materials
CN108181224A (zh) * 2018-01-05 2018-06-19 中国石油大学(华东) 油藏条件下驱替及吸吮毛管力曲线联测装置及方法
US11340208B2 (en) 2018-01-23 2022-05-24 Total Se Method and apparatus for analyzing a rock sample
CN109030315B (zh) * 2018-08-22 2020-11-27 福州大学 低应力起始一维压缩-渗透试验***及其工作方法
CN109883917B (zh) * 2019-01-24 2021-06-04 西南石油大学 一种模拟基质-裂缝静动态渗吸排油的实验装置及方法
CN110068527B (zh) * 2019-04-26 2020-07-10 中国矿业大学 一种非平衡状态下煤岩渗透率自动连续测试装置及其方法
US11249001B2 (en) * 2019-05-23 2022-02-15 Saudi Arabian Oil Company Determination of scanning loops of capillary pressure and relative permeability curves and wettability distribution of rock samples
FR3099577B1 (fr) 2019-07-30 2021-08-13 Cydarex Dispositif pour mesurer des caractéristiques physiques d'un échantillon solide poreux
CN110261285B (zh) * 2019-08-01 2022-04-29 西南石油大学 一种基于超声衰减的自发渗吸测量装置及方法
WO2021067720A1 (fr) * 2019-10-04 2021-04-08 Total S.E. Système de mesure de pression distribuée destiné à des expériences de balayage sur carotte
CN111022009B (zh) * 2019-12-27 2024-07-12 延长油田股份有限公司志丹采油厂 一种脉冲作用下渗吸实验装置及实验方法
CN112096357B (zh) * 2020-09-16 2021-10-15 中国石油大学(北京) 稠油热采相对渗透率测试的产油量校正方法、装置及设备
US11454097B2 (en) 2021-01-04 2022-09-27 Saudi Arabian Oil Company Artificial rain to enhance hydrocarbon recovery
US11965848B2 (en) 2021-12-03 2024-04-23 Saudi Arabian Oil Company Method for determining the electrical properties of a core sample
US11828693B2 (en) * 2022-02-11 2023-11-28 Saudi Arabian Oil Company Centrifuge method for evaluating contact angle and wettability alteration

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4487056A (en) * 1982-09-28 1984-12-11 Phillips Petroleum Company Determination of the imbibition characteristics of a rock formation
US4506542A (en) * 1983-04-22 1985-03-26 Chandler Engineering Company Apparatus and procedure for relative permeability measurements
US4543821A (en) * 1983-12-14 1985-10-01 Texaco Inc. Method and apparatus for measuring relative permeability and water saturation of a core
US4868751A (en) * 1987-09-11 1989-09-19 Mobil Oil Corporation Method for determining relative permeability of a subterranean reservoir
US4926128A (en) * 1989-02-13 1990-05-15 Mobil Oil Corporation Method for utilizing measured resistivities of porous rock under differing fluid saturations to identify fluid distribution equilibrium
FR2666147B1 (fr) * 1990-08-27 1992-10-16 Inst Francais Du Petrole Mesure de la repartition des concentrations de constituants d'un syteme en centrifugation par emission/reception de signaux mecaniques.
US5345819A (en) * 1990-10-22 1994-09-13 Chevron Research And Technology Company Method and apparatus for wellbore stability analysis
US5069065A (en) * 1991-01-16 1991-12-03 Mobil Oil Corporation Method for measuring wettability of porous rock
US5079948A (en) * 1991-01-28 1992-01-14 Mobil Oil Corporation Method for conducting capillary pressure drainage and imbibition on a core sample of a porous rock
US5209104A (en) * 1992-01-23 1993-05-11 Mobil Oil Corporation Method for desaturating a porous rock for electrical resistivity measurements
US5164672A (en) * 1992-02-19 1992-11-17 Mobil Oil Corporation Method for measuring electrical resistivity of a core sample of porous rock during water drainage and imbibition
US5297420A (en) * 1993-05-19 1994-03-29 Mobil Oil Corporation Apparatus and method for measuring relative permeability and capillary pressure of porous rock

Also Published As

Publication number Publication date
NO315822B1 (no) 2003-10-27
FR2708742B1 (fr) 1995-09-01
GB2280512B (en) 1996-12-11
US5679885A (en) 1997-10-21
NO942796D0 (no) 1994-07-27
GB9414998D0 (en) 1994-09-14
NO942796L (no) 1995-01-30
CA2129166C (fr) 2007-07-10
GB2280512A (en) 1995-02-01
FR2708742A1 (fr) 1995-02-10

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