CA1178763A - Device for uniform web pinning - Google Patents

Device for uniform web pinning

Info

Publication number
CA1178763A
CA1178763A CA000436819A CA436819A CA1178763A CA 1178763 A CA1178763 A CA 1178763A CA 000436819 A CA000436819 A CA 000436819A CA 436819 A CA436819 A CA 436819A CA 1178763 A CA1178763 A CA 1178763A
Authority
CA
Canada
Prior art keywords
web
quench roll
vacuum
roll
zone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
CA000436819A
Other languages
French (fr)
Inventor
David E. Heyer
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
DuPont Teijin Films US LP
Original Assignee
EI Du Pont de Nemours and Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from US06/229,159 external-priority patent/US4310295A/en
Application filed by EI Du Pont de Nemours and Co filed Critical EI Du Pont de Nemours and Co
Priority to CA000436819A priority Critical patent/CA1178763A/en
Application granted granted Critical
Publication of CA1178763A publication Critical patent/CA1178763A/en
Expired legal-status Critical Current

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Abstract

TITLE
Device for Uniform Web Pinning ABSTRACT OF THE DISCLOSURE
A device for uniform pinning of molten web material onto a quench roll by means of at least two vacuum zones interacting through a baffle, one vacuum zone extending past the line of contact of the web on the quench roll to encompass a portion of the web edge laid onto the casting drum.

Description

l 178763 TITLE
Device for Uniform Web Pinning 8AC~GROUND
FIELD OF THE INVENTION
During the manufacture of many thermoplastic films, especially films of polyethylene terephthalate, a molten film web is cooled by extrusion onto a quench roll casting drum. Uniform pinning of the web to the quench roll is facilitated by the removal of air proximate the line of contact between the web and the quench roll by vacuum forces to eliminate such air from being trapped under the web during the lay-down so as to mitigate irregularities in the uniformity of cast shee~ing, especially prominent at high speed operation. ~his invention is directed toward improvements in eliminating air pockets and reducing irregularities caused by air turbulence resulting from the vacuum forces applied to the line of-contact between the quench roll and the web.
DESCRIPTION OF PRIOR ART
In the production of film from certain thermoplastic polymers in which such film is formed at temperatures above or near the polymer melting point, it is important to quickly cool the freshly formed film to a temperature below the second order transition temperature, i.e., that temperature at which, as temperature decreases, the polymer goes from a flexible state to a more rigid, glassy state, in order to prevent crystallization which would interfere with subsequent orientation of the film. A
number of devices have been employed to create more intimate contact between the web and the quench roll, the most prominent being, generally, forced air D-5094-1 35 pinning, ele~trostatic pinning, and vacuum pinning.

1 1787~3 Forced air pinning, where the molten web is urged against the quench roll by means of air pressure exerted against the upper surface of the cast web, is of limited use during high speed operation due to film distortions created by air being trapped under the molten web as the web is laid onto the quench roll. Electrostatic pinning, where the cast web is held to the quench roll by means of electrostatic forces, has also been limited to slower operation as air bubbles are trapped under the web at high speeds.
In the recent past, the removal of the air proximate the contact line between the web and the quench roll has been attempted with partial success by vacuum forces which achieve varying degrees of lS uniformity in the pinning process. A major weakness in the use of these vacuum forces stems from air turbulence created by the vacuum, causing the web to vibrate as it flows onto the quench roll, such vibration resulting in a lack of uniformity in the 20 casting and cooling process and hence, the web product. Prior art has exhibited some reduction of air turbulence by utilizing successive vacuum zones with porthole like interconnections or with individual vacuum forces, however, significant air 25 ~urbulence at the line of contact between the web and the quench roll and consequent pinning and quenching irregularities remain. Further, in prior art devices, ambient air movement drawn past the edges of the extruded web, hereinafter "edge leak airl', is 30 essentially straight back, parallel with the movement of the casting drum. This leak air movement gives rise to significant air turbulence proximate the web edge bead and has been shown to bend the edge of the molten web back as the web is flowing from the die 1 ~787~3 lip to the quench roll giving the web edge a scalloped appearance. This scalloping of the edge of the web before it is laid onto the quench roll is referred to herein as bead wobble. In prior art 5 devices, edge leak air necessarily enters the vacuum - zone proximate the molten web through the opening between the edge of the molten web and the vacuum device, thus, creating air turbulence within the device proximate the extruded web. Prior art 10 devices, while mitigating air turbulence and, therefore, viDration of the extruded web, still leave much to be desired at high film manufacturing speeds. No prior suggestion of devices similar to this invention is known wherein there are two vacuum 15 zones interracting only through a close fitting baffle, or skimmer; -- one zone, hereinafter the primary zone, being proximate the line of contact of the web onto the casting drum, the other zone, hereinafter the secondary zone, being distal such 20 line of contact relative to the primary zone, where the vacuum forces acting on the secondary zone do not create air turbulence within the primary zone due to the skimmer. Further, no prior suggestion is known to further mitigate bead wobble by extending the 25 secondary zone to encompass both edges of the web as it is laid onto the drum by use of edge seals in conjunction with a quiescent vacuum zone such that the the edge leak air drawn into the edge seal is substantially perpendicular to the movement of the 30 casting drum.
SUMMARY OF THE INVENTION
During the pinning of molten cast ~eb material onto a quench roll casting drum it is desirable to remove air from the contact line of the l 1787~3 web and the casting drum so as to prevent air from being trapped under the web, while at the same time keeping the turbulence caused by such air removal at a minimum to attain uniform pinning of the web onto the drum. Accordingly, the present invention relates to a vacuum pinning device wherein extruded web material is uniformly pinned to a quench roll casting drum comprising: a vacuum shoe housing at least two interacting vacuum zones, primary and secondary; said primary zone located proximate the surface of the web at the line of contact between the web and the quench roll casting drum; said primary zone having a crevice which runs under a baffle fitted proximate the quench roll casting drum and joining the primary and secondary zones; said secondary zone positioned distal the line of contact between the web and the quench roll casting drum relative to the primary zone; said secondary zone having its outer perimeter surrounded by a proximity seal-with the quench roll casting drum; said secondary zone having a vacuum source connected thereon, said vacuum source being the posterior vacuum source.
Further, the subject invention relates to an edqe seal vacuum chamber, extending from and interconnected with the secondary zone, with one side open to a molten web edge as said web contacts the quench roll; said open side extending on both sides of the contact line of the web with the ~uench roll casting drum whereby the vacuum chamber encompasses a portion of the web on both sides of said contact line; said edge seal vacuum chamber having a vacuum source downstream from an extension of the die lip opening projected onto the surface of the quench roll relative to the movement of the drum, such vacuum l 178~B3 source being the anterior vacuum source independent from the posterior vacuum source connected on the secondary zone; whereby the primary zone is quiescent relative to the secondary zone because the primary zone is isolated from turbulence caused by the posterior vacuum source by means of the baffle, and isolated from edge leak air by means of the edge seal vacuum chamber wherein said edge leak air is drawn into the edge seal vacuum chamber such that the edge leak air is drawn into the edge seal vacuum chamber substantially perpendicular to the movement of the casting drum.
BRIEF DESCRIPTION OF THE DRAWINGS
FIG. 1 is a perspective view of an 15 embodiment of the subject invention.
FIG. 2 is a cross section side view of an embodiment of the device of this invention.
FIG. 3 is a bottom view o~ an embodiment of the device of this invention.
20FIG. 4 is a perspective view of the edge seal of the subject invention.
DETAILED DESCRIPTION OF PREFERRED EMBODIMENT
In FIG. 1, molten thermoplastic web 6 is extruded through extrusion die 1 onto a quench roll 25 casting drum 4 rotating in the direction of arrow 13. Other means of cooling the molten web may also be used such as a moving quench belt. FIG. 1 also depicts the perspective position of vacuum shoe 7, support rollers 25 and edge seal 5 relative to 30 extrusion die 1. Further, the position of primary zone 8 is shown relative to baffle 9, secondary zone 10, labyrinth seal 11 and vacuum source 12.
In FIG. 2 extrusion die 1 can be positioned vertical with the radius of ~uench roll 4, as shown 1 1787~

in F~G. 2, position 1, tilted backward toward the quench roll 2S indicated by the phantom outline identified in FIG. 2 as position 2, or any place between those locations. The preferred position is 2 which allows extrusion of web 6 to be more parallel with the movement of quench roll 4, such preferred position 2 accomodating the draw on the extruded web due to the rotation of the quench roll. Spring seal 3 supports the various positioning of extruder die 1.
In FIG. 2, vacuum shoe 7 houses two vacuum zones interacting only by way of baffle 9 fit closely to quench roll 4, such vacuum zones being d~signated as primary zone 8 and secondary 20ne 10. Primary zone 8 is proximate the surface of web 6 at line of 15 contact 16 between web 6 and quench roll 4.
Secondary zone 10 is distal the line of contact 16 relative to primary zone 8 with edge seals 5 fitted closely to quench roll 4 and serving as extensions of secondary zone 10 encompassing a portion of the edge 20 of molten web 6 as it is laid onto quench roll 4 as said roll rotates in the direction of arrow 13. Edge seals 5 can be used independently witho~t being interconnected with a vacuum zone such as secondary zone 10, for example with a single vacuum chamber 25 device, as a vacuum chamber fitted closely to quench roll 4, with one side open to the molten web edge as said web contacts the quench roll, said open side extending on both sides of the contact line of the web with the quench roll and said edge seals having 30 vacuum source 24 downstream from an extension of the die lip opening projected onto the quench roll, prefera~ly a distance of 0.6 cm to 1.4 cm.
In FIG. 2 and FI~. 3, secondary zone 10 is surrounded by a labyrinth seal 11 which forms a 3~

1 17~7~

proximity seal between vacuum shoe 7 and quench drum 4 under which exists a crevice of from about 0.05 cm to 0.17 cm, maintained by cor.tact of support rollers 25 with drum 4, such labyrinth seal 11 admitting perimeter leak air l7 into secondary zone 10. Primary zone 8 is located adjacent quench roll 4 to leave about a 0.05 cm to 0.17 cm crevice under skimmer 9 to join the primary zone 8 with secondary zone 10. Vacuum source 12 operates directly on secondary zone 10 drawing all leak air along paths 27 and out vacuum source 12, vacuum sources being applied to the primary zone 8 only through the crevice under the skimmer 9.
In FIG. 3 perimeter leak air is drawn under the labyrinth seal 11 into the secondary zone 10 along paths 17 and is exhausted via vacuum source 12, creating high air turbulence depicted by paths 27 in secondary zone 10. In contrast, perimeter leak air does not enter primary zone 8. The isolation of
2~ primary zone 8 is made nearly complete by the use of edge seal 5 in conjunction wi~h the secondary vacuum zone. Edge seals 5 include vacuum source 24 which acts on zone A, an extension of secondary zone 10 further defined as that portion of edge seals 5 downstream from phantom line 26 drawn perpendicular to the movement of the quench roll as an extension of the die lip opening projected onto the surface of the drum into the edge seal. The vacuum force of vacuum source 24 is greater than that of vacuum source 12, the total effect being the creation of a slight pressure gradient ~etween zone A and vacuum source 12, such that the path 15 of leak air is substantially perpendicular to the movement of the casting drum into zone A and then backward into the .

1 178~7B3 secondary zone. In contrast, without use of edge seal 5, vacuum source 12 acting alone causes edge leak air to be drawn essentially parallel to the movement of the quench roll into the primary zone, such air movement tending to create turbulence around the bead in the primary zone and hence tending to make unstable the edges of molten web 6 causing further bead wobble and associated lay-down instabilities. For maximum effect, edge seal 5 must 10 be positioned such that vacuum source 24 penetrates zone A downstream from phantom line 26 relative to the movement of the quench roll, preferably a distance of 0.6 cm to 1.4 cm. This allows the cooperation of vacuum source 24 and vacuum source 12 to be of greatest effect in keeping edge leak air on paths 15 and away from the primary zone.
Consequently, primary zone 8 is a quiescent zone and the molten web edges exhibit reduced bead wobble and hence lay uniformly onto the quench roll as said roll rotates in the direction of arrow 13.
In FIG. 4 edge seal S is shown enlarged in perspective to web 6 as said web is extruded from extrusion die 1 to contact the quench roll 4.
Phantom line 26 is an extention of the die lip 25 opening projected onto the quench roll to define one side of zone A. Due to the influence of vacuum source 24, edge leak air is drawn away from the edge of web 6 along path 15 substantially perpendicular to the movement of drum 4 and into secondary zone 10.
30 This cooperation between vacuum source 24 and secondary zone 10 eliminates edge leak air flow into primary zone a and stabilizes bead lay-down.

ExamPle 1 Polyethylene terephthalate, having an intrinsic viscosity of about 0.53, is extruded at a rate of 408 kg/hour from a 50 cm x 0.18 cm slit die S and cast on a quench roll spaced 0.317 cm from the die lip. Utilizing a device such as that depicted by the figures herein, a differential pressure of 1.57 m H2O is applied to the extruded web with vacuum sources 12, and a differential pressure of greater than 1.57 m H2O is applied by vacuum source 24. At a take-off rate of 45.7 m/min the edges of the extruded web are stable. Pinning is complete and the appearance of the cast sheet is excellent.
ExamPle 2 Polyethylene terephthalate as in Example 1 is extruded at a rate of 408 kg/hour through a 25 cm x O.Z3 cm slit die and cast on a quench rol~
spaced 0.317 cm below the die lip. Utiiizing the device of Example 1, the differential pressure 20 applied by vacuum source 12 is 2 m H2O and that applied by vacuum source 24 is 4.57 m H2O. At a take-off rate of 59.74 m/min, the edges of the extruded web show no tendency to wobble. Appearance of the cast sheet is excellent.
ExamPle 3 Example 2 is repeated except that the polymer extrusion rate is 499 kg/hour, the take-off rate is 80.16 m/min, and the differential pressure applied by vacuum source 12 is increased to 3.68 m 30 ~2 The quality of the resulting film product is similar to that of Example 2.
ExamPle 4 This comparative example is to show how an increased rate of extrusion creates excessive bead 35 wobble when edge seals 5 are not employed.

1 ~78~t;3 The device of this e~ample included two vacuum zones interconnected by means of a rectangular slot 1.27 cm x 63.5 cm cut in the wall separating the two zones. Polyethylene terephthalate melt is extruded at a rate of 272 kg/hour from a 50 cm x 0.18 cm slit die and cast on a rotating quench roll spaced 0.317 cm from the die lip. The web at the point of roll contact is subjected to a vacuum pressure of 50.8 cm H20 created by vacuum source 12. No effor-is made to restrict or in any way redirect thenatural flow of leak air past the edges of the extruded web into the vacuum chambers. At a take-off rate of 45.7 m/min and a cast film thickness of .163 milimeters, the edges of the extruded web wobble in such a manner as to cause the cast film to be of nonuniform width. Increasing pressure and take-off rates increases wobble. Decreasing pressure and take-off rates decreases wobble. In contrast, the increase of pressure and take-off rates when using the device of the subject invention did not display such undesirea~le bead wobble.
ExamDle 5 In this comparative example, the same device as Example 4 is used under the following conditions:
25 Die to drum gap - 0.274 cm; die width - 50.8 cm; rate of extrusion - 272 kg/hour; quench roll speed 43.9 m/min; vacuum 50.8 cm ~2 The device of the subject invention was then operated under similar condi~ions.
To determine the quality of pinning as a function of cast film thickness variation in the machine direction, peak to valley measurements are made at twenty consecutive points 7.5 centimeters apart and the measured thickness variations are 35 averased. The thickness variations in film cast .' 10 using the subject invention is about 0.75 to 1.0%
and, under similar conditions, but using the device of this comparative example, the thickness variation is about twice that value or 1.5 to 2.0%.
This application is a division of copending application Serial No. 394 963, filed January 26, 1982.

Claims (2)

The embodiments of the invention in which an exclusive property or privilege is claimed are defined as follows:
1. A device for uniformly and continuously pinning an extruded thermoplastic web to a quench roll casting drum comprising:
an edge seal vacuum chamber with one side open to a molten web edge as said web contacts a quench roll;
said open side extending on both sides of the contact line of the web with the quench roll wherein the edge seal vacuum chamber encompasses a portion of the web on both sides of said contact line;
said edge seal vacuum chamber having a vacuum source downstream from an extension of the die lip opening projected onto the quench roll relative to the movement of the roll;
whereby, ambient leak air is drawn past the edges of the web into the vacuum chamber such that said leak air is not trapped under the molten web as the web is laid onto the quench roll.
2. The device of Claim 1 wherein the vacuum source is from 0.6 cm to 1.4 cm downstream from the extension of the die lip opening projected onto the quench roll.
CA000436819A 1981-01-28 1983-09-15 Device for uniform web pinning Expired CA1178763A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CA000436819A CA1178763A (en) 1981-01-28 1983-09-15 Device for uniform web pinning

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US06/229,159 US4310295A (en) 1981-01-28 1981-01-28 Device for uniform web pinning
US229,159 1981-01-28
CA000394963A CA1177621A (en) 1981-01-28 1982-01-26 Device for uniform web pinning
CA000436819A CA1178763A (en) 1981-01-28 1983-09-15 Device for uniform web pinning

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CA000394963A Division CA1177621A (en) 1981-01-28 1982-01-26 Device for uniform web pinning

Publications (1)

Publication Number Publication Date
CA1178763A true CA1178763A (en) 1984-12-04

Family

ID=27167193

Family Applications (1)

Application Number Title Priority Date Filing Date
CA000436819A Expired CA1178763A (en) 1981-01-28 1983-09-15 Device for uniform web pinning

Country Status (1)

Country Link
CA (1) CA1178763A (en)

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