BR0310005A - Método para a produção de ácido orgânico - Google Patents
Método para a produção de ácido orgânicoInfo
- Publication number
- BR0310005A BR0310005A BR0310005-7A BR0310005A BR0310005A BR 0310005 A BR0310005 A BR 0310005A BR 0310005 A BR0310005 A BR 0310005A BR 0310005 A BR0310005 A BR 0310005A
- Authority
- BR
- Brazil
- Prior art keywords
- acid
- organic acid
- pka
- ammonium salt
- recycled
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/50—Use of additives, e.g. for stabilisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/02—Preparation of carboxylic acids or their salts, halides or anhydrides from salts of carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
Abstract
"MéTODO PARA A PRODUçãO DE áCIDO ORGâNICO". Um novo método é fornecido pelo qual um ácido orgânico livre pode ser produzido particularmente a partir de um sal de amónio de um ácido orgânico tendo um ponto de ebulição elevado obtenível pela bioconversão de uma fonte de carbono na presença de um agente de neutralização, eficientemente em um custo baixo, e o material usado para a reação e um subproduto podem ser reciclados para a reutilização sem ser disposto. Um sal de amónio do ácido orgânico A tal como um ácido dicarboxílico, um ácido tricarboxílico ou um aminoácido é submetido à cristalização reativa por meio do ácido B como um ácido monocarboxílico que satisfaz a seguinte fórmula (1), para separar o ácido orgânico A livre na forma sólida: pKa (A) <243> pKa (B) (1) onde pKa (A) e pKa (B) representam índices de ionização do ácido orgânico A e do ácido B, respectivamente, contanto que quando eles tiverem valores plurais, eles representam o pKa mínimo entre eles. O licor-mãe de cristalização após a precipitação e separação do ácido orgânico A é, após separação do ácido B e depois um sal de amónio do ácido B, reciclado para uso na etapa de cristalização reativa. O sal de amónio do ácido B é decomposto em ácido B e amónia, os quais são reciclados para uso na etapa de cristalização reativa e como um agente de neutralização na etapa de bioconversão, respectivamente.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2002135656 | 2002-05-10 | ||
JP2002231741 | 2002-08-08 | ||
JP2002231740 | 2002-08-08 | ||
JP2002305989 | 2002-10-21 | ||
PCT/JP2003/005826 WO2003095409A1 (fr) | 2002-05-10 | 2003-05-09 | Procede de production d'acide organique |
Publications (1)
Publication Number | Publication Date |
---|---|
BR0310005A true BR0310005A (pt) | 2005-02-15 |
Family
ID=29424660
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BR0310005-7A BR0310005A (pt) | 2002-05-10 | 2003-05-09 | Método para a produção de ácido orgânico |
Country Status (7)
Country | Link |
---|---|
US (4) | US7217837B2 (pt) |
EP (1) | EP1505052A4 (pt) |
CN (1) | CN100545139C (pt) |
AU (1) | AU2003231444A1 (pt) |
BR (1) | BR0310005A (pt) |
MY (1) | MY137537A (pt) |
WO (1) | WO2003095409A1 (pt) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100368047C (zh) * | 2002-12-27 | 2008-02-13 | 住友化学株式会社 | 结晶方法和结晶装置 |
WO2005045049A1 (ja) * | 2003-11-07 | 2005-05-19 | Mitsubishi Chemical Corporation | 有機酸アンモニウム溶液の製造方法 |
EP1686182A1 (en) * | 2003-11-07 | 2006-08-02 | Mitsubishi Chemical Corporation | Method for producing organic acid salt |
EP3925997B1 (en) | 2005-04-22 | 2024-07-17 | Mitsubishi Chemical Corporation | Biomass-resource-derived polyester and production process thereof |
CN102066305B (zh) | 2008-06-20 | 2015-11-25 | 旭化成化学株式会社 | α-羟酸的制造方法 |
RU2490249C2 (ru) * | 2008-08-28 | 2013-08-20 | Роман Анатольевич ТРУНИН | Способ получения аммонийных солей фумаровой или янтарной кислоты |
BRPI0922836B1 (pt) * | 2008-12-02 | 2018-09-25 | Purac Biochem Bv | processo para a preparação de um sal de succinato monovalente |
KR20120099154A (ko) | 2009-12-31 | 2012-09-06 | 미리안트 코포레이션 | 암모늄 숙신산염을 함유하고 있는 발효 배지로부터의 숙신산의 정제 |
US8624059B2 (en) * | 2010-03-26 | 2014-01-07 | Bioamber S.A.S. | Processes for producing monoammonium succinate from fermentation broths containing diammonium succinate, monoammonium succinate and/or succinic acid, and conversion of monoammonium succinate to succinic acid |
US8410291B2 (en) * | 2010-04-01 | 2013-04-02 | BioAmber International S.á.r.l. | Processes for the production of hydrogenated products |
US8399687B2 (en) | 2010-04-01 | 2013-03-19 | Bioamber International S.A.R.L. | Processes for the production of hydrogenated products |
KR20130020779A (ko) | 2010-04-01 | 2013-02-28 | 바이오엠버 인터내셔널 에스.에이.알.엘. | 숙신산염으로부터 테트라하이드로퓨란, 감마-부티로락톤 및/또는 부탄디올의 제조방법 |
CN102858731A (zh) | 2010-04-01 | 2013-01-02 | 生物琥珀酸有限公司 | 用于从含有琥珀酸二铵的发酵液制备琥珀酸的方法 |
CN103228605A (zh) * | 2010-04-30 | 2013-07-31 | 生物琥珀酸有限公司 | 用于从含有nh4+-ooc-r-coo-nh4+化合物的发酵液制备hooc-r-cooh化合物酸的方法 |
JP2013524834A (ja) * | 2010-04-30 | 2013-06-20 | ビオアンブ,ソシエテ パ アクシオンス シンプリフィエ | Nh4+−ooc−r−coo−nh4+化合物及び/又はhooc−r−cooh化合物の酸を含む発酵培地からのnh4+−ooc−r−cooh化合物の製造方法、及びnh4+−ooc−r−cooh化合物のhooc−r−cooh化合物の酸への変換 |
CN102971298A (zh) * | 2010-06-16 | 2013-03-13 | 生物琥珀酸有限公司 | 从含有己二酸二铵或己二酸一铵的发酵液制备己内酰胺及其衍生物的方法 |
CN102249889B (zh) * | 2010-12-13 | 2014-07-23 | 日照金禾博源生化有限公司 | 一种从柠檬酸母液中提取丁二酸的方法 |
CN102181490B (zh) * | 2011-03-21 | 2012-12-12 | 中粮生物化学(安徽)股份有限公司 | 一种生产柠檬酸的方法 |
CN103045299A (zh) * | 2011-10-17 | 2013-04-17 | 中国石油天然气股份有限公司 | 化学沉淀原油脱钙循环方法 |
DE102013225215A1 (de) | 2013-12-06 | 2015-06-11 | Thyssenkrupp Ag | Verfahren zur Herstellung und Isolierung von Carbonsäureestern |
EP3262080A1 (en) * | 2015-02-24 | 2018-01-03 | The Procter and Gamble Company | Process for molecular weight reduction of ethersuccinylated polysaccharides |
CN114524722A (zh) * | 2020-10-31 | 2022-05-24 | 中国石油化工股份有限公司 | 一种提取长链二元酸的方法 |
CN112552164B (zh) * | 2020-12-08 | 2022-12-09 | 日照金禾博源生化有限公司 | 一种从不合格柠檬酸钠母液中提取苹果酸的工艺方法 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2090947A (en) * | 1934-10-02 | 1937-08-24 | Celanese Corp | Recovery of acidic and basic reagents |
US3488386A (en) * | 1967-06-09 | 1970-01-06 | Quaker Oats Co | Process for recovering acetic acid |
CA955876A (en) * | 1970-10-15 | 1974-10-08 | Edward G. Adamek | Separation of dicarboxylic acids |
US3968152A (en) * | 1972-10-06 | 1976-07-06 | The Lummus Company | Production of aromatic carboxylic acids |
US3833646A (en) * | 1973-04-16 | 1974-09-03 | Sun Research Development | Ammonium aromatic carboxylate conversion to the corresponding acids |
FR2308611A1 (fr) * | 1975-04-24 | 1976-11-19 | Rhone Poulenc Ind | Procede de recuperation de l'acide acetique a partir de ses solutions aqueuses de faible concentration |
JPS6150937A (ja) * | 1984-08-20 | 1986-03-13 | Asahi Chem Ind Co Ltd | カルボン酸アンモン水溶液からカルボン酸の製造法 |
JPS63264546A (ja) * | 1987-04-20 | 1988-11-01 | Asahi Chem Ind Co Ltd | 工業廃酸を利用したカルボン酸の製造法 |
KR920000416B1 (ko) * | 1989-10-13 | 1992-01-13 | 재단법인 한국화학연구소 | 고순도 테레프탈산의 제조방법 |
US5132456A (en) * | 1991-05-07 | 1992-07-21 | The Regents Of The University Of California | Sorption of carboxylic acid from carboxylic salt solutions at PHS close to or above the pKa of the acid, with regeneration with an aqueous solution of ammonia or low-molecular-weight alkylamine |
ES2093934T3 (es) * | 1992-09-30 | 1997-01-01 | Bp Chem Int Ltd | Acidos carboxilicos fijados de forma liberable. |
GB9301532D0 (en) * | 1993-01-27 | 1993-03-17 | Bp Chem Int Ltd | Releasably bound hydroxycarboxylic acids |
US5958744A (en) * | 1997-08-18 | 1999-09-28 | Applied Carbochemicals | Succinic acid production and purification |
-
2003
- 2003-05-08 MY MYPI20031729A patent/MY137537A/en unknown
- 2003-05-09 CN CNB038105950A patent/CN100545139C/zh not_active Expired - Lifetime
- 2003-05-09 BR BR0310005-7A patent/BR0310005A/pt not_active Application Discontinuation
- 2003-05-09 AU AU2003231444A patent/AU2003231444A1/en not_active Abandoned
- 2003-05-09 WO PCT/JP2003/005826 patent/WO2003095409A1/ja active Application Filing
- 2003-05-09 EP EP03725769A patent/EP1505052A4/en not_active Withdrawn
-
2004
- 2004-11-01 US US10/976,822 patent/US7217837B2/en not_active Expired - Lifetime
-
2007
- 2007-03-20 US US11/688,624 patent/US20070167649A1/en not_active Abandoned
- 2007-03-20 US US11/688,647 patent/US20070161816A1/en not_active Abandoned
-
2008
- 2008-11-17 US US12/272,523 patent/US20090137843A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
MY137537A (en) | 2009-02-27 |
WO2003095409A1 (fr) | 2003-11-20 |
US20050070738A1 (en) | 2005-03-31 |
US20090137843A1 (en) | 2009-05-28 |
AU2003231444A1 (en) | 2003-11-11 |
CN100545139C (zh) | 2009-09-30 |
EP1505052A1 (en) | 2005-02-09 |
CN1653027A (zh) | 2005-08-10 |
EP1505052A4 (en) | 2006-05-24 |
US20070167649A1 (en) | 2007-07-19 |
US20070161816A1 (en) | 2007-07-12 |
US7217837B2 (en) | 2007-05-15 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B06A | Patent application procedure suspended [chapter 6.1 patent gazette] | ||
B15K | Others concerning applications: alteration of classification |
Free format text: ALTERADA A CLASSIFICACAO DE C07C 51/02 PARA INT.CL. C07C 51/02, 51/50 Ipc: C07C 51/02 (2006.01) |
|
B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: INDEFIRO O PEDIDO DE ACORDO COM O(S) ARTIGO(S) 8 E 13 DA LPI. |
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B09B | Patent application refused [chapter 9.2 patent gazette] |
Free format text: MANTIDO O INDEFERIMENTO UMA VEZ QUE NAO FOI APRESENTADO RECURSO DENTRO DO PRAZO LEGAL. |