AU629992B2 - Cyclone separator - Google Patents

Description

629992 COMMONWEALTH OF AUSTRALIA PATENTS ACT 1952 COMPLETE SPECIFICATION (Original) FOR OFFICE USE Class Int. Class Application Number: Lodged: Complete Specification Lodged: Accepted: Published: Priority: Related Art: e Name of Applicant: CONOCO SPECIALTY PRODUCTS, INC.

o e Address of Applicant: 600 North Dairy Ashford Road, Houston, Texas, United States of America Actual Inventor(s): Mark Ian GREY of 6 Portland Place, South Yarra 3141, Victoria, Australia Address for Service: DAVIES COLLISON, Patent Attorneys, 1 Little Collins Street, Melbourne, 3000.

t Complete Specification for the invention entitled: CYCLONE SEPARATOR The following statement is a full description of this invention, including the best method of performing it known to us: -1- 901015,dbwdat.028,divl .1, ii ;11 I I i l 1A 1 "CYCLONE SEPARATOR" 2 3 This invention relates generally to cyclone separators 4 for separating multi-phase mixtures such as, for example, oil/water mixtures.

6 Applicant has invented several forms of cyclone 7 separators which are particularly suitable for use with 8 oil/water mixtures and which have varying constructions 9 depending upon the applications of the separators.

Generally, however, the cyclone separators comprise an 11 elongated separating chamber having a feed inlet proximate 12 to one end thereof and, in most cases, an overflow outlet at Seo 13 that end and an underflow outlet at the opposite end 14 thereof, the overflow outlet being for removing the less 15 dense phase and the underflow outlet for the more dense 16 phase.

S 17 In applicant's international applications o 18 PCT/AU85/00010 and PCT/AU85/00166, applicant discloses a 19 particularly advantageous form of feed inlet for use with oil/water mixtures.

21 Whilst the feed inlet as described in the 22 aforementioned specifications provides a significant 23 advantage over the prior art, optimum efficiency can vary 24 due to the make up of the mixture being supplied to the O4i. 25 separator. In some instances, the oil within the mixture f 26 may be in the form of small oil droplets whereas in other 27 instances, the mixture may contain relatively large 28 droplets.

.f 29 It is an object of the present invention to provide an improved cyclone separator which is adapted to operate at a 31 controlled maximum efficiency.

32 33 34 36 37 38 900201,kxispe.003.cyclone. 1 -2- 4 0*0 0 0*14 0 o 0 0 0o 0 0*0 00 4 00 0 0000 a* 00 r0 0004 0 0# err

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L(e Ie J In accordance with the present invention there is provided a cyclone separator for separating a denser liquid component from a less dense liquid component of a multi-phase liquid mixture wherein one liquid phase is in the form of drops dispersed in the other liquid phase, the cyclone separator comprising an elongated separating chamber having a longitudinal axis of symmetry between opposite first and second ends, the separator including at least one feed inlet adjacent the first end and at least one outlet, for admission of the mixture with a tangential flow component, the cyclone separator being characterised by the provision of control means which is adapted to vary the cross-sectional dimension of the at least one feed inlet; means for determining the concentration of one of the liquid phases in the mixture; and means responsive to said determining means for operating the control means.

The present invention also provides a cyclone separator for multi-phase liquid hydrocarbon and water mixtures to separate denser liquid components of the mixture from less dense liquid components thereof, with one liquid phase of the mixture being in the form of droplets dispersed in another liquid phase, and with 20 the distribution of such droplets in the mixture being determinative of the efficiency of the operation of the separator, the cyclone separator comprising: an axially extending separating chamber having an inlet means at one end for admission of the hydrocarbon and water mixture, such admission having a tangential flow component which when varied is operative to affect the efficiency of the separator in response to changes in the droplet distribution and concentration in the admitted mixture; an axially positioned overflow outlet adjacent said one end of said separating chamber, said separating chamber being open and unobstructed throughout its length and having a generally tapered or stepped configuration to form a relatively large cross-sectional size at said one end and a relatively small cross-sectional size at the other end; 901015,dbwpcD17,ivclaims.spc,2 i Ir-- .r-i II 2a underflow outlet means adjacent the other end of the separating chamber opposite said one end, wherein, in use, the denser liquid component of the mixture is directed to the underflow outlet in a fashion such as to encompass an inner axially positioned core of the less dense liquid component which is subjected at least over a substantial part of its length within the chamber to a pressure differential causing it to flow in an unobstructed axial path to said overflow outlet; the cyclone separator being characterized by the provision of control means arranged in the inlet means for varying the tangential flow component in response to changes in the droplet distribution and concentration within the mixture and thereby affect the separation efficiency of the separator by varying the crosssection area of the inlet in a manner that prevents shear forces from being applied to the admitted mixture; means for determining the concentration of droplets of one of the phases in the other; and means responsive to such determining means for operating said control means.

The present invention further provides a method for separating a denser liquid component from a less dense liquid component of a multi-phase liquid i 20 mixture in a cyclone separator, with one liquid phase being in the form of droplets disposed in another liquid phase, and with the distribution of such droplets in the mixture being determinative of the efficiency of the operation of the separator, Otto wherein the cy(cone separator is comprised of an axially extending separation I chamber having a feed inlet at one end for admission of the mixture into the separation chamber, control means for varying the cross-section area of the feed inlet, and an outlet adjacent the other end of the separating chamber, the method comprising the steps of: feeding the multi-phase mixture having liquid droplets into the feed inlet at the one end, determining the concentration of the one phase of liquid droplets in the other liquid phase, 901015,dbwspc.017,divdlim.spc,3 'U-l C4~-~r~rrrr~~(UcuariPI(1~C1' 2b operating the control means in response to the liquid droplet concentration determination to vary the cross-sectional area of the feed inlet and thereby maintain the operationali efficiency of the separator at a high level.

The present invention also provides a method for maintaining a high efficiency of operation of a hydrocyclone separator to separate a multi-phase liquid hydrocarbon and water mixture, with one liquid phase of the mixture being in the form of droplets dispersed in another liquid phase, and with the distribution of such droplets in the mixture being determinative of the efficiency of the operation of the separator, comprising the steps of: feeding a hydrocarbon and water mixture into the hydrocyclone separator through a variable feed inlet opening into an unobstructed and open separation chamber; imparting a tangential flow component to the mixture as it feeds from the inlet into the unobstructed separation chamber; and adjusting the cross-sectional area of the feed inlet in response to changes in o g the droplet distribution of one liquid phase in another liquid phase to maintain the efficiency of the separator.

The present invention further provides a cyclone separator for separating a s multi-phase liquid mixture into a less dense liquid component and a denser liquid component, one liquid phase of the mixture being dispersed in droplet form in the other liquid phase, said separator comprising an elongated separating chamber having a longitudinal axis of symmetry between opposite first and second ends, at i 25 least one feed inlet adjacent the first end, at least one outlet, and means for varying the cross-sectional dimension of said at least one inlet in response to determining flow parameters of said at least one inlet and/or said at least one outlet.

The present invention also provides a method of separating a multi-phase liquid mixture into a less dense liquid component and a denser liquid component, one liquid phase of the mixture being dispersed in droplet form in the other liquid 90015,dbwspcD17,dPvcaimS.spc,4 1 2c phase, said method comprising separating said mixture with a cyclone separator comprising an elongated separating chamber having a longitudinal axis of symmetry between opposite first and second ends, at least one feed inlet adjacent the first end, ant at least one outlet; and varying the cross-sectional dimension of said at least one inlet in response to determining flow parameters of said at least one inlet and/or said at least one outlet.

Preferred embodiments of the invention will hereinafter be described with reference to the accompanying drawings in which: Figure 1 is. a cross-sectional side elevation of one form of feed inlet according to the present invention; 09 a Figure 2 is a cross-sectional side elevation of another form of feed inlet according to the invention; 15 Figure 3 is a schematic sectional side elevation of a typical cyclone separator; Figure 4 is a detailed axial cross-sectional view of the feed inlet of a cyclone separator as described in PCT/AU85/00166; Figure 5 is a similar view to that of Figure 4 but showing preferred profiles; 20 and Figure 6 is a block diagram of a control syoem according to the invention.

P

Post" p t f. *1 90015dbwape.017,divlaimsc.spc sa, 0 0O o oo 0; 0 0000 00)0 0.0 0 0 0000 000~ 0 00 0O 0 00 0 0J 0 -3- Referring firstly to Figure 3, a type of cyclone separator generally indicated at 1 is shown and comprises a separating chamber 2 having at least one feed inlet 3 and an underflow outlet 4 and an overflow outlet 5. The cyclone separator shown is only of a general form but may for example take the specific form of that described in PCT/AU85/00166 or any other suitable configuration.

The separator functions generally in accordance with past practice in that the fluid mixture admitted into the separating chamber via the feed inlet 3 is subjected to centrifugal action causing the separated liquid components to 15 be ejected, on the one hand from the outlet and on the other through the outlet 5. Thus, the denser phase material flows to the underflow outlet 4 in an annular cross-sectioned flow around the wall of the separating chamber whilst the lighter phase forms a central core which is subjected to differential pressure action driving the fluid therein out the overflow outlet Referring now to Figure 4, an inlet profile of the type described in PCT/AU85/00166 is shown in more detail. Here, the feed inlet of the separator is shown as comprising an inlet tract 80 together with a portion of the separating chamber of the separator which is lengthwise adjacent thereto. In this regard, generally, although the separator shown in Figure 3 is described as having distinct portions of successively decreasing diameters, it is not essential that the separator be so formed I -4as it could, for example, exhibit any generally tapered configuration extending from a larger diameter end adjacent the overflow outlet to a smaller cross-section end adjacent the underflow outlet. The tract 80 is shown as having an outer profile 82 and an inner profile 84.

Here, the diameter D of the cyclone separator as shown in Figure 4 corresponds to the diameter dl in Figure 3, since the inlet tract 80 (as in the case of the Figure 3 construction) communicates with the separating chamber at the larger diameter end thereof.

tThe tract 80 is considered as extending o ofrom a location indicated generally by reference 15 numeral 85 inwardly towards the separating chamber. The location 85 is defined as a point S,r' beyond which, reckoned in the direction inwardly towards the separating chamber the flow of inlet liquid cannot be described by the simple 20 flow equations. More particularly, the points 83, 87 on the outer and inner profiles aligned i with location 85 are points where, if the profiles were projected outwardly therefrom in parallel 4> relationship the separator would operate substantially the same as if the profiles were continued in the profiled configurations described.

By the term "outwardly projected" is me:ant 1 a projection from the respective profile which is substantially tangential at the point of meeting the respective profile. From the respective points 83, 87 on the outer and inner profiles respectively the profiles extend in spiral fashion inwardly to meet the circumferential surface 86 of the separating chamber. Locations -lil~i: ux 5 1 at which the profiles so meet circumference 86 as designated 2 respectively by letters and Practically, although 3 the profile 84 is shown as joining circumference 86 by 4 continuance of the profile inwardly until it meets the 1| 5 circumference 86 at the point for mechanical reasons it 6 is frequently simpler and more effective to round the 7 junction between the profile 84 and the circumference 86 by 8 providing a rounded portion 84a (indicated by broken lines).

9 The inner and outer profiles are preferably generally 10 described by the following equations:- 11 1i 12 a P 2 a a 13 S o e 14 0.35 a 1.5, where a and q'are constants and D S 15 is the length of the outer profile 82 of the inlet tract, 16 viewed axially of the separating chamber, D being the S 17 diameter of the portion of the separating chamber at which 18 circumference 86 prevails. This profile length is that Cs I t 19 extending between points and 83. a D is the length of the inner profile 84, viewed axially of the separating 21 chamber. This profile length is that extending between 22 points and 87.

23 Generally, the outer profile 82 is such that vector T o S 24 describing the location of any particular point on the outer 25 profile and contained in a plane normal to said axis, and 26 having its origin at location is such that as the a 27 magnitude of the vector T increases, an angle 8 between the S, 28 vector T and a tangent 92 to circumference 86 passing 1 t 29 through said location never decreases substantially 31 32 33 34 36 37 38 900201,kxlspe.003. I -r -6and never becomes less than negative 0.1 radian for all magnitudes of T less than D n Similarly, a vector U, describing the location of any particular point on the inner profile 84 and having its point of origin at location is such that as the magnitude of vector U increases, the angle o- between vector U and a tangent 93 to said circumference which passes through said location never lj decreases and never becomes less than negative 0.52 radian, for all magnitudes of vector U less than a D, at least for substantial magnitudes of vector U. By substantial magnitude So of vector U, we mean that in the vicinity of a 15 the location vector U may not be defined because of possible rounding of the inner profile I 000 as previously described.

The cross-sectional area Ai of the tract measured in a radial and axial plane passing 20 through the location where the inner profile 84 actually terminates (location or the 00 extremity of the portion 84a as the case may be) is preferably defined as:- 0 0.02 <4 Ai/ 71D 2 0.1 It is also preferred that the following relationship holds between the constants n and a a n 2 7 a

I-I

mrYsanu -7- The described relationship between the constants a and n is most appropriate where, relatively speaking, the separator has a maximum diameter which is relatively more than the diameter of the underflow outlet. However where this ratio is relatively smaller, such as less than 3 it may be preferable to place greater restrictions on the relative values of the constants a and n The following may then be appropriate:- A. D/d 3 oo 0 oo a n 2 T a and S 0.35 a 2.

Here, d represents the underflow outlet diameter corresponding to diameter d 3 in Figure 3.

Referring now to Figure 5, in one construction o in accordance with the invention, the angle p measured about the axis of the separator between the points and was 860. The inner 20 profile 84 was terminated by a curved portion 84a co-joining with circumference 86, this portion had a curvature of approximately and located some 1100 around the axis of the separator from the point In this instance, it was found that the following mathematical relationship was appropriate for describing the profiles 82, 84: -8ro 0.5 D 0.0143 D ZO 1.4 0.0057 D Z O 1,8 0.00157 D Z 0 2 8 0.00286 D ZO r i 0.5 D 0.0714 D Z 2 0.00714 D Zi 3 0.0143 D Z i 4 0.00714 D Zj 0 94 o *9 *o 9 0'4"4 0090 0 9 0 90 0 0 9 Ia 4 ttr~A where r 0 is the distance from the axis cf the separator to any particular point on the outer profile 82, r i is the distance from the axis of the separator to any particular point on the inner profile 84, Z 0 is the angle, reckoned 10 from the line 91 joining the axis of the separator and the point in a clockwise direction around the axis of the separator to any point on the outer profile 82 and Z i is the angle, reckoned from the line 100 in a clockwise direction to any particular point on the inner profile 84. These equations describing the profiles 82, 84 generally may prevail for angles Z 0

Z

i in the range 00 Z 150° 00 Zi range 240 Z i 600 or at least in the 600.

The tract 80 may have a rectangular transverse cross-section such as having longer sides extending parallel to the axis of the separator and of length W and shorter sides contained in planes normal to the axis of the separator and of

I

-9length t. In this case the following relationships may prevail:t x W Ai, and t D/6.

Generally, W will be greater than t.

While forming the feed inlet of the separator with the described configurations permits only a single inlet to be employed, the described SA*" configurations may be advantageously employed 10 even where more than one inlet is provided.

O The term "involute" is used in this specification to describe a curve being the locus of the end of a piece of strin7 uncoiled from a base circle. The inner and outer profiles of the li or each inlet tract as described are generally formed as involute curves. Each profile may however, have cojoinig sections defined by S000 So 0 cojoining involute curves having respective o0* "oo S defining base circles of differing diameters, or, the projected start points on the respective base circles may be relatively circumferentially spaced.

Referring to Figures 1 and 2 of the drawings, the feed inlet 3 comprises an adjustable control :25 member 12 in the form of a pivotally mounted flap 13. The flap 13 has a contoured surface 14 which conforms to the inner profile as shown in Figures 4 and 5. The control member shown '1 I i ~s I in Figure 2 is the same as that shown in Figure 1 except that the leading edge thereof has been shortened.

The control member 12 is idapted to increase or reduce the cross-sectional dimension of feed inlet depending on the type of mixture being handled by the cyclone separator. Movement of the control member 12 may be effected manually or by a suitable form of drive means operatively connected thereto.

Where a drive means is used a control 0 system may be provided for sensing the condition of the incoming mixture the drive means being responsive to signals received from the control 15 system. By such an arrangement, the cyclone separator can separate at all times at substantially 0 maximum efficiency.

Referring to Figure b, the control system for cyclune separator 40 may comprise two purameters 41 and 42 for measuring the concentration of the mixture. These purameters are operatively connected Sto a mircoprocesser 43 which assesses the information provided from the purameters.

0 0° The microprocesser provides a signal tu ,oter 44 which 25 in turn controls the opening or closing of the flap.

In practice it is best to have the inlet opening open a selected distance depending on the drop size distribution in the mixture the size of the droplets having an effect on the efficiency of the operation of the separator.

Claims (9)

1. A cyclone separator for separating a denser liquid component from a less dense liquid component of a multi-phase liquid mixture wherein one liquid phase is in the form of drops dispersed in the other liquid phase, the cyclone separator comprising an elongated separating chamber having a longitudinal axis of symmetry between opposite first and second ends, the separator including at least one feed inlet adjacent the first end and at least one outlet, for admission of the mixture with a tangential flow component, the cyclone separator being characterised by the provision of control means which is adapted to vary the cross- sectional dimension of the at least one feed inlet; means for determining the concentration of one of the liquid phases in the oq* mixture; and e means responsive to said determining means for operating the control means. 0

2. The apparatus of claim 1 wherein said means for determining the concentration of the one phase further includes measurement means for determining the droplet distribution of one phase in the mixture at the feed inlet to the separator.

3. The apparatus of claim 1 wherein said means for determining the concentration in the mixture further includes means for determining the droplet distribution of one phase in the mixture at an outlet of the separator. 2

4. The apparatus of claim 1 wherein said determining means further includes means for measuring the concentration of the dispersed phase of the mixture within the other phase.

5. The apparatus of claim 4 and further including means for assessing the measurements of droplet distribution and concentration at said feed inlet and outlet, 901015,dbwape.0I7,divdaimi.sppeI I r-

12- and means responsive to said assessing means for operating said control means. 6. The cyclone separator of claim 1, and further including an inlet tract having upper and lower profiles intersecting with and terminating in a feed inlet near said one end of said separating chamber to form the tangential flow component of the admitted mixture. 7. The cyclone separator of claim 6 wherein 0.02 4A/tD 2 0.1 where A is the cross-sectional area of the inlet tract measured in the plane substantially perpendicular to the inlet tract at a point of termination of the lower profile of the inlet tract with the feed inlet in the one end of the separating chamber and D is the :oo 0 diameter of the separating chamber at said feed inlet. ce 0 P 8. A cyclone separator for multi-phase liquid hydrocarbon and water mixtures S oto separate denser liquid components of the mixture from less dense liquid components thereof, with one liquid phase of the mixture being in the form of droplets dispersed in another liquid phase, and with the distribution of such droplets in the mixture being determinative of the efficiency of the operation of the separator, the cyclone separator comprising: an axially extending separating chamber having an inlet means at one end o for admission of the hydrocarbon and water mixture, such admission having a tangential flow component which when varied is operative to affect the efficiency of the separator in response to changes in the droplet distribution and concentration in the admitted mixture; an axially positioned overflow outlet adjacent said one end of said separating chamber, said separating chamber being open and unobstructed throughout its length and having a generally tapered or stepped configuration to form a relatively large cross-sectional size at said one end and a relatively small cross-sectional size at the other end; underflow outlet means adjacent the other end of the separating chamber S901015,dbwspe.017,divcarns.spc,12 13 opposite said one end, wherein, in use, the denser liquid component of the mixture is directed to the underflow outlet in a fashion such as to encompass an inner axially positioned core of the less dense liquid component which is subjected at least over a substantial part of its length within the chamber to a pressure differential causing it to flow in an unobstructed axial path to said overflow outlet; the cyclone separator being characterized by the provision of control means arranged in the inlet means for varying the tangential flow component in response to changes in the droplet distribution and concentration within the mixture and thereby affect the separation efficiency of the separator by varying the cross- section area of the inlet in a manner that prevents shear forces flrom being applied to the admitted mixture; oo means for determining the concentration of droplets of one of the phases in the other; and means responsive to such determining means for operating said control means. a 9. The cyclone separator of claim 8 wherein said inlet means is comprised of an inlet tract having upper and lower profiles intersecting with and terminating in a feed inlet near said one end of said separating chamber to form the tangential flow component of the admitted mixture. o 10. The cyclone separator of claim 9 wherein 0.02 4A/JD 2 0.1 where A, is the cross-sectional area of the inlet tract measured in a plane substantially perpendicular to the inlet tract at a point of termination of the lower profile of the 25 inlet tract with the feed inlet in the one end of the separating chamber and D is the diameter of the separation chamber at the feed inlet. 11. A method for separating a denser liquid component from a less dense liquid component of a multi-phase liquid mixture in a cyclone separator, with one liquid phase being in the form of droplets disposed in another liquid phase, and with the distribution of such droplets in the mixture being determinative of the efficiency of 901015,dbwape.017,divaims.spe.13 14 the operation of the separator, wherein the cyclone separator is comprised of an axially extending separation chamber having a feed inlet at one end for admission of the mixture into the separation chamber, control means for varying the; cross- section area of the feed inlet, and an outlet adjacent the other end of the separating chamber, the method comprising the steps of: feeding the multi-phase mixture having liquid droplets into the feed inlet at the one end, determining the concentration of the one phase of liquid droplets in the other liquid phase, operating the control means in response to the liquid droplet concentration determination to vary the cross-sectional area of the feed inlet and thereby maintain the operational efficiency of the separator at a high level. I 12. The method of claim 11 wherein the mixture is comprised of at least two phases including a liquid hydrocarbon phase and a water phase, with one of such o**o phases being in the form of droplets in the other phase and further including determining the concentration of one phase in the other phase at the feed inlet to the separator. SJi t 20 13. The method of claim 11 and further including determining the concentration of droplets of one phase in the other phase, such determination being made at an 4* outlet at the other end of the separation chamber.

14. The method of claim 13 and further including also determining the concentration of one phase in another at an outlet of the separation chamber; assessing the determination of concentrations at the inlet and an outlet of the separation chamber, and operating the control means in response to the assessment of concentration at the inlet and an outlet of the separation chamber. A method for maintaining a high efficiency of operation of a hydrocyclone 901015,dbwspce.17,divclainspc,I4 I I ~I ca~m 15 separator to separate a multi-phase liquid hydrocarbon and water mixture, with one liquid phase of the mixture being in the form of droplets dispersed in another liquid phase, and with the distribution of such droplets in the mixture being determinative of the efficiency of the operation of the separator, comprising the steps of: feeding a hydrocarbon and water mixture into the hydrocyclone separator through a variable feed inlet opening into an unobstructed and open separation chamber; imparting a tangential flow component to the mixture as it feeds from the inlet into the unobstructed separation chamber; and adjusting the cross-sectional area of the feed inlet in response to changes in the droplet distribution of one liquid phase in another liquid phase to maintain the efficiency of the separator. 15 16. The method of claim 15 wherein the inlet has a cross-sectional area of A tand the separation chamber is circular and has a diameter at the feed inlet of D and further including maintaining the cross-sectional area of the feed inlet so that 0.02 4A/D 2 0.1. Sd.4 20 17. A cyclone separator for separating a multi-phase liquid mixture into a less dense liquid component and a denser liquid component, one liquid phase of the mixture being dispersed in droplet form in the other liquid phase, said separator comprising an elongated separating chamber having a longitudinal axis of symmetry between opposite first and second ends, at least one feed inlet adjacent the first end, at least one outlet, and means for varying the cross-sectional dimension of said at least one inlet in response to determining flow parameters of said at least one inlet and/or said at least one outlet.

18. A cyclone separator as claimed in claim 17, wherein the liquid phases are oil and water. 90101 Sdbwpc.017,divcI 16

19. A method of separating a multi-phase liquid mixture into a less dense liquid component and a denser liquid component, one liquid phase of the mixture being dispersed in droplet form in the other liquid phase, said method comprising separating said mixture with a cyclone separator comprising an elongated separating chamber having a longitudinal axis of symmetry between opposite first and second ends, at least one feed inlet adjacent the first end, and at least one outlet, and varying the cross-sectional dimension of said at least one inlet in response to determining flow parameters of said at least one inlet and/or said at least one outlet. A method of separating a liquid mixture as claimed in claim 2, wherein the liquid phases are oil and water. DATED this 15th day of October, 1990. CONOCO SPECIALTY PRODUCTS, INC. Sit By its Patent Attorneys S 20 DAVIES COLLISON A 4 a. a B l t i t 901015dbwpe,017,divlaims.sp,l 6