AU5093699A - Detergent tablet - Google Patents

Detergent tablet

Info

Publication number
AU5093699A
AU5093699A AU50936/99A AU5093699A AU5093699A AU 5093699 A AU5093699 A AU 5093699A AU 50936/99 A AU50936/99 A AU 50936/99A AU 5093699 A AU5093699 A AU 5093699A AU 5093699 A AU5093699 A AU 5093699A
Authority
AU
Australia
Prior art keywords
phase
detergent tablet
mould
tablet
enzyme
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU50936/99A
Inventor
Brenda Frances Bennie
Christopher James Binder
Valerio Del Duca
Andrea Esposito
Patrizio Ricci
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Procter and Gamble Co
Original Assignee
Procter and Gamble Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from GBGB9815525.2A external-priority patent/GB9815525D0/en
Application filed by Procter and Gamble Co filed Critical Procter and Gamble Co
Publication of AU5093699A publication Critical patent/AU5093699A/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047Detergents in the form of bars or tablets
    • C11D17/0065Solid detergents containing builders
    • C11D17/0073Tablets
    • C11D17/0086Laundry tablets
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/38Cationic compounds
    • C11D1/62Quaternary ammonium compounds
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D17/00Detergent materials or soaps characterised by their shape or physical properties
    • C11D17/0047Detergents in the form of bars or tablets
    • C11D17/0065Solid detergents containing builders
    • C11D17/0073Tablets
    • C11D17/0078Multilayered tablets
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246Silicates, e.g. diatomaceous earth
    • C11D3/1253Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/126Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite in solid compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/02Inorganic compounds ; Elemental compounds
    • C11D3/12Water-insoluble compounds
    • C11D3/124Silicon containing, e.g. silica, silex, quartz or glass beads
    • C11D3/1246Silicates, e.g. diatomaceous earth
    • C11D3/1253Layer silicates, e.g. talcum, kaolin, clay, bentonite, smectite, montmorillonite, hectorite or attapulgite
    • C11D3/1273Crystalline layered silicates of type NaMeSixO2x+1YH2O
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/22Carbohydrates or derivatives thereof
    • C11D3/222Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3703Macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3707Polyethers, e.g. polyalkyleneoxides
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3746Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3769(Co)polymerised monomers containing nitrogen, e.g. carbonamides, nitriles or amines
    • C11D3/3776Heterocyclic compounds, e.g. lactam
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3792Amine oxide containing polymers
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38609Protease or amylase in solid compositions only
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/38Products with no well-defined composition, e.g. natural products
    • C11D3/386Preparations containing enzymes, e.g. protease or amylase
    • C11D3/38645Preparations containing enzymes, e.g. protease or amylase containing cellulase
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/40Dyes ; Pigments
    • C11D3/42Brightening agents ; Blueing agents
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66Non-ionic compounds
    • C11D1/72Ethers of polyoxyalkylene glycols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Molecular Biology (AREA)
  • Emergency Medicine (AREA)
  • Detergent Compositions (AREA)
  • Control Of Motors That Do Not Use Commutators (AREA)
  • Polishing Bodies And Polishing Tools (AREA)
  • Sealing With Elastic Sealing Lips (AREA)

Abstract

A multi-phase detergent tablet comprising: a) a first phase in the form of a shaped body having at least one mould therein; and b) a second phase in the form of a compressed body adhesively contained within said mould, and wherein the second phase comprises an enzyme. The multi-phase tablets provide improved dissolution and cleaning characteristics together with excellent tablet integrity and strength.
AU50936/99A 1998-07-17 1999-07-09 Detergent tablet Abandoned AU5093699A (en)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
GBGB9815525.2A GB9815525D0 (en) 1998-07-17 1998-07-17 Detergent tablet
GB9815525 1998-07-17
GB9911218A GB2339791B (en) 1998-07-17 1999-05-17 Detergent tablet
GB9911218 1999-05-17
PCT/US1999/015492 WO2000004129A2 (en) 1998-07-17 1999-07-09 Detergent tablet

Publications (1)

Publication Number Publication Date
AU5093699A true AU5093699A (en) 2000-02-07

Family

ID=26314050

Family Applications (2)

Application Number Title Priority Date Filing Date
AU49643/99A Ceased AU761595B2 (en) 1998-07-17 1999-07-09 Detergent tablet
AU50936/99A Abandoned AU5093699A (en) 1998-07-17 1999-07-09 Detergent tablet

Family Applications Before (1)

Application Number Title Priority Date Filing Date
AU49643/99A Ceased AU761595B2 (en) 1998-07-17 1999-07-09 Detergent tablet

Country Status (22)

Country Link
EP (3) EP0976819B1 (en)
JP (2) JP2002520482A (en)
CN (1) CN1309694A (en)
AT (3) ATE212660T1 (en)
AU (2) AU761595B2 (en)
BR (1) BR9912833A (en)
CA (2) CA2337402C (en)
DE (3) DE69900833T2 (en)
DK (2) DK0976819T3 (en)
ES (3) ES2208477T3 (en)
FI (1) FI4407U1 (en)
FR (1) FR2782092B1 (en)
IE (1) IES990570A2 (en)
IT (2) ITMI991510A1 (en)
MA (1) MA24934A1 (en)
NL (1) NL1012584C1 (en)
PL (1) PL189559B1 (en)
PT (2) PT976819E (en)
RU (1) RU2203933C2 (en)
SK (1) SK612001A3 (en)
TR (1) TR200100093T2 (en)
WO (2) WO2000004128A2 (en)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IES990573A2 (en) * 1998-07-17 2000-03-08 Procter & Gamble Detergent tablet
DK0979864T3 (en) * 1998-07-17 2002-04-22 Procter & Gamble Process for the preparation of detergent tablets
ATE212660T1 (en) * 1998-07-17 2002-02-15 Procter & Gamble DETERGENT TABLET
DE29911484U1 (en) * 1998-07-17 2000-02-24 Procter & Gamble Detergent tablet
ATE325183T1 (en) 1999-03-09 2006-06-15 Procter & Gamble METHOD FOR PRODUCING COATED SURFACTANT PARTICLES
GB9911949D0 (en) 1999-05-21 1999-07-21 Unilever Plc Detergent compositions
DE19937428A1 (en) * 1999-08-07 2001-02-08 Henkel Kgaa Detergent tablets
EP1090981A1 (en) * 1999-10-07 2001-04-11 The Procter & Gamble Company Fabric rejuvenating treatment
EP1090980A1 (en) * 1999-10-07 2001-04-11 The Procter & Gamble Company Fabric rejuvenating treatment
GB0015350D0 (en) * 2000-06-23 2000-08-16 Reckitt Benckiser Nv Improvements in or relating to compositions
DE10053416A1 (en) 2000-10-27 2002-05-08 Bsh Bosch Siemens Hausgeraete Process for the mechanical cleaning of textiles or solid objects
EP1201741A1 (en) 2000-10-31 2002-05-02 The Procter & Gamble Company Detergent compositions
EP1405900B1 (en) * 2002-10-01 2006-03-08 Unilever Plc Detergent compositions
US7820198B2 (en) 2004-10-19 2010-10-26 Arch Chemicals, Inc. Pool chemical tablet
EP1676904B1 (en) 2005-01-04 2009-05-06 Unilever N.V. Detergent tablets
EP1705240A1 (en) 2005-03-23 2006-09-27 Unilever N.V. Detergent tablets
ES2313539T3 (en) 2005-03-23 2009-03-01 Unilever N.V. DETERGENT COMPOSITIONS IN THE FORM OF PILLS.
EP1746151A1 (en) 2005-07-20 2007-01-24 Unilever N.V. Detergent tablet compositions
EP1746152A1 (en) 2005-07-20 2007-01-24 Unilever N.V. Detergent compositions
EP1903099A1 (en) * 2006-09-22 2008-03-26 Dalli-Werke GmbH & Co. KG Coated detergent compositions and manufacture process
US7781387B2 (en) * 2008-01-22 2010-08-24 Access Business Group International, Llc. Automatic phosphate-free dishwashing detergent providing improved spotting and filming performance
GB0913808D0 (en) 2009-08-07 2009-09-16 Mcbride Robert Ltd Dosage form detergent products
EP3034596B2 (en) * 2014-12-17 2021-11-10 The Procter & Gamble Company Detergent composition
EP3034597A1 (en) 2014-12-17 2016-06-22 The Procter and Gamble Company Detergent composition
EP3034588B1 (en) * 2014-12-17 2019-04-24 The Procter and Gamble Company Detergent composition
KR20180136542A (en) * 2016-04-27 2018-12-24 바스프 에스이 Formulations, their manufacture and use, and suitable ingredients
US11021680B2 (en) 2016-09-07 2021-06-01 Ecolab Usa Inc. Detergent compositions containing a stabilized enzyme by phosphonates
CN110373287B (en) * 2019-08-15 2021-11-09 广州立白企业集团有限公司 Automatic dish-washing machine cleaning sheet with multiphase structure
GB202115335D0 (en) * 2021-10-25 2021-12-08 Econic Tech Ltd Surface-active agent

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GB911204A (en) * 1960-07-28 1962-11-21 Unilever Ltd Bleaching compositions
GB1307387A (en) * 1969-02-18 1973-02-21 Lion Fat Oil Co Ltd Cleansing agent having a shell structure
ZA752732B (en) * 1974-05-15 1976-12-29 Colgate Palmolive Co Unitary detergent compositions and washing methods
US3962107A (en) * 1974-06-24 1976-06-08 Johnson & Johnson Enzyme-containing denture cleanser tablet
JPS5476836A (en) * 1977-12-02 1979-06-19 Kukidento Kuruto Kurisupu Kg Tablet for cleaning false tooth and production thereof
US4460490A (en) * 1980-12-18 1984-07-17 Jeyes Group Limited Lavatory cleansing blocks
ATE45495T1 (en) * 1984-02-08 1989-09-15 Richardson Gmbh ANTI-PLATURE TABLET FOR CLEANING DENTAL PROSTHESES.
DE3541146A1 (en) * 1985-11-21 1987-05-27 Henkel Kgaa MULTILAYERED DETERGENT TABLETS FOR MACHINE DISHWASHER
GB9015503D0 (en) * 1990-07-13 1990-08-29 Unilever Plc Detergent composition
JP2898375B2 (en) * 1990-08-20 1999-05-31 ポーラ化成工業株式会社 Composite solid and method for producing the same
US5133892A (en) * 1990-10-17 1992-07-28 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing detergent tablets
GB9022724D0 (en) * 1990-10-19 1990-12-05 Unilever Plc Detergent compositions
JPH07109499A (en) * 1993-10-08 1995-04-25 Osaka Seiyaku:Kk Foaming detergent
ES2155613T3 (en) * 1995-07-13 2001-05-16 Reckitt Benckiser Nv PRODUCT IN THE FORM OF A DISHWASHER TABLET.
US5900395A (en) * 1996-12-23 1999-05-04 Lever Brothers Company Machine dishwashing tablets containing an oxygen bleach system
US5837663A (en) * 1996-12-23 1998-11-17 Lever Brothers Company, Division Of Conopco, Inc. Machine dishwashing tablets containing a peracid
GB2327949A (en) * 1997-08-02 1999-02-10 Procter & Gamble Detergent tablet
JP2001522933A (en) * 1997-11-10 2001-11-20 ザ、プロクター、エンド、ギャンブル、カンパニー Detergent tablet
US6413928B1 (en) * 1997-11-10 2002-07-02 The Procter & Gamble Company Process for preparing a detergent tablet
ATE241003T1 (en) * 1997-11-10 2003-06-15 Procter & Gamble MULTI-LAYER DETERGENT TABLET WITH BOTH COMPRESSED AND NON-COMPRESSED PARTS
BR9814905A (en) * 1997-11-26 2001-10-23 Procter & Gamble Detergent tablet
ATE317002T1 (en) * 1997-11-26 2006-02-15 Procter & Gamble DETERGENT TABLET
DE69830334T2 (en) * 1997-11-26 2006-02-02 The Procter & Gamble Company, Cincinnati DETERGENT TABLET
JP2001524595A (en) * 1997-11-26 2001-12-04 ザ、プロクター、エンド、ギャンブル、カンパニー Detergent tablet
DE29911484U1 (en) * 1998-07-17 2000-02-24 Procter & Gamble Detergent tablet
DK0979864T3 (en) * 1998-07-17 2002-04-22 Procter & Gamble Process for the preparation of detergent tablets
EP1144567B1 (en) * 1998-07-17 2004-09-22 The Procter & Gamble Company Detergent tablet
ATE212660T1 (en) * 1998-07-17 2002-02-15 Procter & Gamble DETERGENT TABLET
IES990573A2 (en) * 1998-07-17 2000-03-08 Procter & Gamble Detergent tablet
TR200100092T2 (en) * 1998-07-17 2001-10-22 The Procter & Gamble Company Detergent tablet

Also Published As

Publication number Publication date
CA2333894A1 (en) 2000-01-27
JP2002520481A (en) 2002-07-09
PT1144584E (en) 2006-10-31
CA2337402A1 (en) 2000-01-27
EP0976819A1 (en) 2000-02-02
FIU990321U0 (en) 1999-07-16
WO2000004128A3 (en) 2000-03-30
BR9912833A (en) 2001-10-09
DE69931812D1 (en) 2006-07-20
AU4964399A (en) 2000-02-07
DK1144584T3 (en) 2006-10-09
CA2333894C (en) 2004-02-03
IES990570A2 (en) 2000-03-08
EP1098955A2 (en) 2001-05-16
WO2000004129A3 (en) 2001-08-23
WO2000004128A2 (en) 2000-01-27
ITMI991570A1 (en) 2001-01-15
ATE250661T1 (en) 2003-10-15
WO2000004129A2 (en) 2000-01-27
DK0976819T3 (en) 2002-05-13
ES2172290T3 (en) 2002-09-16
CN1309694A (en) 2001-08-22
PL189559B1 (en) 2005-08-31
EP0976819B1 (en) 2002-01-30
ES2208477T3 (en) 2004-06-16
DE69911623T2 (en) 2004-07-01
NL1012584C1 (en) 2000-01-25
FI4407U1 (en) 2000-05-18
AU761595B2 (en) 2003-06-05
PT976819E (en) 2002-06-28
ES2267278T3 (en) 2007-03-01
SK612001A3 (en) 2001-07-10
NL1012584A1 (en) 2000-01-19
CA2337402C (en) 2004-05-04
ATE329001T1 (en) 2006-06-15
PL345973A1 (en) 2002-01-14
ITMI991510A1 (en) 1999-12-18
ITMI991570A0 (en) 1999-07-15
FR2782092A1 (en) 2000-02-11
MA24934A1 (en) 2000-04-01
DE69900833D1 (en) 2002-03-14
ATE212660T1 (en) 2002-02-15
DE69911623D1 (en) 2003-10-30
EP1144584B1 (en) 2006-06-07
ITMI991510A0 (en) 1999-07-09
TR200100093T2 (en) 2002-09-23
FR2782092B1 (en) 2004-11-05
EP1144584A2 (en) 2001-10-17
DE69931812T2 (en) 2007-05-31
DE69900833T2 (en) 2002-10-31
JP2002520482A (en) 2002-07-09
RU2203933C2 (en) 2003-05-10
EP1144584A3 (en) 2002-09-11

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Legal Events

Date Code Title Description
MK6 Application lapsed section 142(2)(f)/reg. 8.3(3) - pct applic. not entering national phase