AU2001264408A1 - Process for the production of cyclohexanone oxime - Google Patents

Process for the production of cyclohexanone oxime

Info

Publication number
AU2001264408A1
AU2001264408A1 AU2001264408A AU6440801A AU2001264408A1 AU 2001264408 A1 AU2001264408 A1 AU 2001264408A1 AU 2001264408 A AU2001264408 A AU 2001264408A AU 6440801 A AU6440801 A AU 6440801A AU 2001264408 A1 AU2001264408 A1 AU 2001264408A1
Authority
AU
Australia
Prior art keywords
cyclohexanone oxime
synthesis zone
hydroxylammonium
production
cyclohexanone
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Abandoned
Application number
AU2001264408A
Inventor
Marc Blaauw
Henk Oevering
Alex Pit
Theodorus Friederich Maria Riesthuis
Antonius Jacobus Franciscus Simons
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Koninklijke DSM NV
Original Assignee
DSM NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by DSM NV filed Critical DSM NV
Publication of AU2001264408A1 publication Critical patent/AU2001264408A1/en
Abandoned legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00Nitrogen; Compounds thereof
    • C01B21/082Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14Hydroxylamine; Salts thereof
    • C01B21/1409Preparation
    • C01B21/1418Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00Systems containing only non-condensed rings
    • C07C2601/12Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Process for the production of cyclohexanone oxime in which a phosphate-containing aqueous reaction medium is cycled from a hydroxylammonium synthesis zone to a cyclohexanone oxime synthesis zone and back to the hydroxylammonium synthesis zone, in which hydroxylammonium synthesis zone hydroxylammonium is fomed by catalytic reduction of nitrate with hydrogen, and in which cyclohexanone oxime synthesis zone hydroxylammonium is reacted with cyclohexanone to form cyclohexanone oxime, wherein the phosphate concentration in the acqueous reaction medium entering the cyclohexanone oxime synthesis zone is higher than 3.0 mol/l.
AU2001264408A 2000-06-05 2001-05-31 Process for the production of cyclohexanone oxime Abandoned AU2001264408A1 (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP00201970 2000-06-05
EP00201970 2000-06-05
PCT/NL2001/000428 WO2001094297A1 (en) 2000-06-05 2001-05-31 Process for the production of cyclohexanone oxime

Publications (1)

Publication Number Publication Date
AU2001264408A1 true AU2001264408A1 (en) 2001-12-17

Family

ID=8171597

Family Applications (1)

Application Number Title Priority Date Filing Date
AU2001264408A Abandoned AU2001264408A1 (en) 2000-06-05 2001-05-31 Process for the production of cyclohexanone oxime

Country Status (13)

Country Link
US (1) US6759556B2 (en)
EP (1) EP1301468B1 (en)
JP (1) JP4856839B2 (en)
KR (1) KR100794087B1 (en)
CN (1) CN1200928C (en)
AT (1) ATE272612T1 (en)
AU (1) AU2001264408A1 (en)
BR (1) BR0111439B1 (en)
DE (1) DE60104699T2 (en)
MX (1) MXPA02011962A (en)
MY (1) MY124874A (en)
TW (1) TWI265920B (en)
WO (1) WO2001094297A1 (en)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP1318141A1 (en) * 2001-12-04 2003-06-11 Dsm Nv Process for treating an aqueous medium containing phosphate, cyclohexanone and cyclohexanone oxime
EP1451149B1 (en) 2001-12-04 2007-02-14 DSM IP Assets B.V. Process for treating an aqueous medium containing cyclohexanone oxime and cyclohexanone
US7423178B2 (en) * 2003-01-30 2008-09-09 Dsm Ip Assets B.V. Process for treating an organic solution comprising cyclohexanone oxime, cyclohexanone, and an organic solvent
BRPI0410604A (en) * 2003-05-23 2006-06-20 Dsm Ip Assets Bv process for preparing caprolactam
TW200829542A (en) * 2007-01-05 2008-07-16 China Petrochemical Dev Corp Hydroxylamine -oximination cycling system
CN103492312B (en) 2011-04-22 2016-11-02 Capiii有限公司 The method preparing azanol
CN104892452A (en) * 2014-03-04 2015-09-09 江苏艾科维科技有限公司 Preparation method for ketoxime

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL141502B (en) * 1969-09-20 1974-03-15 Stamicarbon CONTINUOUS PREPARATION OF CYCLOHEXANONOXIME.
BE759915A (en) * 1969-12-06 1971-06-04 Stamicarbon RECYCLING PROCESS FOR THE PREPARATION AND TREATMENT OF A HYDROXYLAMMONIUM SALT SOLUTION
BE759914A (en) * 1969-12-06 1971-06-04 Stamicarbon RECYCLING PROCESS FOR THE PREPARATION AND TREATMENT OF A HYDROXYLAMMONIUM SALT SOLUTION
NL7001906A (en) * 1970-02-11 1971-08-13
NL7004350A (en) * 1970-03-26 1971-09-28 Stamicarbon
NL7405630A (en) * 1974-04-26 1975-10-28 Stamicarbon CIRCUIT PROCESS FOR THE PREPARATION OF CYCLOHEXANONOXIME.

Also Published As

Publication number Publication date
WO2001094297A1 (en) 2001-12-13
KR100794087B1 (en) 2008-01-10
JP2004501122A (en) 2004-01-15
MXPA02011962A (en) 2003-07-14
KR20030007871A (en) 2003-01-23
DE60104699T2 (en) 2005-08-18
CN1200928C (en) 2005-05-11
CN1446194A (en) 2003-10-01
ATE272612T1 (en) 2004-08-15
BR0111439A (en) 2003-06-03
EP1301468A1 (en) 2003-04-16
DE60104699D1 (en) 2004-09-09
MY124874A (en) 2006-07-31
US20040039231A1 (en) 2004-02-26
US6759556B2 (en) 2004-07-06
TWI265920B (en) 2006-11-11
BR0111439B1 (en) 2011-08-09
JP4856839B2 (en) 2012-01-18
EP1301468B1 (en) 2004-08-04

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