ATE378109T1 - Verfahren zur hydroformylierung von ethylenisch ungesättigten verbindungen mittels einer zweizähnigen diphosphin-zusammensetzung mit einer verbrückenden gruppe enthaltend sp2-hybridisierte und an die phosphoratome gebundene kohlenstoffatome - Google Patents
Verfahren zur hydroformylierung von ethylenisch ungesättigten verbindungen mittels einer zweizähnigen diphosphin-zusammensetzung mit einer verbrückenden gruppe enthaltend sp2-hybridisierte und an die phosphoratome gebundene kohlenstoffatomeInfo
- Publication number
- ATE378109T1 ATE378109T1 AT03798198T AT03798198T ATE378109T1 AT E378109 T1 ATE378109 T1 AT E378109T1 AT 03798198 T AT03798198 T AT 03798198T AT 03798198 T AT03798198 T AT 03798198T AT E378109 T1 ATE378109 T1 AT E378109T1
- Authority
- AT
- Austria
- Prior art keywords
- sup
- hydroformylation
- line
- bridging group
- formulae
- Prior art date
Links
- VURFVHCLMJOLKN-UHFFFAOYSA-N diphosphane Chemical compound PP VURFVHCLMJOLKN-UHFFFAOYSA-N 0.000 title abstract 4
- 150000001875 compounds Chemical class 0.000 title abstract 2
- 238000007037 hydroformylation reaction Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title 1
- 125000004437 phosphorous atom Chemical group 0.000 abstract 2
- 229910052698 phosphorus Inorganic materials 0.000 abstract 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 abstract 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052799 carbon Inorganic materials 0.000 abstract 1
- 125000004432 carbon atom Chemical group C* 0.000 abstract 1
- 229910002091 carbon monoxide Inorganic materials 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000001768 cations Chemical class 0.000 abstract 1
- 238000006243 chemical reaction Methods 0.000 abstract 1
- -1 halide anions Chemical class 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 239000003446 ligand Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 125000006413 ring segment Chemical group 0.000 abstract 1
- 125000005750 substituted cyclic group Chemical group 0.000 abstract 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
- B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
- B01J31/2419—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member
- B01J31/2428—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member with more than one complexing phosphine-P atom
- B01J31/2433—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising P as ring member with more than one complexing phosphine-P atom comprising aliphatic or saturated rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
- B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
- B01J31/2442—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems
- B01J31/2461—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems and phosphine-P atoms as ring members in the condensed ring system or in a further ring
- B01J31/2471—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems and phosphine-P atoms as ring members in the condensed ring system or in a further ring with more than one complexing phosphine-P atom
- B01J31/2476—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems and phosphine-P atoms as ring members in the condensed ring system or in a further ring with more than one complexing phosphine-P atom comprising aliphatic or saturated rings
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/16—Catalysts comprising hydrides, coordination complexes or organic compounds containing coordination complexes
- B01J31/24—Phosphines, i.e. phosphorus bonded to only carbon atoms, or to both carbon and hydrogen atoms, including e.g. sp2-hybridised phosphorus compounds such as phosphabenzene, phosphole or anionic phospholide ligands
- B01J31/2404—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring
- B01J31/2442—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems
- B01J31/2461—Cyclic ligands, including e.g. non-condensed polycyclic ligands, the phosphine-P atom being a ring member or a substituent on the ring comprising condensed ring systems and phosphine-P atoms as ring members in the condensed ring system or in a further ring
- B01J31/248—Bridged ring systems, e.g. 9-phosphabicyclononane
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/49—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide
- C07C45/50—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reaction with carbon monoxide by oxo-reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/30—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group
- C07C67/333—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton
- C07C67/343—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
- C07C67/347—Preparation of carboxylic acid esters by modifying the acid moiety of the ester, such modification not being an introduction of an ester group by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by addition to unsaturated carbon-to-carbon bonds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/547—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom
- C07F9/6564—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms
- C07F9/6568—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus atoms as the only ring hetero atoms
- C07F9/65683—Heterocyclic compounds, e.g. containing phosphorus as a ring hetero atom having phosphorus atoms, with or without nitrogen, oxygen, sulfur, selenium or tellurium atoms, as ring hetero atoms having phosphorus atoms as the only ring hetero atoms the ring phosphorus atom being part of a phosphine
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
- B01J2231/30—Addition reactions at carbon centres, i.e. to either C-C or C-X multiple bonds
- B01J2231/32—Addition reactions to C=C or C-C triple bonds
- B01J2231/321—Hydroformylation, metalformylation, carbonylation or hydroaminomethylation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
- B01J2531/80—Complexes comprising metals of Group VIII as the central metal
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
- B01J2531/80—Complexes comprising metals of Group VIII as the central metal
- B01J2531/82—Metals of the platinum group
- B01J2531/824—Palladium
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/26—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24
- B01J31/28—Catalysts comprising hydrides, coordination complexes or organic compounds containing in addition, inorganic metal compounds not provided for in groups B01J31/02 - B01J31/24 of the platinum group metals, iron group metals or copper
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
- Catalysts (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP02256696 | 2002-09-26 |
Publications (1)
Publication Number | Publication Date |
---|---|
ATE378109T1 true ATE378109T1 (de) | 2007-11-15 |
Family
ID=32039202
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
AT03798198T ATE378109T1 (de) | 2002-09-26 | 2003-09-24 | Verfahren zur hydroformylierung von ethylenisch ungesättigten verbindungen mittels einer zweizähnigen diphosphin-zusammensetzung mit einer verbrückenden gruppe enthaltend sp2-hybridisierte und an die phosphoratome gebundene kohlenstoffatome |
Country Status (10)
Country | Link |
---|---|
US (2) | US7250538B2 (de) |
EP (1) | EP1542798B1 (de) |
JP (1) | JP4101803B2 (de) |
CN (1) | CN100363319C (de) |
AT (1) | ATE378109T1 (de) |
AU (1) | AU2003299066A1 (de) |
CA (1) | CA2500095C (de) |
DE (1) | DE60317533T2 (de) |
WO (1) | WO2004028689A2 (de) |
ZA (1) | ZA200502080B (de) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB0403592D0 (en) | 2004-02-18 | 2004-03-24 | Lucite Int Uk Ltd | A catalyst system |
GB0516556D0 (en) | 2005-08-12 | 2005-09-21 | Lucite Int Uk Ltd | Improved catalyst system |
AU2006314268C1 (en) | 2005-11-17 | 2014-01-09 | Lucite International Uk Limited | Carbonylation of ethylenically unsaturated compounds |
WO2007067257A2 (en) | 2005-12-02 | 2007-06-14 | Vanderbilt University | Broad-emission nanocrystals and methods of making and using same |
GB0607494D0 (en) | 2006-04-13 | 2006-05-24 | Lucite Int Uk Ltd | Metal complexes |
JP2010511600A (ja) | 2006-12-02 | 2010-04-15 | ルーサイト インターナショナル ユーケー リミテッド | 新規のカルボニル化配位子及びエチレン性不飽和化合物のカルボニル化におけるその使用 |
GB2451325A (en) * | 2007-07-24 | 2009-01-28 | Shell Int Research | Hydroformylation process |
GB0812297D0 (en) | 2008-07-04 | 2008-08-13 | Lucite Int Uk Ltd | Novel carbonylation ligand sand thier use of in the carbonylation of ethylenically unsaturated compounds |
US20100069679A1 (en) * | 2008-09-12 | 2010-03-18 | Eastman Chemical Company | Acetylene tolerant hydroformylation catalysts |
GB201000078D0 (en) | 2010-01-05 | 2010-02-17 | Lucite Int Uk Ltd | Process for the carbonylation of ethylenically unsaturated compounds, novel carbonylation ligands and catalyst systems incorporatng such ligands |
CN104425248B (zh) * | 2013-08-28 | 2017-10-27 | 无锡华润上华科技有限公司 | 重掺杂p型衬底背封工艺方法 |
JP2015137232A (ja) * | 2014-01-20 | 2015-07-30 | Jx日鉱日石エネルギー株式会社 | ノルボルナン−2−スピロ−α−シクロアルカノン−α’−スピロ−2’’−ノルボルナン−5,5’’,6,6’’−テトラカルボン酸及びそのエステル類の製造方法 |
JP2015137230A (ja) * | 2014-01-20 | 2015-07-30 | Jx日鉱日石エネルギー株式会社 | ノルボルナン−2−スピロ−α−シクロアルカノン−α’−スピロ−2’’−ノルボルナン−5,5’’,6,6’’−テトラカルボン酸及びそのエステル類の製造方法 |
Family Cites Families (32)
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US2042011A (en) | 1934-12-06 | 1936-05-26 | Gulf Res & Dev Corp | Producing flocculation in oil well strata |
FR2671132B1 (fr) | 1990-12-28 | 1997-06-13 | Inst Francais Du Petrole | Suspension de particules solides pour reduire les disparites de permeabilites d'une formation geologique heterogene, application a la recuperation d'hydrocarbures et procede d'injection. |
DE69210054T2 (de) | 1991-01-15 | 1996-12-12 | Shell Int Research | Carbonylierung von Olefinen |
DE69200122T2 (de) * | 1991-02-15 | 1994-09-29 | Shell Int Research | Katalytisches System für die Carbonylierung. |
GB9111583D0 (en) | 1991-05-30 | 1991-07-24 | Shell Int Research | Carbonylation catalyst system |
ES2123823T3 (es) | 1993-08-19 | 1999-01-16 | Shell Int Research | Procedimiento de hidroformilacion. |
BE1008343A3 (nl) | 1994-05-06 | 1996-04-02 | Dsm Nv | Bidentaat fosfineligand |
GB2306344A (en) * | 1995-10-25 | 1997-05-07 | Shell Int Research | Catalysed hydroformylation |
WO1997018894A1 (fr) * | 1995-11-22 | 1997-05-29 | Firmenich S.A. | Catalyseurs de ruthenium et leur utilisation dans l'hydrogenation asymetrique de cyclopentenones |
US5780684A (en) * | 1996-01-16 | 1998-07-14 | Shell Oil Company | Hydroformylation reactions |
US6103927A (en) * | 1996-04-16 | 2000-08-15 | Shell Oil Company | Process for the carbonylation of ethylenically unsaturated compounds |
JP2002513376A (ja) | 1996-06-14 | 2002-05-08 | ザ ペン ステイト リサーチ ファウンデイション | 環式キラルホスフィン配位子を有する遷移金属錯体を触媒とする不斉合成 |
DE19652350A1 (de) | 1996-12-17 | 1998-06-18 | Studiengesellschaft Kohle Mbh | Neue Katalysatoren aus Übergangsmetallverbindungen und 4,5-Diphosphinoacridin-Liganden |
US6214763B1 (en) * | 1997-05-20 | 2001-04-10 | Firmenich Sa | Ruthenium catalysts and their use in the asymmetric hydrogenation of weakly coordinating substrates |
US6127582A (en) * | 1997-08-27 | 2000-10-03 | Shell Oil Company | Hydroformylation process |
EP0903333B1 (de) * | 1997-09-18 | 2001-11-07 | Shell Internationale Researchmaatschappij B.V. | Hydroformylierungsverfahren |
EP0922691B1 (de) * | 1997-12-03 | 2004-04-28 | Shell Internationale Research Maatschappij B.V. | Hydroformylierungsverfahren |
US6156936A (en) * | 1998-03-16 | 2000-12-05 | Shell Oil Company | Hydroformylation of olefin feeds containing dienes |
JP3730428B2 (ja) * | 1998-12-22 | 2006-01-05 | 富士通株式会社 | 半導体装置試験用コンタクタの製造方法 |
WO2001014299A1 (en) * | 1999-08-23 | 2001-03-01 | The Penn State Research Foundation | Chiral ligands, transition-metal complexes thereof and uses thereof in asymmetric reactions |
MY127093A (en) * | 2000-05-17 | 2006-11-30 | Lucite Int Uk Ltd | Bidentate ligands useful in catalyst systems |
JP4874501B2 (ja) * | 2000-08-14 | 2012-02-15 | サソール テクノロジー(プロプライエタリー)リミテッド | 含酸素製品の製造 |
MY127097A (en) * | 2000-09-27 | 2006-11-30 | Dsm Ip Assets Bv | Process for the carbonylation of a conjugated diene |
GB0026890D0 (en) | 2000-11-03 | 2000-12-20 | Ici Plc | Catalyst |
JP2004517901A (ja) * | 2001-01-19 | 2004-06-17 | カイロテック・テクノロジー・リミテッド | 配位子およびその使用 |
WO2002064250A2 (en) * | 2001-01-31 | 2002-08-22 | Shell Internationale Research Maatschappij B.V. | Process for the carbonylation of ethylenically unsaturated compounds, bidentate diphosphine composition used in this process and processes for preparation of this bidentate diphosphine composition |
DE10106348A1 (de) | 2001-02-09 | 2002-08-14 | Basf Ag | Als Katalysator oder zur Herstellung eines Katalysatorsystems geeignete Verbindung |
CN1308337C (zh) * | 2001-11-09 | 2007-04-04 | 国际壳牌研究有限公司 | 用于不饱和化合物羰基化的双齿配位体 |
US6743921B2 (en) * | 2002-01-24 | 2004-06-01 | Dsm Catalytica Pharmaceuticals, Inc. | Process for the preparation of nonracemic syn-1-(4-hydroxy-phenyl)-2-(4-hydroxy-4-phenyl-piperidin-1-yl)-1-propanol compounds |
US6806391B2 (en) * | 2002-07-31 | 2004-10-19 | Shell Oil Company | Process for the carbonylation of ethylenically unsaturated compounds and bidentate diphosphine composition used in this process |
CN1684931A (zh) * | 2002-09-26 | 2005-10-19 | 国际壳牌研究有限公司 | 伯醇的制备方法 |
US7265242B2 (en) * | 2004-02-26 | 2007-09-04 | Shell Oil Company | Process for the carbonylation of ethylenically or acetylenically unsaturated compounds |
-
2003
- 2003-09-24 JP JP2004539074A patent/JP4101803B2/ja not_active Expired - Fee Related
- 2003-09-24 CA CA2500095A patent/CA2500095C/en not_active Expired - Fee Related
- 2003-09-24 CN CNB038230062A patent/CN100363319C/zh not_active Expired - Fee Related
- 2003-09-24 AT AT03798198T patent/ATE378109T1/de not_active IP Right Cessation
- 2003-09-24 WO PCT/EP2003/050654 patent/WO2004028689A2/en active IP Right Grant
- 2003-09-24 EP EP03798198A patent/EP1542798B1/de not_active Expired - Lifetime
- 2003-09-24 AU AU2003299066A patent/AU2003299066A1/en not_active Abandoned
- 2003-09-24 US US10/670,105 patent/US7250538B2/en not_active Expired - Fee Related
- 2003-09-24 DE DE60317533T patent/DE60317533T2/de not_active Expired - Lifetime
-
2005
- 2005-03-11 ZA ZA2005/02080A patent/ZA200502080B/en unknown
-
2007
- 2007-06-07 US US11/759,623 patent/US7414155B2/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
AU2003299066A1 (en) | 2004-04-19 |
CA2500095C (en) | 2011-10-18 |
CA2500095A1 (en) | 2004-04-08 |
DE60317533T2 (de) | 2008-09-18 |
US20040167362A1 (en) | 2004-08-26 |
US7414155B2 (en) | 2008-08-19 |
CN100363319C (zh) | 2008-01-23 |
WO2004028689A3 (en) | 2004-07-29 |
US20070238892A1 (en) | 2007-10-11 |
JP4101803B2 (ja) | 2008-06-18 |
ZA200502080B (en) | 2005-11-30 |
EP1542798A2 (de) | 2005-06-22 |
CN1684769A (zh) | 2005-10-19 |
WO2004028689A2 (en) | 2004-04-08 |
US7250538B2 (en) | 2007-07-31 |
DE60317533D1 (de) | 2007-12-27 |
JP2006500415A (ja) | 2006-01-05 |
AU2003299066A8 (en) | 2004-04-19 |
EP1542798B1 (de) | 2007-11-14 |
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