ATE213060T1 - Lufttrennungsverfahren und vorrichtung zur herstellung von stickstoff - Google Patents

Lufttrennungsverfahren und vorrichtung zur herstellung von stickstoff

Info

Publication number
ATE213060T1
ATE213060T1 AT96308058T AT96308058T ATE213060T1 AT E213060 T1 ATE213060 T1 AT E213060T1 AT 96308058 T AT96308058 T AT 96308058T AT 96308058 T AT96308058 T AT 96308058T AT E213060 T1 ATE213060 T1 AT E213060T1
Authority
AT
Austria
Prior art keywords
bottoms
liquid
stream
column
vaporised
Prior art date
Application number
AT96308058T
Other languages
English (en)
Inventor
Joseph P Naumovitz
Original Assignee
Boc Group Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Boc Group Inc filed Critical Boc Group Inc
Application granted granted Critical
Publication of ATE213060T1 publication Critical patent/ATE213060T1/de

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/044Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air using a single pressure main column system only
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04048Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04006Providing pressurised feed air or process streams within or from the air fractionation unit
    • F25J3/04048Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams
    • F25J3/04066Providing pressurised feed air or process streams within or from the air fractionation unit by compression of cold gaseous streams, e.g. intermediate or oxygen enriched (waste) streams of oxygen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04248Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion
    • F25J3/04284Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams
    • F25J3/04321Generation of cold for compensating heat leaks or liquid production, e.g. by Joule-Thompson expansion using internal refrigeration by open-loop gas work expansion, e.g. of intermediate or oxygen enriched (waste-)streams of oxygen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2200/00Processes or apparatus using separation by rectification
    • F25J2200/72Refluxing the column with at least a part of the totally condensed overhead gas
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2230/00Processes or apparatus involving steps for increasing the pressure of gaseous process streams
    • F25J2230/52Processes or apparatus involving steps for increasing the pressure of gaseous process streams the fluid being oxygen enriched compared to air, e.g. "crude oxygen"
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/02Recycle of a stream in general, e.g. a by-pass stream
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/50Processes or apparatus involving steps for recycling of process streams the recycled stream being oxygen
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/02Bath type boiler-condenser using thermo-siphon effect, e.g. with natural or forced circulation or pool boiling, i.e. core-in-kettle heat exchanger
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2250/00Details related to the use of reboiler-condensers
    • F25J2250/20Boiler-condenser with multiple exchanger cores in parallel or with multiple re-boiling or condensing streams

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Emergency Medicine (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Separation By Low-Temperature Treatments (AREA)
  • Treating Waste Gases (AREA)
  • Separation Of Gases By Adsorption (AREA)
AT96308058T 1995-11-07 1996-11-06 Lufttrennungsverfahren und vorrichtung zur herstellung von stickstoff ATE213060T1 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US08/553,173 US5582034A (en) 1995-11-07 1995-11-07 Air separation method and apparatus for producing nitrogen

Publications (1)

Publication Number Publication Date
ATE213060T1 true ATE213060T1 (de) 2002-02-15

Family

ID=24208392

Family Applications (1)

Application Number Title Priority Date Filing Date
AT96308058T ATE213060T1 (de) 1995-11-07 1996-11-06 Lufttrennungsverfahren und vorrichtung zur herstellung von stickstoff

Country Status (17)

Country Link
US (1) US5582034A (de)
EP (1) EP0773417B1 (de)
JP (1) JP4057668B2 (de)
KR (1) KR100198352B1 (de)
CN (1) CN1103438C (de)
AT (1) ATE213060T1 (de)
AU (1) AU704118B2 (de)
CA (1) CA2183511C (de)
DE (1) DE69619062T2 (de)
IL (1) IL119056A (de)
MX (1) MX9603980A (de)
MY (1) MY118753A (de)
PL (1) PL316839A1 (de)
SG (1) SG44970A1 (de)
TR (1) TR199600708A2 (de)
TW (1) TW360618B (de)
ZA (1) ZA967298B (de)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5689973A (en) * 1996-05-14 1997-11-25 The Boc Group, Inc. Air separation method and apparatus
JP2875206B2 (ja) * 1996-05-29 1999-03-31 日本エア・リキード株式会社 高純度窒素製造装置及び方法
US5924307A (en) * 1997-05-19 1999-07-20 Praxair Technology, Inc. Turbine/motor (generator) driven booster compressor
US5836175A (en) * 1997-08-29 1998-11-17 Praxair Technology, Inc. Dual column cryogenic rectification system for producing nitrogen
JP3719832B2 (ja) * 1997-10-14 2005-11-24 日本エア・リキード株式会社 超高純度窒素及び酸素の製造装置
US5868006A (en) * 1997-10-31 1999-02-09 The Boc Group, Inc. Air separation method and apparatus for producing nitrogen
US5934106A (en) * 1998-01-27 1999-08-10 The Boc Group, Inc. Apparatus and method for producing nitrogen
US6279345B1 (en) 2000-05-18 2001-08-28 Praxair Technology, Inc. Cryogenic air separation system with split kettle recycle
US6494060B1 (en) 2001-12-04 2002-12-17 Praxair Technology, Inc. Cryogenic rectification system for producing high purity nitrogen using high pressure turboexpansion
CN100443838C (zh) * 2005-04-20 2008-12-17 苏州市兴鲁空分设备科技发展有限公司 一种返流膨胀空气分离的方法和装置
CN100400995C (zh) * 2006-11-22 2008-07-09 苏州市兴鲁空分设备科技发展有限公司 空气分离的方法和装置
DE102007024168A1 (de) * 2007-05-24 2008-11-27 Linde Ag Verfahren und Vorrichtung zur Tieftemperatur-Luftzerlegung
DE102007051183A1 (de) 2007-10-25 2009-04-30 Linde Aktiengesellschaft Verfahren zur Tieftemperatur-Luftzerlegung
DE102007051184A1 (de) 2007-10-25 2009-04-30 Linde Aktiengesellschaft Verfahren und Vorrichtung zur Tieftemperatur-Luftzerlegung
DE102008064117A1 (de) 2008-12-19 2009-05-28 Linde Ag Verfahren und Vorrichtung zur Tieftemperaturzerlegung von Luft
JP5415192B2 (ja) * 2009-03-16 2014-02-12 Jfeスチール株式会社 空気の成分分離方法および装置
EP2236964B1 (de) * 2009-03-24 2019-11-20 Linde AG Verfahren und Vorrichtung zur Tieftemperatur-Luftzerlegung
EP2662653A1 (de) 2012-05-08 2013-11-13 Linde Aktiengesellschaft Verfahren und Vorrichtung zur Gewinnung von wasserstofffreiem Stickstoff
EP2789958A1 (de) 2013-04-10 2014-10-15 Linde Aktiengesellschaft Verfahren zur Tieftemperaturzerlegung von Luft und Luftzerlegungsanlage
CN103776240B (zh) * 2014-01-13 2016-07-06 浙江海天气体有限公司 单压缩双增压双膨胀高纯氮制取装置
EP3059536A1 (de) 2015-02-19 2016-08-24 Linde Aktiengesellschaft Verfahren und Vorrichtung zur Gewinnung eines Druckstickstoffprodukts
EP3290843A3 (de) 2016-07-12 2018-06-13 Linde Aktiengesellschaft Verfahren und vorrichtung zur erzeugung von druckstickstoff und flüssigstickstoff durch tieftemperaturzerlegung von luft

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2120374B (en) * 1982-05-11 1985-09-18 Petrocarbon Dev Ltd Improvements in the production of nitrogen from air
JPS61110872A (ja) * 1984-11-02 1986-05-29 日本酸素株式会社 窒素製造方法
JPH05187767A (ja) * 1992-01-14 1993-07-27 Teisan Kk 超高純度窒素製造方法及びその装置
US5363657A (en) * 1993-05-13 1994-11-15 The Boc Group, Inc. Single column process and apparatus for producing oxygen at above-atmospheric pressure
US5396772A (en) * 1994-03-11 1995-03-14 The Boc Group, Inc. Atmospheric gas separation method

Also Published As

Publication number Publication date
DE69619062D1 (de) 2002-03-21
IL119056A0 (en) 1996-11-14
DE69619062T2 (de) 2002-10-31
MY118753A (en) 2005-01-31
KR100198352B1 (ko) 1999-06-15
JPH09132404A (ja) 1997-05-20
TR199600708A2 (tr) 1997-05-21
EP0773417A2 (de) 1997-05-14
KR970025674A (ko) 1997-06-24
SG44970A1 (en) 1997-12-19
US5582034A (en) 1996-12-10
CA2183511A1 (en) 1997-05-08
JP4057668B2 (ja) 2008-03-05
EP0773417B1 (de) 2002-02-06
IL119056A (en) 2000-07-16
AU6430596A (en) 1997-05-15
PL316839A1 (en) 1997-05-12
TW360618B (en) 1999-06-11
AU704118B2 (en) 1999-04-15
EP0773417A3 (de) 1998-02-04
CA2183511C (en) 1999-10-12
ZA967298B (en) 1997-05-22
CN1152108A (zh) 1997-06-18
MX9603980A (es) 1997-05-31
CN1103438C (zh) 2003-03-19

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