AR128428A1 - Formas cristalinas de indoxacarb - Google Patents
Formas cristalinas de indoxacarbInfo
- Publication number
- AR128428A1 AR128428A1 ARP230100247A ARP230100247A AR128428A1 AR 128428 A1 AR128428 A1 AR 128428A1 AR P230100247 A ARP230100247 A AR P230100247A AR P230100247 A ARP230100247 A AR P230100247A AR 128428 A1 AR128428 A1 AR 128428A1
- Authority
- AR
- Argentina
- Prior art keywords
- indoxacarb
- crystalline form
- xrpd pattern
- solid
- isopropanolate
- Prior art date
Links
- 239000005907 Indoxacarb Substances 0.000 title abstract 11
- VBCVPMMZEGZULK-NRFANRHFSA-N indoxacarb Chemical compound C([C@@]1(OC2)C(=O)OC)C3=CC(Cl)=CC=C3C1=NN2C(=O)N(C(=O)OC)C1=CC=C(OC(F)(F)F)C=C1 VBCVPMMZEGZULK-NRFANRHFSA-N 0.000 title abstract 11
- 238000000634 powder X-ray diffraction Methods 0.000 abstract 4
- 239000007787 solid Substances 0.000 abstract 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 abstract 3
- 238000000034 method Methods 0.000 abstract 3
- OGHBATFHNDZKSO-UHFFFAOYSA-N propan-2-olate Chemical compound CC(C)[O-] OGHBATFHNDZKSO-UHFFFAOYSA-N 0.000 abstract 3
- 239000012453 solvate Substances 0.000 abstract 3
- 239000003905 agrochemical Substances 0.000 abstract 2
- 230000009418 agronomic effect Effects 0.000 abstract 2
- 238000001816 cooling Methods 0.000 abstract 2
- 238000001914 filtration Methods 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 238000002360 preparation method Methods 0.000 abstract 2
- 241000607479 Yersinia pestis Species 0.000 abstract 1
- 239000012872 agrochemical composition Substances 0.000 abstract 1
- 230000001476 alcoholic effect Effects 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000009472 formulation Methods 0.000 abstract 1
- 239000002917 insecticide Substances 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 238000001291 vacuum drying Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D273/00—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00
- C07D273/02—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00 having two nitrogen atoms and only one oxygen atom
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N47/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
- A01N47/08—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
- A01N47/28—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
- A01N47/38—Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Indole Compounds (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
La presente divulgación se refiere a formas en estado sólido de indoxacarb o su solvato, procesos para su preparación y composiciones agroquímicas de los mismos. Reivindicación 1: Una forma cristalina B de indoxacarb, que se caracteriza por datos seleccionados de uno o más de los siguientes: i. un patrón de XRPD que tiene picos a 13,5, 13,8, 16,2, 21,2, y 21,4 grados 2-q ± 0,2 grados 2-q; ii. un patrón de XRPD sustancialmente como se muestra en la Figura 1. Reivindicación 3: Una forma cristalina I de Isopropanolato de indoxacarb, caracterizada por datos seleccionados de uno o más de los siguientes: i. un patrón de XRPD que tiene un pico a 5.8 grados 2-q ± 0,2 grados 2-q; ii. un patrón de XRPD sustancialmente como se muestra en la Figura 5. Reivindicación 7: Un método para controlar plagas de lepidópteros mediante la utilización de una forma cristalina de acuerdo con una cualquiera de las reivindicaciones 1 - 4, una composición agroquímica de acuerdo con la reivindicación 5, o una formulación agroquímica de acuerdo con la reivindicación 6, como un insecticida tanto en entornos agronómicos como no agronómicos. Reivindicación 8: Un proceso de preparación de la forma cristalina de indoxacarb de acuerdo con la reivindicación 1, que comprende someter una solución de Forma A de indoxacarb en un sistema de disolvente alcohólico seguido de reflujo, enfriamiento, filtración y secado al vacío para obtener una forma sólida, que es la Forma B de indoxacarb. Reivindicación 11: Un proceso para la preparación de la forma cristalina de solvato de isopropanolato de indoxacarb de acuerdo con la reivindicación 3, que comprende disolver la Forma A de indoxacarb en alcohol Isopropílico a alta temperatura, y luego enfriar sometiendo la solución con indoxacarb sólido adicional seguido por agitación, filtrado y secado para obtener un sólido, que es la Forma I de Solvato de isopropanolato de indoxacarb.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| IN202211005633 | 2022-02-02 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR128428A1 true AR128428A1 (es) | 2024-05-08 |
Family
ID=85283629
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP230100247A AR128428A1 (es) | 2022-02-02 | 2023-02-02 | Formas cristalinas de indoxacarb |
Country Status (2)
| Country | Link |
|---|---|
| AR (1) | AR128428A1 (es) |
| WO (1) | WO2023148735A1 (es) |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5462938A (en) | 1990-12-21 | 1995-10-31 | Annus; Gary D. | Arthropodicidal oxadiazinyl, thiadiazinyl and triazinyl carboxanilides |
| WO1993019045A1 (en) | 1992-03-26 | 1993-09-30 | E.I. Du Pont De Nemours And Company | Arthropodicidal amides |
| EP1357107B1 (en) | 1994-04-20 | 2005-09-07 | E.I. Du Pont De Nemours And Company | Indanones and carbamate, and their use in the preparation of arthropodicial oxadiazines |
| CN105111164B (zh) * | 2013-10-11 | 2018-03-09 | 浙江大学 | 精茚虫威的晶型 |
| AU2017200535A1 (en) * | 2017-01-27 | 2018-08-16 | Rotam Agrochem International Company Limited | A novel crystalline form of indoxacarb, a process for its preparation and use of the same |
| PL3601243T3 (pl) | 2017-03-29 | 2022-04-19 | Adama Makhteshim Ltd. | Układ katalityczny do skalowalnego wytwarzania indoksakarbu |
| EP3997074A4 (en) | 2019-07-10 | 2023-07-05 | Gharda Chemicals Limited | PROCESS FOR OBTAINING INDOXACARB CRYSTALS WITH SPECIFIC PURITY AND ENANTIOMER RATIO |
| WO2021005549A1 (en) | 2019-07-10 | 2021-01-14 | Gharda Chemicals Limited | A process for isolating s-isomer crystals of indoxacarb |
-
2023
- 2023-02-02 WO PCT/IL2023/050118 patent/WO2023148735A1/en unknown
- 2023-02-02 AR ARP230100247A patent/AR128428A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| WO2023148735A1 (en) | 2023-08-10 |
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