AR087321A1 - Metodo para preparar surfactantes a base de acido acilamidocarboxilico graso - Google Patents
Metodo para preparar surfactantes a base de acido acilamidocarboxilico grasoInfo
- Publication number
- AR087321A1 AR087321A1 ARP120102706A ARP120102706A AR087321A1 AR 087321 A1 AR087321 A1 AR 087321A1 AR P120102706 A ARP120102706 A AR P120102706A AR P120102706 A ARP120102706 A AR P120102706A AR 087321 A1 AR087321 A1 AR 087321A1
- Authority
- AR
- Argentina
- Prior art keywords
- salt
- mixture
- acilamidocarboxilic
- fat
- acyl glycinate
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Se provee un procedimiento para la preparación de un ácido de glicinato de acilo C8-22 o su sal, por medio de la reacción y el calentamiento de una mezcla de glicina o sal de ésta con un éster de ácido graso en un medio seleccionado entre el grupo compuesto por glicerol, propilenglicol y combinaciones de ellos, y donde la mezcla tiene un pKa que oscila entre 9,5 y 13.Reivindicación 1: Un procedimiento para la preparación de un ácido de glicinato de acilo C8-22 o su sal, que incluye: (i) hacer reaccionar una mezcla de glicina o sal de ésta con un éster de ácido graso en un medio seleccionado entre el grupo compuesto por glicerol, propilenglicol y combinaciones de ellos, y donde la mezcla tiene un pKa que oscila entre 9,5 y 13; (ii) calentar la mezcla para formar el ácido de glicinato de acilo C8-22 o sal de éste; y (iii) recuperar el ácido de glicinato de acilo C8-22 o sal de éste en una masa resultante de la reacción.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US13/192,489 US8697897B2 (en) | 2011-07-28 | 2011-07-28 | Method for preparing fatty acyl amido carboxylic acid based surfactants |
| US13/343,726 US8822711B2 (en) | 2011-07-28 | 2012-01-05 | Method for preparing fatty acyl amido carboxylic acid based surfactants |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| AR087321A1 true AR087321A1 (es) | 2014-03-12 |
Family
ID=46581996
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ARP120102706A AR087321A1 (es) | 2011-07-28 | 2012-07-26 | Metodo para preparar surfactantes a base de acido acilamidocarboxilico graso |
Country Status (12)
| Country | Link |
|---|---|
| US (1) | US8822711B2 (es) |
| EP (1) | EP2736878B1 (es) |
| JP (1) | JP5940665B2 (es) |
| CN (1) | CN103649043B (es) |
| AR (1) | AR087321A1 (es) |
| BR (1) | BR112014001385B1 (es) |
| CA (1) | CA2839050C (es) |
| EA (1) | EA023748B1 (es) |
| ES (1) | ES2592754T3 (es) |
| MX (1) | MX2014001147A (es) |
| WO (1) | WO2013014268A1 (es) |
| ZA (1) | ZA201309449B (es) |
Families Citing this family (19)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9156777B2 (en) | 2012-07-03 | 2015-10-13 | Stepan Company | Process for preparing N-acyl amino acid salts |
| CA2892035C (en) | 2012-11-21 | 2019-11-05 | Serum Institute Of India Ltd. | Production of neisseria meningitidis x capsular polysaccharide |
| CA2907229A1 (en) | 2013-03-15 | 2014-09-18 | Modular Genetics, Inc. | Generation of acyl amino acids |
| CA2914544A1 (en) | 2013-07-05 | 2015-01-08 | Akzo Nobel Chemicals International B.V. | The synthesis of new anionic surfactants and their use as collectors in froth flotation of non-sulphidic ores |
| ES2670770T3 (es) | 2013-08-19 | 2018-06-01 | Stepan Company | Proceso para la preparación de sales de N-acil aminoácidos |
| CN104607095A (zh) * | 2015-01-30 | 2015-05-13 | 北京工商大学 | 一种制备脂肪酰基苏氨酸钠和包含这种表面活性剂的组合物的方法 |
| CN104741032A (zh) * | 2015-01-30 | 2015-07-01 | 北京工商大学 | 一种制备脂肪酰基蛋氨酸钠和包含这种表面活性剂的组合物的方法 |
| CN104607098A (zh) * | 2015-01-30 | 2015-05-13 | 北京工商大学 | 相转移催化制备油脂酰基亮氨酸钠和包含这种化合物的表面活性剂组合物的方法 |
| KR101880791B1 (ko) * | 2015-10-08 | 2018-07-20 | 주식회사 엘지생활건강 | 아실 글리시네이트 또는 이의 염의 합성 방법 및 이를 사용한 인체 세정제 조성물 |
| CN105439882B (zh) * | 2015-11-11 | 2018-02-09 | 成都惠恩精细化工有限责任公司 | 一种快速、高效的n‑脂肪酰氨基酸盐表面活性剂合成方法 |
| KR101874024B1 (ko) * | 2016-06-29 | 2018-07-04 | 에이케이켐텍 주식회사 | 아미노산계 계면활성제의 제조방법 |
| WO2018001680A1 (de) | 2016-06-29 | 2018-01-04 | Evonik Degussa Gmbh | Verfahren zur herstellung von tensiden |
| KR101915613B1 (ko) * | 2016-09-08 | 2018-11-06 | 주식회사 엘지생활건강 | 아실 알라니네이트 염의 제조방법 및 이를 포함하는 세정제 조성물 |
| KR20190024334A (ko) | 2017-08-31 | 2019-03-08 | 노승호 | 아실글리시네이트 제조방법 및 그것을 이용한 인체세정용 조성물 |
| KR20200007760A (ko) | 2019-12-06 | 2020-01-22 | 노승호 | 아실글리시네이트 제조방법 및 그것을 이용한 인체세정용 조성물 |
| CN111718274B (zh) * | 2020-06-18 | 2023-05-02 | 广州宏度精细化工有限公司 | 油脂酰氨基酸盐的制备方法 |
| EP4256014A1 (en) | 2020-12-01 | 2023-10-11 | Basf Se | Process for preparing surfactant solutions with n-acyl amino acid salts |
| CN115703716A (zh) * | 2021-08-03 | 2023-02-17 | Hg生化有限公司 | 生产氨基酸基表面活性剂的方法 |
| CN114394911A (zh) * | 2021-12-28 | 2022-04-26 | 赞宇科技集团股份有限公司 | 一种月桂酰基谷氨酸钠表面活性剂的制备方法 |
Family Cites Families (27)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3836551A (en) | 1970-01-30 | 1974-09-17 | Roehm Gmbh | Method for making salts of n-acylamino carboxylic acids |
| JPS5758653A (en) | 1980-09-26 | 1982-04-08 | Sagami Chem Res Center | Production of n-acylaminoacid |
| JPH0739380B2 (ja) * | 1986-10-14 | 1995-05-01 | ライオン株式会社 | 脂肪酸アルカノ−ルアミドの製造方法 |
| CA2092182C (en) * | 1990-09-28 | 1998-08-11 | Daniel Stedman Connor | Catalyzed process for glucamide detergents |
| US5194639A (en) * | 1990-09-28 | 1993-03-16 | The Procter & Gamble Company | Preparation of polyhydroxy fatty acid amides in the presence of solvents |
| ES2139737T3 (es) | 1993-03-30 | 2000-02-16 | Ajinomoto Kk | Composicion detergente. |
| WO1995007882A1 (en) * | 1993-09-14 | 1995-03-23 | The Procter & Gamble Company | Synthesis of amido acids from carboxylic acid esters and amino acid salts |
| JPH09509416A (ja) * | 1994-02-17 | 1997-09-22 | ザ、プロクター、エンド、ギャンブル、カンパニー | トリグリセリドからのポリヒドロキシ脂肪酸アミドの合成 |
| DE4408957A1 (de) | 1994-03-17 | 1995-09-21 | Basf Ag | Verfahren zur Herstellung von N-Acylaminocarbonsäuren und N-Acylaminosulfonsäuren sowie deren Alkalimetallsalzen |
| US5646318A (en) * | 1995-04-26 | 1997-07-08 | Akzo Nobel Nv | Process for the preparation of hydroxyalkylamides |
| US5710295A (en) | 1995-06-06 | 1998-01-20 | Hampshire Chemical Corp. | Preparation of alkali metal acyl amino acids |
| US5723673A (en) * | 1995-06-07 | 1998-03-03 | The Procter & Gamble Company | Process for preparing amides of N-alkyl polyhydroxyalkyls |
| JPH11509526A (ja) * | 1995-06-07 | 1999-08-24 | ザ プロクター アンド ギャンブル カンパニー | Ｎ−アルキルポリヒドロキシアルキルアミンのアミドの製造方法 |
| DE19525512A1 (de) * | 1995-07-13 | 1997-01-16 | Basf Ag | Verfahren zur Herstellung von N-Acylaminocarbonsäuren und N-Acylaminosulfonsäuren sowie deren Alkalimetallsalzen |
| JPH0967591A (ja) | 1995-09-04 | 1997-03-11 | Kao Corp | 洗浄剤組成物 |
| JP2006052233A (ja) * | 1996-03-08 | 2006-02-23 | Kaneka Corp | Ｎω−トリフルオロアセチル−塩基性アミノ酸の製造法 |
| FR2786187B1 (fr) | 1998-11-19 | 2001-11-09 | Univ Paris Curie | Composes du type 2-acylamino-2-deoxy-glucono-1,5-lactone, procede d'obtention, compositions les comportant et utilisations |
| WO2002057217A2 (de) | 2001-01-18 | 2002-07-25 | Cognis Deutschland Gmbh & Co. Kg | Verfahren zur herstellung von acylaminosäuren |
| US6703517B2 (en) | 2001-11-26 | 2004-03-09 | Ajinomoto Co., Inc. | Method for preparing N-long chain acyl neutral amino acid |
| US20050176615A1 (en) | 2002-06-25 | 2005-08-11 | Koichi Kinoshita | Detergent compositions |
| US6958085B1 (en) | 2003-03-26 | 2005-10-25 | The United States Of America As Represented By The Administrator Of The National Aeronautics And Space Administration | High performance immobilized liquid membrane for carbon dioxide separations |
| BRPI0414953B1 (pt) | 2003-10-03 | 2016-10-25 | Ajinomoto Kk | composição de limpeza, e, método para preparar um sal de n-acilglicina de cadeia longa |
| JP4696507B2 (ja) | 2004-09-13 | 2011-06-08 | 味の素株式会社 | 洗浄剤組成物 |
| US7318854B2 (en) | 2004-10-29 | 2008-01-15 | New Jersey Institute Of Technology | System and method for selective separation of gaseous mixtures using hollow fibers |
| US20070299269A1 (en) | 2006-06-27 | 2007-12-27 | Conopco, Inc., D/B/A Unilever | Process for converting primary amidoalcohols to amidocarboxylic acids in high yield |
| DE102006038853A1 (de) | 2006-08-18 | 2008-02-21 | Clariant International Limited | Verfahren zur Herstellung von Acylglycinaten mittels Direktoxidation |
| DE102007055265A1 (de) * | 2007-11-20 | 2009-05-28 | Clariant International Ltd. | Verfahren zur Herstellung von Acylglycinaten |
-
2012
- 2012-01-05 US US13/343,726 patent/US8822711B2/en active Active
- 2012-07-26 AR ARP120102706A patent/AR087321A1/es unknown
- 2012-07-27 MX MX2014001147A patent/MX2014001147A/es active IP Right Grant
- 2012-07-27 EA EA201490361A patent/EA023748B1/ru not_active IP Right Cessation
- 2012-07-27 EP EP12740172.7A patent/EP2736878B1/en active Active
- 2012-07-27 JP JP2014522109A patent/JP5940665B2/ja active Active
- 2012-07-27 CA CA2839050A patent/CA2839050C/en active Active
- 2012-07-27 BR BR112014001385-3A patent/BR112014001385B1/pt active IP Right Grant
- 2012-07-27 WO PCT/EP2012/064772 patent/WO2013014268A1/en active Application Filing
- 2012-07-27 ES ES12740172.7T patent/ES2592754T3/es active Active
- 2012-07-27 CN CN201280034881.8A patent/CN103649043B/zh active Active
-
2013
- 2013-12-13 ZA ZA2013/09449A patent/ZA201309449B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| US20130030202A1 (en) | 2013-01-31 |
| US8822711B2 (en) | 2014-09-02 |
| CA2839050A1 (en) | 2013-01-31 |
| JP5940665B2 (ja) | 2016-06-29 |
| WO2013014268A1 (en) | 2013-01-31 |
| BR112014001385A2 (pt) | 2017-02-14 |
| ZA201309449B (en) | 2015-04-29 |
| EP2736878A1 (en) | 2014-06-04 |
| EP2736878B1 (en) | 2016-06-22 |
| EA201490361A1 (ru) | 2014-05-30 |
| BR112014001385B1 (pt) | 2019-10-08 |
| CA2839050C (en) | 2019-03-26 |
| MX2014001147A (es) | 2014-02-27 |
| EA023748B1 (ru) | 2016-07-29 |
| JP2014527519A (ja) | 2014-10-16 |
| CN103649043A (zh) | 2014-03-19 |
| ES2592754T3 (es) | 2016-12-01 |
| CN103649043B (zh) | 2015-09-23 |
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| Date | Code | Title | Description |
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| FB | Suspension of granting procedure |