WO2008041833A8 - Proceso para fabricación de hidróxido de magnesio nanométrico, monodisperso y estable y producto obtenido - Google Patents

Proceso para fabricación de hidróxido de magnesio nanométrico, monodisperso y estable y producto obtenido

Info

Publication number
WO2008041833A8
WO2008041833A8 PCT/MX2007/000045 MX2007000045W WO2008041833A8 WO 2008041833 A8 WO2008041833 A8 WO 2008041833A8 MX 2007000045 W MX2007000045 W MX 2007000045W WO 2008041833 A8 WO2008041833 A8 WO 2008041833A8
Authority
WO
WIPO (PCT)
Prior art keywords
magnesium hydroxide
phase
particles
monodispersed
resulting product
Prior art date
Application number
PCT/MX2007/000045
Other languages
English (en)
French (fr)
Other versions
WO2008041833A1 (es
Inventor
Martinez Jesus Manuel Martinez
Perez Ricardo Benavides
Rojas Jose Gertrudis Bocanegra
Original Assignee
Ind Penoles Sa De Cv
Martinez Jesus Manuel Martinez
Perez Ricardo Benavides
Rojas Jose Gertrudis Bocanegra
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Ind Penoles Sa De Cv, Martinez Jesus Manuel Martinez, Perez Ricardo Benavides, Rojas Jose Gertrudis Bocanegra filed Critical Ind Penoles Sa De Cv
Priority to ES07747191.0T priority Critical patent/ES2533766T3/es
Priority to EP07747191.0A priority patent/EP2088125B1/en
Priority to CA2665523A priority patent/CA2665523C/en
Priority to CN200780044729.7A priority patent/CN101600651B/zh
Priority to BRPI0715311-2A priority patent/BRPI0715311A2/pt
Priority to KR1020097009146A priority patent/KR101370206B1/ko
Priority to US12/443,835 priority patent/US20110045299A1/en
Priority to JP2009531329A priority patent/JP5226688B2/ja
Publication of WO2008041833A1 publication Critical patent/WO2008041833A1/es
Publication of WO2008041833A8 publication Critical patent/WO2008041833A8/es
Priority to IL197708A priority patent/IL197708A0/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/14—Magnesium hydroxide
    • C01F5/22—Magnesium hydroxide from magnesium compounds with alkali hydroxides or alkaline- earth oxides or hydroxides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
    • C01F5/00—Compounds of magnesium
    • C01F5/14—Magnesium hydroxide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00—Crystal-structural characteristics
    • C01P2002/70—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data
    • C01P2002/72—Crystal-structural characteristics defined by measured X-ray, neutron or electron diffraction data by d-values or two theta-values, e.g. as X-ray diagram
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/01—Particle morphology depicted by an image
    • C01P2004/04—Particle morphology depicted by an image obtained by TEM, STEM, STM or AFM
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/51—Particles with a specific particle size distribution
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00—Particle morphology
    • C01P2004/60—Particles characterised by their size
    • C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00—Physical properties of inorganic compounds
    • C01P2006/22—Rheological behaviour as dispersion, e.g. viscosity, sedimentation stability
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
    • Y10T428/00—Stock material or miscellaneous articles
    • Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
    • Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Inorganic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Geology (AREA)
  • Nanotechnology (AREA)
  • Physics & Mathematics (AREA)
  • Composite Materials (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)

Abstract

La presente invención se refiere a un método para preparación de partículas nanométricas de hidróxido de magnesio, teniendo un diámetro promedio de entre 90 y 110 nm, pudiendo estar en un rango de 20 a 160 nm, con características de monodispersión y estabilidades superiores a 12 meses y en un amplio rango de concentraciones. El proceso consta de 3 etapas: una etapa de reacción realizada en 2 pasos, una de maduración y una de purificación. El primer paso de la reacción se realiza en una zona de micromezclado, y el segundo paso es de estabilización de la suspensión. En la segunda etapa, se establece la maduración de las partículas mediante un tratamiento químico-mecánico. La última etapa está diseñada para purificar y concentrar el material, así como la preparación del mismo para integrarse al medio deseado. Las partículas obtenidas son redispersables en diferentes medios, tales como agua, resinas alquidáliσas, fenólicas, nitrocelulosa, poliuretano, vinílicas, acrílicas, alcoholes, y en una amplia variedad de materiales orgánicos y polímeros tales como polietileno de alta y baja densidad, Nylon, ABS y/o mezclas de los mismos.
PCT/MX2007/000045 2006-10-03 2007-04-03 Proceso para fabricación de hidróxido de magnesio nanométrico, monodisperso y estable y producto obtenido WO2008041833A1 (es)

Priority Applications (9)

Application Number Priority Date Filing Date Title
ES07747191.0T ES2533766T3 (es) 2006-10-03 2007-04-03 Método para producir hidróxido de magnesio nanométrico, mono disperso y estable y el producto resultante
EP07747191.0A EP2088125B1 (en) 2006-10-03 2007-04-03 Method for producing stable, monodispersed, nanometric magnesium hydroxide and resulting product
CA2665523A CA2665523C (en) 2006-10-03 2007-04-03 Method for producing stable, monodispersed, nanometric magnesium hydroxide and resulting product
CN200780044729.7A CN101600651B (zh) 2006-10-03 2007-04-03 单分散的稳定的纳米级氢氧化镁的制造方法及所得产品
BRPI0715311-2A BRPI0715311A2 (pt) 2006-10-03 2007-04-03 processo para a produção de mg (oh) 2 nanométrico, mono-disperso e estável e pasa de hidróxido de magnésio
KR1020097009146A KR101370206B1 (ko) 2006-10-03 2007-04-03 나노미터크기의 단분산되고 안정한 수산화마그네슘의 제조 방법 및 생성물
US12/443,835 US20110045299A1 (en) 2006-10-03 2007-04-03 Method for producing stable, monodispersed, nanometric magnesium hydroxide and resulting product
JP2009531329A JP5226688B2 (ja) 2006-10-03 2007-04-03 単分散しておりかつ安定であるナノメートルの水酸化マグネシウムの製造方法、およびその生成物
IL197708A IL197708A0 (en) 2006-10-03 2009-03-19 Process for the fabrication of manometric, zonodispersed and stable magnesium hydroxide and product obtained

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
MXNL06000070A MXNL06000070A (es) 2006-10-03 2006-10-03 Proceso para fabricacion de hidroxido de magnesio nanometrico, monodisperso y estable y producto obtenido.
MXNL/A/2006/000070 2006-10-03

Publications (2)

Publication Number Publication Date
WO2008041833A1 WO2008041833A1 (es) 2008-04-10
WO2008041833A8 true WO2008041833A8 (es) 2008-06-26

Family

ID=39268655

Family Applications (1)

Application Number Title Priority Date Filing Date
PCT/MX2007/000045 WO2008041833A1 (es) 2006-10-03 2007-04-03 Proceso para fabricación de hidróxido de magnesio nanométrico, monodisperso y estable y producto obtenido

Country Status (12)

Country Link
US (1) US20110045299A1 (es)
EP (1) EP2088125B1 (es)
JP (1) JP5226688B2 (es)
KR (1) KR101370206B1 (es)
CN (1) CN101600651B (es)
BR (1) BRPI0715311A2 (es)
CA (1) CA2665523C (es)
ES (1) ES2533766T3 (es)
IL (1) IL197708A0 (es)
MX (1) MXNL06000070A (es)
RU (1) RU2415811C2 (es)
WO (1) WO2008041833A1 (es)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102008031361A1 (de) * 2008-07-04 2010-01-14 K+S Aktiengesellschaft Verfahren zur Herstellung von grob- und/oder nanoskaligen, gecoateten, desagglomerierten Magnesiumhydroxiparikeln
CN102060314B (zh) * 2010-11-30 2012-06-20 沈阳鑫劲粉体工程有限责任公司 一种采用轻烧氧化镁粉合成片状阻燃级氢氧化镁的制备方法
US20120315466A1 (en) * 2011-06-09 2012-12-13 Prc-Desoto International, Inc. Coating compositions including magnesium hydroxide and related coated substrates
CN102275958B (zh) * 2011-07-29 2013-02-06 武汉工程大学 利用硫酸镁原料制备氢氧化镁的方法
JP2014187075A (ja) 2013-03-21 2014-10-02 Toshiba Corp 光結合装置
US20160207788A1 (en) * 2013-04-08 2016-07-21 Tata Chemicals Limited Redispersible magnesium hydroxide and a process for manufacturing the same
RU2561379C2 (ru) * 2013-10-29 2015-08-27 Открытое Акционерное Общество "Каустик" Наночастицы антипирена гидроксида магния и способ их производства
WO2015089777A1 (zh) * 2013-12-18 2015-06-25 中国科学院福建物质结构研究所 一种制造轻质、高比表面积、花球型纳米氢氧化镁的方法
KR102085040B1 (ko) * 2016-09-07 2020-03-05 교와 가가꾸고교 가부시키가이샤 미립자 복합 금속 수산화물, 그 소성물, 그 제조 방법 및 그 수지 조성물
WO2018048142A1 (ko) * 2016-09-12 2018-03-15 주식회사 단석산업 합성 하이드로마그네사이트 입자 및 그의 제조방법
CN106517262A (zh) * 2016-10-21 2017-03-22 吴迪 一种球形纳米氧化镁的制备方法
CN109437258B (zh) * 2018-12-05 2021-02-26 河北镁神科技股份有限公司 一种导热塑料专用氧化镁粉体的制备方法
CN110255590A (zh) * 2019-08-02 2019-09-20 辽宁星空新能源发展有限公司 一种快速沉淀制备氢氧化镁二维纳米片的方法
JP2022186528A (ja) * 2021-06-04 2022-12-15 セトラスホールディングス株式会社 微粒子水酸化マグネシウムを含む殺菌性組成物及び破骨細胞分化抑制用組成物
CN115893459A (zh) * 2022-12-20 2023-04-04 山东沃特斯德新材料科技有限公司 一种多功能水溶性纳米氢氧化镁原液的制备方法
WO2024191320A1 (ru) * 2023-03-15 2024-09-19 Общество с ограниченной ответственностью "ИРКУТСКАЯ НЕФТЯНАЯ КОМПАНИЯ" Способ извлечения гидроксида магния из поликомпонентного гидроминерального сырья

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2404550A (en) * 1941-11-05 1946-07-23 Alfred M Thomsen Method of obtaining magnesia and potash from the waters of the great salt lake
US3692898A (en) * 1970-11-05 1972-09-19 Sterling Drug Inc Aqueous magnesium hydroxide suspensions
JPS5133520B2 (es) * 1972-10-17 1976-09-20
DE3479647D1 (en) * 1983-01-24 1989-10-12 Calgon Corp Aqueous stable magnesium hydroxide suspensions which are dispersible in oil
JPS62132708A (ja) * 1985-12-03 1987-06-16 Nok Corp セラミツクス超微粒子の製造法
WO1992012097A1 (en) * 1990-12-26 1992-07-23 The Dow Chemical Company Magnesium hydroxide having stacked layer, crystalline structure and process therefor
IE921328A1 (en) * 1992-04-23 1993-11-03 Defped Ltd Particulate magnesium hydroxide
MY113181A (en) * 1994-07-23 2001-12-31 Orica Australia Pty Ltd Magnesium hydroxide slurries
IN183464B (es) * 1994-07-25 2000-01-15 Orica Australia Pty Ltd
US5824279A (en) * 1995-01-19 1998-10-20 Martin Marietta Magnesia Specialties, Inc. Process for producing stabilized magnesium hydroxide slurries
US6149967A (en) * 1995-10-09 2000-11-21 Dai Nippon Printing Co., Ltd. Sol solution and method for film formation
CA2320133C (en) * 1998-12-14 2007-05-22 Kyowa Chemical Industry Co., Ltd. Magnesium hydroxide particles, method of the production thereof, and resin composition containing the same
CN1359853A (zh) * 2000-12-19 2002-07-24 中国科学技术大学 针状或薄片状纳米氢氧化镁及其制备方法
CN1142098C (zh) 2000-12-28 2004-03-17 北京化工大学 一种纳米尺寸氢氧化镁的制备方法
CN1332116A (zh) * 2001-08-20 2002-01-23 杜以波 均质流体法制备纳米氢氧化镁
CN1128199C (zh) 2001-09-19 2003-11-19 北京化工大学 一种纳米氢氧化镁阻燃材料制备新工艺
US20030141485A1 (en) * 2002-01-17 2003-07-31 Cesar-Emilio Zertuche-Rodriguez Long term-stabilized magnesium hydroxide suspension for covering iron mineral, a process for its production and application
CN1389521A (zh) 2002-06-26 2003-01-08 冯永成 高抑烟型阻燃剂纳米氢氧化镁的制备及表面处理新方法

Also Published As

Publication number Publication date
JP2010505722A (ja) 2010-02-25
BRPI0715311A2 (pt) 2013-01-01
EP2088125B1 (en) 2014-12-31
IL197708A0 (en) 2009-12-24
CA2665523C (en) 2012-10-09
CA2665523A1 (en) 2008-04-10
CN101600651A (zh) 2009-12-09
RU2009116639A (ru) 2010-11-10
EP2088125A4 (en) 2010-11-10
ES2533766T3 (es) 2015-04-15
KR101370206B1 (ko) 2014-03-05
CN101600651B (zh) 2014-02-12
MXNL06000070A (es) 2008-10-24
US20110045299A1 (en) 2011-02-24
RU2415811C2 (ru) 2011-04-10
KR20090094071A (ko) 2009-09-03
WO2008041833A1 (es) 2008-04-10
EP2088125A1 (en) 2009-08-12
JP5226688B2 (ja) 2013-07-03

Similar Documents

Publication Publication Date Title
WO2008041833A8 (es) Proceso para fabricación de hidróxido de magnesio nanométrico, monodisperso y estable y producto obtenido
KR101197386B1 (ko) 나노 크기의, 단분산성 및 안정한 금속 은의 제조 방법 및 그로부터 얻어지는 생성물
Li et al. Monoclinic BiVO4 with regular morphologies: hydrothermal synthesis, characterization and photocatalytic properties
Jang et al. Synthesis of mesoporous spherical silica via spray pyrolysis: Pore size control and evaluation of performance in paclitaxel pre-purification
He et al. Tuning pore size of mesoporous silica nanoparticles simply by varying reaction parameters
EP1630136A4 (en) FINE PARTICLES OF SURFACE-MODIFIED TITANIUM DIOXIDE AND DISPERSION AND METHOD OF PREPARING THEREOF
Han et al. Facile synthesis of MoS2/Fe3O4 nanocomposite with excellent Photo-Fenton-like catalytic performance
EP2361679A3 (en) Ultrastable particle-stabilized emulsions
WO2008115812A3 (en) Aerogel particles and methods of making same
DE60335189D1 (de) Verfahren zur herstellung von kristallinischen nanopartikeldispersionen
MX2009003984A (es) Particulas submicrobianas amorfas.
JP2012519647A5 (es)
Carvallho et al. Dye removal from textile industrial effluents by adsorption on exfoliated graphite nanoplatelets: kinetic and equilibrium studies
CN105143417A (zh) 高摩尔质量生物材料的水热处理方法
WO2008058958A3 (de) Verfahren zur herstellung einer minisuspoemulsion oder suspension von submikronen kern/schale-partikeln
TW200630300A (en) Single-crystalline diamond fine powder and method for producing the same
Nandiyanto et al. Mesopore-free silica shell with nanometer-scale thickness-controllable on cationic polystyrene core
MXPA02008235A (es) Proceso para la fabricacion de pigmentos.
de Andrade et al. Innovative adsorbent based on graphene oxide decorated with Fe2O3/ZnO nanoparticles for removal of dipyrone from aqueous medium
WO2002040402A1 (fr) Solides inorganiques mesoporeux, leur procede de preparation et leurs utilisations notamment comme catalyseurs et adsorbants
MY147403A (en) Composition containing medicine extremely slightly solube in water and method for preparation thereof
Sangsuradet et al. Modified hierarchical zeolite X derived from riceberry rice husk for propionic acid adsorption
WO2009071862A3 (fr) Poudre de particules nanometriques purifiee
Shi et al. Effects of synthetic routes on the compositional and structural properties of dendritic mesoporous organosilica nanoparticles: The unexpected reversed “double-edged sword” role of reaction time
EP2903935B1 (en) Compositions and processes for synthesizing cubic mesoporous silicas having "noodle-like" morphology

Legal Events

Date Code Title Description
WWE Wipo information: entry into national phase

Ref document number: 200780044729.7

Country of ref document: CN

121 Ep: the epo has been informed by wipo that ep was designated in this application

Ref document number: 07747191

Country of ref document: EP

Kind code of ref document: A1

DPE1 Request for preliminary examination filed after expiration of 19th month from priority date (pct application filed from 20040101)
WWE Wipo information: entry into national phase

Ref document number: 549/MUMNP/2009

Country of ref document: IN

ENP Entry into the national phase

Ref document number: 2009531329

Country of ref document: JP

Kind code of ref document: A

ENP Entry into the national phase

Ref document number: 2665523

Country of ref document: CA

NENP Non-entry into the national phase

Ref country code: DE

WWE Wipo information: entry into national phase

Ref document number: 1020097009146

Country of ref document: KR

Ref document number: 2007747191

Country of ref document: EP

ENP Entry into the national phase

Ref document number: 2009116639

Country of ref document: RU

Kind code of ref document: A

WWE Wipo information: entry into national phase

Ref document number: 12443835

Country of ref document: US

DPE1 Request for preliminary examination filed after expiration of 19th month from priority date (pct application filed from 20040101)
ENP Entry into the national phase

Ref document number: PI0715311

Country of ref document: BR

Kind code of ref document: A2

Effective date: 20090403