US3861652A

US3861652A - Mixing device

Info

Publication number: US3861652A
Application number: US306921A
Authority: US
Inventors: Richard Allen Clark; John William Coryell
Original assignee: EI Du Pont de Nemours and Co
Current assignee: EIDP Inc
Priority date: 1972-11-15
Filing date: 1972-11-15
Publication date: 1975-01-21
Anticipated expiration: 1992-01-21
Also published as: AR199931A1; NL7315604A; BR7308926D0; CA991632A; GB1394519A

Abstract

The use of a screen structure between groups of static mixing elements located in a conduit through which tow or more liquids flow increases mixing efficiency.

Description

United States Patent I [191 Clark et al.

[ 1 Jan. 21, 1975 MIXING DEVICE Inventors: Richard Allen Clark; John William Coryell, both of Waynesboro, Va.

Assignee: E. I. du Pont de Nemours and C0.,

Wilmington, Del.

Filed: Nov. 15, 1972 Appl. No.: 306,921

US. Cl. 259/4 Int. Cl B011 15/02 Field of Search 259/4, 18, 36, 60; 138/38 References Cited UNITED STATES PATENTS 11/1966 Armeniades 259/4 8/1967 Katzer 259/4 3,635,444 1/l972 Potter 259/4 3,664,638 5/1972 Grout H 259/4 3,704,006 11/1972 Grout 4. 259/4 Primary Examiner-Robert W. Jenkins [57] ABSTRACT The use of a screen structure between groups of static mixing elements locatedin a conduit through which tow or more liquids flow increases mixing efficiency.

2 Claims, 2 Drawing Figures Patented Jan. 21, 1975 3,861,652

MIXING DEVICE BACKGROUND OF THE INVENTION This invention relates to a device for mixing two or more liquids of highly differing viscosities. In particular, the invention is concerned with an improvement on a mixer having no moving parts.

Armeniades et al., in U.S. Pat. No. 3,286,992 disclose a mixer that consists of a hollow tube or pipe containing a series of curved dividing elements that provide repeated division and recombination of the materials to be mixed as they flow through the tube. The chief mechanisms for accomplishing mixing in such a device are flow division and radial mixing. Flow inversion and backmixing contribute to a lesser extent. Where miscible liquid systems are being combined, diffusion across the flow strata in the mixer enhances mixing somewhat. However, for an all-liquid system in which the constituents possess widely differing viscosities, mixing performance is determined almost exclusively by the amount of flow division attained. In such systems in which the viscosity ratio of the liquids is 1,000 or higher, globules or islands of the high viscosity component tend to form after passing the first few curved dividing elements of the mixer. These discrete particles then pass the remaining elements essentially unchanged. This problem is aggravated in those systems in which the low viscosity component is in volumetric excess.

Attempts to overcome this problem by increasing the number of dividing elements often result in a prohibitively large pressure drop through the mixer. The problem of excessive pressure drop through such mixers is recognized by Grout et al., U.S. Pat. No. 3,664,638.

SUMMARY OF THE INVENTION It has been found that the problem of undissolved high viscosity inhomogeneities in such systems may be overcome by the use of one or more fine mesh screens or other foraminous structures placed between sets of Armeniades et al. mixer elements. The use of a screen between the mixer elements greatly increases the mixing efficiency. Thus, fewer mixer elements are needed and a lower pressure drop results.

BRIEF DESCRIPTION OF THE DRAWING FIG. 1 is a partially sectioned view of one embodiment of the invention, showing a screen section be tween mixing sections;

FIG. 2 is a partial perspective view partly in section of the screen section of FIG. 1.

DETAILED DESCRIPTION OF THE ILLUSTRATED EMBODIMENT In the drawing, a hollow cylindrical tube of uniform cross section consists of a premixing section 12, an initial mixing section 13, a screen section 14 and a final mixing section 15. Low viscosity liquid A is fed directly into premixing section 12 and high viscosity liquid B is introduced through flow distributor 16 having several orifices 17. From delivery end 18 of the tube issues a homogeneous mixture of A and B. Within the initial mixing section 13 and final mixing section of tube 10 are sets of

curved elements

20, 21, 22, etc., and 30, 29, etc., respectively. As more fully described in the aforementioned Armeniades et al. patent, the downstream edge of each of the

elements

20, 21 29, 30,

are positioned at a substantial angle to the upstream edge of the next adjacent one. The elements are preferably physically connected, eg. by welding or brazing at their contact point 33. Two cylindrical screens 34 having solid end plates 36 are mounted in the end walls 35 of screen section 14.

The screens placed between sets of the curved mixer elements are positioned in such a way that the liquid stream is required to pass through the meshes of the screens. The screens may be planar, cylindrical or of any desired shape. If planar, they are conveniently positioned transversely in the hollow tube between sets of the mixing elements. If cylindrical, they may be positioned, for example, as shown in the drawing. ln general, a screen having a mesh opening approximately. equal to the maximum particle size of the undissolved high viscosity globules gives satisfactory results. In such a case, the screen does not serve as a filter since the averageparticle size is smaller than the mesh opening, However, the invention will operate satisfactorily even if the average particle size is not smaller than the mesh opening. Usually screens of I00 mesh or finerwill be effective and are preferred.

In an example, a mixer consisting of a set of 35 Armeniades et al. elements followed by two ZOO-mesh cy-- lindrical screens followed in turn by a set of 21 elements produced complete mixing in the following system: 4 parts of a high viscosity liquid (440 poises) and 6 parts of a low viscosity solvent (1 centipoise) at 30C.

The viscosity ratio was 44,000/1. Good'mixing was indicated by no'discernible globules of the high viscosity component in the effluent and no buildup on the screens. Similar results were obtained in a two component liquid system having a viscosity ratio of approximately 150,000/l.

In the operation of the embodiment illustrated in the drawing, it is preferred that the coaxially oriented flow distributor l6 and the initial mixing section 13 be disposed within 10 of a vertical position, most preferably, absolutely vertical. Flow direction, either up or down, has not been found to make a significant difference in efficiency of mixing.

The concept of using fine mesh screens between sets of Armeniades et'al. mixer elements for the purpose of dividing or dispersing the higher viscosity component is applicable to any liquid system. It is especially beneficial in those cases where precise drop size is a critical objective or in those instances where an excessive number of mixer elements would otherwise be required to achieve the desired degree of mixing and/or in'obtaining homogeneous mixing with minimum pressure drop.

Although the invention has been described using two spaced groups of elements or mixing sections l3, 15 of the same diameter, more than two mixing sections as well as mixing sections of differing diameters may be used with a screen section incorporated between at least two of the mixing sections.

What is claimed is:

1. In a device for mixing a plurality of flowing liquids including a hollow cylindrical tube and a plurality of curved mixing elements positioned in said tube. the improvement comprising: said elements being formed in spaced groups and a cylindrical shaped screen positioned between at least two spaced groups of elements, said screen having a diameter less than the diameter of the conduit, said screen being connected to the walls of the conduit at one end and being closed at the other groups of elements, said second screen being the same end. as the first screen and having its closed end adjacent 2. The device as defined in claim 1, including a secthe closed end of the first screen. ond cylindrical shaped screen positioned between said

Claims

1. In a device for mixing a plurality of flowing liquids including a hollow cylindrical tube and a plurality of curved mixing elements positioned in said tube, the improvement comprising: said elements being formed in spaced groups and a cylindrical shaped screen positioned between at least two spaced groups of elements, said screen having a diameter less than the diameter of the conduit, said screen being connected to the walls of the conduit at one end and being closed at the other end.

2. The device as defined in claim 1, including a second cylindrical shaped screen positioned between said groups of elements, said second screen being the same as the first screen and having its closed end adjacent the closed end of the first screen.