US1300250A - Process of making adhesive material. - Google Patents
Process of making adhesive material. Download PDFInfo
- Publication number
- US1300250A US1300250A US5967315A US5967315A US1300250A US 1300250 A US1300250 A US 1300250A US 5967315 A US5967315 A US 5967315A US 5967315 A US5967315 A US 5967315A US 1300250 A US1300250 A US 1300250A
- Authority
- US
- United States
- Prior art keywords
- adhesive material
- roll
- mixture
- web
- adhesive
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000853 adhesive Substances 0.000 title description 17
- 230000001070 adhesive effect Effects 0.000 title description 17
- 239000000463 material Substances 0.000 title description 11
- 238000000034 method Methods 0.000 title description 5
- 239000000203 mixture Substances 0.000 description 16
- 239000003292 glue Substances 0.000 description 8
- 235000015110 jellies Nutrition 0.000 description 5
- 239000008274 jelly Substances 0.000 description 5
- 239000004615 ingredient Substances 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- 239000002904 solvent Substances 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 239000006188 syrup Substances 0.000 description 2
- 235000020357 syrup Nutrition 0.000 description 2
- 235000015192 vegetable juice Nutrition 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 235000011054 acetic acid Nutrition 0.000 description 1
- 125000000218 acetic acid group Chemical group C(C)(=O)* 0.000 description 1
- 235000015165 citric acid Nutrition 0.000 description 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid group Chemical class C(CC(O)(C(=O)O)CC(=O)O)(=O)O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 1
- 238000010411 cooking Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 239000004744 fabric Substances 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 239000011877 solvent mixture Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000002906 tartaric acid Nutrition 0.000 description 1
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D67/00—Processes specially adapted for manufacturing semi-permeable membranes for separation processes or apparatus
- B01D67/0002—Organic membrane manufacture
- B01D67/0009—Organic membrane manufacture by phase separation, sol-gel transition, evaporation or solvent quenching
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B29—WORKING OF PLASTICS; WORKING OF SUBSTANCES IN A PLASTIC STATE IN GENERAL
- B29D—PRODUCING PARTICULAR ARTICLES FROM PLASTICS OR FROM SUBSTANCES IN A PLASTIC STATE
- B29D7/00—Producing flat articles, e.g. films or sheets
- B29D7/01—Films or sheets
Definitions
- My invention relates to a method of manufacturing the novel adhesive material fully described in an application filed November 4, 1915, Serial No. 59,672.
- I have described in detail an adhesive material composed of animal glue, .insp'issated vegetable juices, a solvent composed of tartaric, acetic, and citric acids and Water, and a small quantity of sodium chlorid.
- I Said adhesive when completed is preferably in the form of a sheet or tape without a fabric or paper backing and is dry and non-adhesive at ordinary atmospheric temperatures, but becomes fluid 2nd strongly adhesive on the application of cat.
- I dissolve five per cent. of sodium chlorid in the acid solvent, equal portions ofanimal glue and this solvent containing the chlorid of sodium are then put together and allowed to-soak five or six hours, or even longer, forming a glue'je'lly.
- Two parts of the inspissated vegetable juices and one part of the acid solvent mixture such as stated arecooked syrup mixture are then'mixed in the proportion of about two parts of the glue jelly to one of the cooked syrup mixture in a jacketed kettle and heated to a temperature of about 160 to 180 Fahr. being ma1ntained at this temperature and thoroughly stirred for about two hours.
- the mixture thus produced is placed in a jacketed trough or basin 11 inwhich the mixture is maintained at a proper temperature to keep it in liquid form and at the same time to drive off as little of the solvent contained therein as possible.
- a roll 12 is mounted to revolve in the basin, the lower part of the roll dipping in the mixture.
- a doctor or scraper arranged on one side of the roll and adjustable by means of the screw l t to or from the periphery of the roll so as to allow the operator to control the thickness of the layer of adhesive material taken up by the roll as it revolves.
- an inclined scraper 15 On the opposite side of the roll from the doctor, is an inclined scraper 15, the top edge.
- This inclined scraper is at an angle of about 45 and has raised sides to keep the adhesive material from running over the edges as it runs down the incline of the scraper.
- an endless metal belt 16 which travel-s forward at a correct speed so that the adhesive material is laid in a continuous web 30 on this belt or apron. The thickness of the web is varied according to the position at which the doctor or scraper is set with relation to the surface of the roll 12.
- cooling pipes by which the apron 16 is-maintained at a low temperature so that it instantly chills the adhesive.
- the metal apron 16 is of considerable length and inclosed in a box 18 through which a current of air is circulated by a fan 19, to produce a slight drying action by removing a small amount of the moisture from the sur-, face of the Web of adhesive material.
- a small amount of oil or some other suitable substance is applied to the surface of the traveling apron to prevent the web adhering to it. This oil is applied to the outer side of the metal apron by means of a felt covered roll 22 and any surplus is removed by a similar roll 23:
- a trough 20 by'which there is applied to the top surface of the strip of At 24 is shown a soft felt or bristle roll which removes from the surface of the Web of adhesive material the surplus powder and also fubs or polishes the surface imparting to it a texture something like that of rubber tissue.
- the web of adhesive material passes around the guide rolls 25 and 26 and then under the second trough 27 which deposits powder 28 on the opposite side of the strip.
- a roll similar to the roll 24 which treats the surfaceun the same way, the Web of adhesive, material being at this time supported on a of the ingredients and allowing them to soak for a period of time to form a glue jelly, cooklng a mixture of other ingredients until the said -mixture congeals quickly when dropped in cold water and mixing the said glue jelly with said cooked mixture and then heating the combined mixture, then forming a Web of said combined mixtures after they have been heated.
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dispersion Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mechanical Engineering (AREA)
- Adhesives Or Adhesive Processes (AREA)
Description
C. H. CROWELL.
PROCESS OF MAKING ADHESIVE MATERIAL.
APPLICATION FILED NOV. 4, 1915.
1,300,250. Patented Apr. 15,1919.
O G O ff To all whom it may concern:
CHARLES H. CROWELL, OF BROOKLYN, NEW YORK.
PROCESS OF MAKING ADHESIVE MATEBIAL- I Specification of Letters Patent.
Patented Apr. 15, 1919.
Application filed November '4, 1915. Serial No. 59,673.
Be it known that I, CHARLES H. CRowELL', a citizen of the United States, residing at Brooklyn, county of Kings, Stateof New York, have invented a certain new and useful Improvement in Processes of Making Adhesive Material, of which the following is a specification, reference being had therein to the accompanying drawings.
My invention relates to a method of manufacturing the novel adhesive material fully described in an application filed November 4, 1915, Serial No. 59,672.
In that application, I have described in detail an adhesive material composed of animal glue, .insp'issated vegetable juices, a solvent composed of tartaric, acetic, and citric acids and Water, and a small quantity of sodium chlorid. I Said adhesive when completed is preferably in the form of a sheet or tape without a fabric or paper backing and is dry and non-adhesive at ordinary atmospheric temperatures, but becomes fluid 2nd strongly adhesive on the application of cat.
My invention will be fully understood by reference to the following description taken in connection with the accompanying drawings, and the novel features thereof are pointed out and clearly defined in the claims at the close of this specification. M
In the drawing the figure is a side elevation of an apparatus by means of which certain steps of the herein described process are practised. It will be understood that it-is necessary to heat or cook as a partof the method of manufacture of the mixture but it has not-been thought necessary to illustrate any device for performing this step as the ordinary open jacketed steamkettle may be employed. c
In the manufacture of my adhesive in accordance with the herein described process,
I dissolve five per cent. of sodium chlorid in the acid solvent, equal portions ofanimal glue and this solvent containing the chlorid of sodium are then put together and allowed to-soak five or six hours, or even longer, forming a glue'je'lly. Two parts of the inspissated vegetable juices and one part of the acid solvent mixture such as stated arecooked syrup mixture are then'mixed in the proportion of about two parts of the glue jelly to one of the cooked syrup mixture in a jacketed kettle and heated to a temperature of about 160 to 180 Fahr. being ma1ntained at this temperature and thoroughly stirred for about two hours.
The mixture thus produced is placed in a jacketed trough or basin 11 inwhich the mixture is maintained at a proper temperature to keep it in liquid form and at the same time to drive off as little of the solvent contained therein as possible. A roll 12 is mounted to revolve in the basin, the lower part of the roll dipping in the mixture. At 13 is shown a doctor or scraper arranged on one side of the roll and adjustable by means of the screw l t to or from the periphery of the roll so as to allow the operator to control the thickness of the layer of adhesive material taken up by the roll as it revolves.
On the opposite side of the roll from the doctor, is an inclined scraper 15, the top edge.
- of which is pressed against the roll 12. This inclined scraper is at an angle of about 45 and has raised sides to keep the adhesive material from running over the edges as it runs down the incline of the scraper. Below this scraper 15, is an endless metal belt 16 which travel-s forward at a correct speed so that the adhesive material is laid in a continuous web 30 on this belt or apron. The thickness of the web is varied according to the position at which the doctor or scraper is set with relation to the surface of the roll 12. At 17 are shown cooling pipes by which the apron 16 is-maintained at a low temperature so that it instantly chills the adhesive. The metal apron 16 is of considerable length and inclosed in a box 18 through which a current of air is circulated by a fan 19, to produce a slight drying action by removing a small amount of the moisture from the sur-, face of the Web of adhesive material. A small amount of oil or some other suitable substance is applied to the surface of the traveling apron to prevent the web adhering to it. This oil is applied to the outer side of the metal apron by means of a felt covered roll 22 and any surplus is removed by a similar roll 23:
At the end of the apron farthest from the roll 12 is located a trough 20 by'which there is applied to the top surface of the strip of At 24 is shown a soft felt or bristle roll which removes from the surface of the Web of adhesive material the surplus powder and also fubs or polishes the surface imparting to it a texture something like that of rubber tissue. After passing the roll 24 the web of adhesive material passes around the guide rolls 25 and 26 and then under the second trough 27 which deposits powder 28 on the opposite side of the strip. At 29 is shown a roll similar to the roll 24 which treats the surfaceun the same way, the Web of adhesive, material being at this time supported on a of the ingredients and allowing them to soak for a period of time to form a glue jelly, cooklng a mixture of other ingredients until the said -mixture congeals quickly when dropped in cold water and mixing the said glue jelly with said cooked mixture and then heating the combined mixture, then forming a Web of said combined mixtures after they have been heated.
2. The method of making a web of adhesive which consists in mixing together some of the ingredients and allowing them to soak for a period of time to form a glue jelly, cooking a mixture of other ingredients until the said mixture congeals quickly when dropped in cold water and mixing the said glue jelly with said cooked mixture and then heating the combined mixture, then forming a 'Web of said combined mixtures after they have been heated, and then chilling the web to harden the same.
In testimony whereof I afiix my signature, in presence of two witnesses.
CHARLES H. CROWELL.
Witnesses:
GEORGE P. DIKE, ALICE H. MORRISON.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US5967315A US1300250A (en) | 1915-11-04 | 1915-11-04 | Process of making adhesive material. |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US5967315A US1300250A (en) | 1915-11-04 | 1915-11-04 | Process of making adhesive material. |
Publications (1)
Publication Number | Publication Date |
---|---|
US1300250A true US1300250A (en) | 1919-04-15 |
Family
ID=3367791
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
US5967315A Expired - Lifetime US1300250A (en) | 1915-11-04 | 1915-11-04 | Process of making adhesive material. |
Country Status (1)
Country | Link |
---|---|
US (1) | US1300250A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3602944A (en) * | 1969-01-30 | 1971-09-07 | Licencia Talalmanyokat | Apparatus for the manufacture of synthetic leather |
-
1915
- 1915-11-04 US US5967315A patent/US1300250A/en not_active Expired - Lifetime
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3602944A (en) * | 1969-01-30 | 1971-09-07 | Licencia Talalmanyokat | Apparatus for the manufacture of synthetic leather |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
US2251295A (en) | Method and apparatus for coating sheet materials | |
US2221019A (en) | Coating of film bases | |
US1300250A (en) | Process of making adhesive material. | |
US1318464A (en) | A cobporation of dela | |
US3950561A (en) | Shortening chip manufacture | |
US1157149A (en) | Apparatus for making sheet material. | |
US904231A (en) | Process of manufacturing butterin. | |
US1047760A (en) | Manufacture of a fish food. | |
US1582158A (en) | Method of and apparatus for making sheet ice | |
US1239766A (en) | Process of drying casein. | |
US1608147A (en) | Method and apparatus for withdrawing water from substances and immediately thereafter binding the water | |
US2040549A (en) | Method and apparatus for making sheet rubber | |
US1445004A (en) | Method of and apparatus for solidifying materials | |
US3554765A (en) | Preparation of plasticized cheese | |
US668162A (en) | Process of desiccating milk. | |
US2728952A (en) | Method of making films | |
US1401965A (en) | Apparatus eor manufacturing glue | |
US1321401A (en) | Process and apparatus for making wax films. | |
GB1603150A (en) | Method and apparatus for the formation of bean curd film | |
US326687A (en) | Edward gilbert sparks | |
US1339327A (en) | Method of manufacturing prepardd roofing | |
US2675779A (en) | Apparatus for making films | |
US1651939A (en) | Apparatus for coating articles | |
US1965509A (en) | Method of forming small particle products from gelatinizing substances | |
GB306622A (en) | Improvements in and relating to the manufacture of glue, gelatine and other like material in the form of globules or pellets |