JPH0138787B2 - - Google Patents

Info

Publication number: JPH0138787B2
Authority: JP; Japan
Prior art keywords: isocyanurate; hydroxypropyl; water; acetonyl; acid
Prior art date: 1982-11-17
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Expired

Application number

JP20241282A

Other languages

English (en)

Japanese (ja)

Other versions

JPS5993064A (ja

Inventor

Hisao Kitano

Fumio Tanimoto

Yoshiharu Inoe

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Seisan Kaihatsu Kagaku Kenkyusho

Original Assignee

Seisan Kaihatsu Kagaku Kenkyusho

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1982-11-17

Filing date

1982-11-17

Publication date

1989-08-16

1982-11-17 Application filed by Seisan Kaihatsu Kagaku Kenkyusho filed Critical Seisan Kaihatsu Kagaku Kenkyusho

1982-11-17 Priority to JP20241282A priority Critical patent/JPS5993064A/ja

1984-05-29 Publication of JPS5993064A publication Critical patent/JPS5993064A/ja

1989-08-16 Publication of JPH0138787B2 publication Critical patent/JPH0138787B2/ja

Status Granted legal-status Critical Current

Links

-1 acetonyl isocyanurate Chemical compound 0.000 claims description 39
ZFSLODLOARCGLH-UHFFFAOYSA-N isocyanuric acid Chemical compound OC1=NC(O)=NC(O)=N1 ZFSLODLOARCGLH-UHFFFAOYSA-N 0.000 claims description 12
150000001875 compounds Chemical class 0.000 claims description 10
KOMNUTZXSVSERR-UHFFFAOYSA-N 1,3,5-tris(prop-2-enyl)-1,3,5-triazinane-2,4,6-trione Chemical compound C=CCN1C(=O)N(CC=C)C(=O)N(CC=C)C1=O KOMNUTZXSVSERR-UHFFFAOYSA-N 0.000 claims description 8
239000002798 polar solvent Substances 0.000 claims description 6
239000007983 Tris buffer Substances 0.000 claims description 5
238000004519 manufacturing process Methods 0.000 claims description 3
230000001590 oxidative effect Effects 0.000 claims description 2
QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 34
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 29
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 24
QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 18
239000000047 product Substances 0.000 description 14
238000006243 chemical reaction Methods 0.000 description 13
239000000203 mixture Substances 0.000 description 13
239000000284 extract Substances 0.000 description 12
238000000034 method Methods 0.000 description 11
238000003756 stirring Methods 0.000 description 11
CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 10
239000007800 oxidant agent Substances 0.000 description 10
238000007254 oxidation reaction Methods 0.000 description 10
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 9
YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 9
230000003647 oxidation Effects 0.000 description 9
MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 description 8
HEDRZPFGACZZDS-MICDWDOJSA-N Trichloro(2H)methane Chemical compound [2H]C(Cl)(Cl)Cl HEDRZPFGACZZDS-MICDWDOJSA-N 0.000 description 8
239000011541 reaction mixture Substances 0.000 description 8
239000002253 acid Substances 0.000 description 7
RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 6
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 6
WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 6
238000000921 elemental analysis Methods 0.000 description 6
NUJOXMJBOLGQSY-UHFFFAOYSA-N manganese dioxide Chemical compound O=[Mn]=O NUJOXMJBOLGQSY-UHFFFAOYSA-N 0.000 description 6
239000002994 raw material Substances 0.000 description 6
239000000243 solution Substances 0.000 description 6
125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 description 5
GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 5
239000007864 aqueous solution Substances 0.000 description 5
KRVSOGSZCMJSLX-UHFFFAOYSA-L chromic acid Substances O[Cr](O)(=O)=O KRVSOGSZCMJSLX-UHFFFAOYSA-L 0.000 description 5
AWJWCTOOIBYHON-UHFFFAOYSA-N furo[3,4-b]pyrazine-5,7-dione Chemical compound C1=CN=C2C(=O)OC(=O)C2=N1 AWJWCTOOIBYHON-UHFFFAOYSA-N 0.000 description 5
229910017604 nitric acid Inorganic materials 0.000 description 5
239000002904 solvent Substances 0.000 description 5
HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
238000001816 cooling Methods 0.000 description 4
238000004821 distillation Methods 0.000 description 4
230000036571 hydration Effects 0.000 description 4
238000006703 hydration reaction Methods 0.000 description 4
150000003839 salts Chemical class 0.000 description 4
PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 3
HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
125000001539 acetonyl group Chemical group [H]C([H])([H])C(=O)C([H])([H])* 0.000 description 3
238000004458 analytical method Methods 0.000 description 3
229940117975 chromium trioxide Drugs 0.000 description 3
LSRJXMDEXXKFCD-UHFFFAOYSA-L chromium(6+) dihydroxy(dioxo)chromium oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Cr+6].O[Cr](O)(=O)=O LSRJXMDEXXKFCD-UHFFFAOYSA-L 0.000 description 3
GAMDZJFZMJECOS-UHFFFAOYSA-N chromium(6+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Cr+6] GAMDZJFZMJECOS-UHFFFAOYSA-N 0.000 description 3
239000013078 crystal Substances 0.000 description 3
238000000354 decomposition reaction Methods 0.000 description 3
229910052736 halogen Inorganic materials 0.000 description 3
239000007788 liquid Substances 0.000 description 3
239000007791 liquid phase Substances 0.000 description 3
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 3
239000000126 substance Substances 0.000 description 3
230000019635 sulfation Effects 0.000 description 3
238000005670 sulfation reaction Methods 0.000 description 3
JYEUMXHLPRZUAT-UHFFFAOYSA-N 1,2,3-triazine Chemical group C1=CN=NN=C1 JYEUMXHLPRZUAT-UHFFFAOYSA-N 0.000 description 2
OJVAMHKKJGICOG-UHFFFAOYSA-N 2,5-hexanedione Chemical group CC(=O)CCC(C)=O OJVAMHKKJGICOG-UHFFFAOYSA-N 0.000 description 2
HSJKGGMUJITCBW-UHFFFAOYSA-N 3-hydroxybutanal Chemical compound CC(O)CC=O HSJKGGMUJITCBW-UHFFFAOYSA-N 0.000 description 2
YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 2
KRHYYFGTRYWZRS-UHFFFAOYSA-N Fluorane Chemical compound F KRHYYFGTRYWZRS-UHFFFAOYSA-N 0.000 description 2
NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 2
230000002378 acidificating effect Effects 0.000 description 2
150000007513 acids Chemical class 0.000 description 2
230000015572 biosynthetic process Effects 0.000 description 2
SOCTUWSJJQCPFX-UHFFFAOYSA-N dichromate(2-) Chemical compound [O-][Cr](=O)(=O)O[Cr]([O-])(=O)=O SOCTUWSJJQCPFX-UHFFFAOYSA-N 0.000 description 2
GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 description 2
238000001035 drying Methods 0.000 description 2
238000000605 extraction Methods 0.000 description 2
238000002329 infrared spectrum Methods 0.000 description 2
230000035484 reaction time Effects 0.000 description 2
238000001953 recrystallisation Methods 0.000 description 2
GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 description 2
238000001179 sorption measurement Methods 0.000 description 2
238000001228 spectrum Methods 0.000 description 2
238000003786 synthesis reaction Methods 0.000 description 2
IHCCLXNEEPMSIO-UHFFFAOYSA-N 2-[4-[2-(2,3-dihydro-1H-inden-2-ylamino)pyrimidin-5-yl]piperidin-1-yl]-1-(2,4,6,7-tetrahydrotriazolo[4,5-c]pyridin-5-yl)ethanone Chemical compound C1C(CC2=CC=CC=C12)NC1=NC=C(C=N1)C1CCN(CC1)CC(=O)N1CC2=C(CC1)NN=N2 IHCCLXNEEPMSIO-UHFFFAOYSA-N 0.000 description 1
VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
VCUFZILGIRCDQQ-KRWDZBQOSA-N N-[[(5S)-2-oxo-3-(2-oxo-3H-1,3-benzoxazol-6-yl)-1,3-oxazolidin-5-yl]methyl]-2-[[3-(trifluoromethoxy)phenyl]methylamino]pyrimidine-5-carboxamide Chemical compound O=C1O[C@H](CN1C1=CC2=C(NC(O2)=O)C=C1)CNC(=O)C=1C=NC(=NC=1)NCC1=CC(=CC=C1)OC(F)(F)F VCUFZILGIRCDQQ-KRWDZBQOSA-N 0.000 description 1
UIIMBOGNXHQVGW-DEQYMQKBSA-M Sodium bicarbonate-14C Chemical compound [Na+].O[14C]([O-])=O UIIMBOGNXHQVGW-DEQYMQKBSA-M 0.000 description 1
VYGUBTIWNBFFMQ-UHFFFAOYSA-N [N+](#[C-])N1C(=O)NC=2NC(=O)NC2C1=O Chemical group [N+](#[C-])N1C(=O)NC=2NC(=O)NC2C1=O VYGUBTIWNBFFMQ-UHFFFAOYSA-N 0.000 description 1
GOPYZMJAIPBUGX-UHFFFAOYSA-N [O-2].[O-2].[Mn+4] Chemical class [O-2].[O-2].[Mn+4] GOPYZMJAIPBUGX-UHFFFAOYSA-N 0.000 description 1
150000001299 aldehydes Chemical class 0.000 description 1
229910001854 alkali hydroxide Inorganic materials 0.000 description 1
150000008044 alkali metal hydroxides Chemical class 0.000 description 1
239000012670 alkaline solution Substances 0.000 description 1
150000001336 alkenes Chemical class 0.000 description 1
229910000147 aluminium phosphate Inorganic materials 0.000 description 1
RQPZNWPYLFFXCP-UHFFFAOYSA-L barium dihydroxide Chemical compound [OH-].[OH-].[Ba+2] RQPZNWPYLFFXCP-UHFFFAOYSA-L 0.000 description 1
229910001863 barium hydroxide Inorganic materials 0.000 description 1
238000009835 boiling Methods 0.000 description 1
125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
239000003054 catalyst Substances 0.000 description 1
239000003153 chemical reaction reagent Substances 0.000 description 1
BULLHNJGPPOUOX-UHFFFAOYSA-N chloroacetone Chemical compound CC(=O)CCl BULLHNJGPPOUOX-UHFFFAOYSA-N 0.000 description 1
229910052804 chromium Inorganic materials 0.000 description 1
239000011651 chromium Substances 0.000 description 1
AHXGRMIPHCAXFP-UHFFFAOYSA-L chromyl dichloride Chemical compound Cl[Cr](Cl)(=O)=O AHXGRMIPHCAXFP-UHFFFAOYSA-L 0.000 description 1
239000004927 clay Substances 0.000 description 1
229940125904 compound 1 Drugs 0.000 description 1
229940125782 compound 2 Drugs 0.000 description 1
230000018044 dehydration Effects 0.000 description 1
238000006297 dehydration reaction Methods 0.000 description 1
239000003814 drug Substances 0.000 description 1
229940079593 drug Drugs 0.000 description 1
239000003995 emulsifying agent Substances 0.000 description 1
238000002474 experimental method Methods 0.000 description 1
125000000524 functional group Chemical group 0.000 description 1
230000000887 hydrating effect Effects 0.000 description 1
229910052739 hydrogen Inorganic materials 0.000 description 1
239000001257 hydrogen Substances 0.000 description 1
XLSMFKSTNGKWQX-UHFFFAOYSA-N hydroxyacetone Chemical compound CC(=O)CO XLSMFKSTNGKWQX-UHFFFAOYSA-N 0.000 description 1
239000000463 material Substances 0.000 description 1
239000003607 modifier Substances 0.000 description 1
JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
150000001451 organic peroxides Chemical class 0.000 description 1
238000006864 oxidative decomposition reaction Methods 0.000 description 1
JRKICGRDRMAZLK-UHFFFAOYSA-L persulfate group Chemical group S(=O)(=O)([O-])OOS(=O)(=O)[O-] JRKICGRDRMAZLK-UHFFFAOYSA-L 0.000 description 1
238000006116 polymerization reaction Methods 0.000 description 1
239000012286 potassium permanganate Substances 0.000 description 1
239000000843 powder Substances 0.000 description 1
239000012264 purified product Substances 0.000 description 1
230000009257 reactivity Effects 0.000 description 1
229920006395 saturated elastomer Polymers 0.000 description 1
229910052938 sodium sulfate Inorganic materials 0.000 description 1
235000011152 sodium sulphate Nutrition 0.000 description 1
235000010265 sodium sulphite Nutrition 0.000 description 1
239000007787 solid Substances 0.000 description 1
239000007858 starting material Substances 0.000 description 1
125000001424 substituent group Chemical group 0.000 description 1
230000002194 synthesizing effect Effects 0.000 description 1
229920003002 synthetic resin Polymers 0.000 description 1
239000000057 synthetic resin Substances 0.000 description 1
150000003509 tertiary alcohols Chemical class 0.000 description 1
LENZDBCJOHFCAS-UHFFFAOYSA-N tris Chemical compound OCC(N)(CO)CO LENZDBCJOHFCAS-UHFFFAOYSA-N 0.000 description 1
238000005292 vacuum distillation Methods 0.000 description 1
238000005406 washing Methods 0.000 description 1

Landscapes

Compositions Of Macromolecular Compounds (AREA)
Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

JP20241282A 1982-11-17 1982-11-17 アセトニルイソシアヌレ−トの製造法 Granted JPS5993064A (ja)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
JP20241282A JPS5993064A (ja)	1982-11-17	1982-11-17	アセトニルイソシアヌレ−トの製造法

Applications Claiming Priority (1)

Application Number	Priority Date	Filing Date	Title
JP20241282A JPS5993064A (ja)	1982-11-17	1982-11-17	アセトニルイソシアヌレ−トの製造法

Publications (2)

Publication Number	Publication Date
JPS5993064A JPS5993064A (ja)	1984-05-29
JPH0138787B2 true JPH0138787B2 (ko)	1989-08-16

Family

ID=16457072

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
JP20241282A Granted JPS5993064A (ja)	1982-11-17	1982-11-17	アセトニルイソシアヌレ−トの製造法

Country Status (1)

Country	Link
JP (1)	JPS5993064A (ko)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
DE3416564A1 (de) *	1982-12-16	1985-11-07	Aluminum Co Of America	Verfahren zur herstellung von silizium-aluminiumoxynitrid
JP3692659B2 (ja) *	1996-10-23	2005-09-07	日産化学工業株式会社	フラックス組成物
CN115536603B (zh) *	2022-10-19	2023-11-21	南通大学	一种有机中间体的制备方法

1982
- 1982-11-17 JP JP20241282A patent/JPS5993064A/ja active Granted

Also Published As

Publication number	Publication date
JPS5993064A (ja)	1984-05-29

Publication	Publication Date	Title
JP2694961B2 (ja)	1997-12-24	有機溶剤の痕跡を含まぬ高純度アルジトールジアセタールの製法
EP0150996A2 (en)	1985-08-07	Manufacture of heptanoic acid derivatives
JPH0138787B2 (ko)	1989-08-16
US4098806A (en)	1978-07-04	Process for functionalizing perfluorohalogenoalkanes
US4093667A (en)	1978-06-06	Preparation of 4-n-hexylresorcinol
DK166411B1 (da)	1993-05-17	Fremgangsmaade til fremstilling af 2,4-dichlor-5-fluor-benzoesyre
DE2161526A1 (de)	1972-06-22	Verfahren zur Herstellung von PoIybromphenylderivatmethacrylsäuree stern
US4061681A (en)	1977-12-06	Method for the preparation of mono- or poly [dialkyl or dicycloalkylphosphonylmethyl] aromatic carbocyclic compounds
US2962502A (en)	1960-11-29	Preparation of 2, 2'-bipyridyl
US3825572A (en)	1974-07-23	Epimeric mixtures of the lactone 3,6-dihydro-4,5-dimethyl-5-phenyl-alpha-pyrone
Becker	1969	Oxidative trimerization of 2, 4-diphenylphenol
US4925970A (en)	1990-05-15	Process for producing cyclohexadiene thioether
JP3801623B2 (ja)	2006-07-26	酸素含有の脂肪族化合物および４−ヒドロキシ−２，５−ジメチル−３（２ｈ）−フラノンの製造のための中間生成物としてのその使用
US4021443A (en)	1977-05-03	Perchlorodiazafulvene
US3046308A (en)	1962-07-24	O-allyl-n, n-diallylhydroxylamine and method of preparation
US3256340A (en)	1966-06-14	Condensation reactions in dimethyl sulfoxide solution and sulfoxides
US3109032A (en)	1963-10-29	Bis (dichlorovinyl) disulfides
JPS6116252B2 (ko)	1986-04-28
US2550439A (en)	1951-04-24	Production of unsaturated organic compounds
US5763624A (en)	1998-06-09	Process for the synthesis of 1-pyridiniumpropane-3-sulphonate
US3347941A (en)	1967-10-17	Triphenyl methane free radicals and their preparation
US4058567A (en)	1977-11-15	Cyclopentene sulfoxides
SU570592A1 (ru)	1977-08-30	Способ получени алкиловых эфиров пропаргилового спирта
US4052434A (en)	1977-10-04	Prostaglandin intermediates
US4028369A (en)	1977-06-07	Preparation of glycol (2-(p-chlorophenoxy)-2-methylpropionate)-2-nicotinate