JP7405141B2 - サマリウム鉄窒素系磁性材料 - Google Patents
サマリウム鉄窒素系磁性材料 Download PDFInfo
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- JP7405141B2 JP7405141B2 JP2021522251A JP2021522251A JP7405141B2 JP 7405141 B2 JP7405141 B2 JP 7405141B2 JP 2021522251 A JP2021522251 A JP 2021522251A JP 2021522251 A JP2021522251 A JP 2021522251A JP 7405141 B2 JP7405141 B2 JP 7405141B2
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- 239000000696 magnetic material Substances 0.000 title claims description 58
- PRQMIVBGRIUJHV-UHFFFAOYSA-N [N].[Fe].[Sm] Chemical compound [N].[Fe].[Sm] PRQMIVBGRIUJHV-UHFFFAOYSA-N 0.000 title claims description 23
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 15
- 239000013078 crystal Substances 0.000 claims description 14
- 229910052772 Samarium Inorganic materials 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 8
- 229910052742 iron Inorganic materials 0.000 claims description 5
- 229910052719 titanium Inorganic materials 0.000 claims description 3
- 229910052726 zirconium Inorganic materials 0.000 claims description 2
- 229910011208 Ti—N Inorganic materials 0.000 description 23
- 239000000843 powder Substances 0.000 description 13
- 239000010936 titanium Substances 0.000 description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 239000000203 mixture Substances 0.000 description 8
- 229910000859 α-Fe Inorganic materials 0.000 description 6
- 229910045601 alloy Inorganic materials 0.000 description 5
- 239000000956 alloy Substances 0.000 description 5
- 238000005121 nitriding Methods 0.000 description 5
- 238000010791 quenching Methods 0.000 description 5
- 239000012300 argon atmosphere Substances 0.000 description 4
- 238000010438 heat treatment Methods 0.000 description 4
- 238000001095 inductively coupled plasma mass spectrometry Methods 0.000 description 4
- 239000000463 material Substances 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 3
- 230000000052 comparative effect Effects 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 229910052761 rare earth metal Inorganic materials 0.000 description 3
- 150000002910 rare earth metals Chemical class 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- KZUNJOHGWZRPMI-UHFFFAOYSA-N samarium atom Chemical compound [Sm] KZUNJOHGWZRPMI-UHFFFAOYSA-N 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- 229910052804 chromium Inorganic materials 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000011156 evaluation Methods 0.000 description 2
- 229910052733 gallium Inorganic materials 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 2
- 229910052748 manganese Inorganic materials 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052750 molybdenum Inorganic materials 0.000 description 2
- 229910052758 niobium Inorganic materials 0.000 description 2
- 239000012299 nitrogen atmosphere Substances 0.000 description 2
- 238000000634 powder X-ray diffraction Methods 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 229910052720 vanadium Inorganic materials 0.000 description 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- YYXHRUSBEPGBCD-UHFFFAOYSA-N azanylidyneiron Chemical compound [N].[Fe] YYXHRUSBEPGBCD-UHFFFAOYSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 229910017052 cobalt Inorganic materials 0.000 description 1
- 239000010941 cobalt Substances 0.000 description 1
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000005347 demagnetization Effects 0.000 description 1
- 230000001747 exhibiting effect Effects 0.000 description 1
- 230000004907 flux Effects 0.000 description 1
- 229910052735 hafnium Inorganic materials 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 230000002427 irreversible effect Effects 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 150000004767 nitrides Chemical class 0.000 description 1
- 230000000171 quenching effect Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
- B22F1/14—Treatment of metallic powder
- B22F1/145—Chemical treatment, e.g. passivation or decarburisation
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
- H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
- H01F1/047—Alloys characterised by their composition
- H01F1/053—Alloys characterised by their composition containing rare earth metals
- H01F1/055—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
- H01F1/059—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and Va elements, e.g. Sm2Fe17N2
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/001—Ferrous alloys, e.g. steel alloys containing N
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/005—Ferrous alloys, e.g. steel alloys containing rare earths, i.e. Sc, Y, Lanthanides
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/10—Ferrous alloys, e.g. steel alloys containing cobalt
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C38/00—Ferrous alloys, e.g. steel alloys
- C22C38/14—Ferrous alloys, e.g. steel alloys containing titanium or zirconium
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01F—MAGNETS; INDUCTANCES; TRANSFORMERS; SELECTION OF MATERIALS FOR THEIR MAGNETIC PROPERTIES
- H01F1/00—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties
- H01F1/01—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials
- H01F1/03—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity
- H01F1/032—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials
- H01F1/04—Magnets or magnetic bodies characterised by the magnetic materials therefor; Selection of materials for their magnetic properties of inorganic materials characterised by their coercivity of hard-magnetic materials metals or alloys
- H01F1/047—Alloys characterised by their composition
- H01F1/053—Alloys characterised by their composition containing rare earth metals
- H01F1/055—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5
- H01F1/059—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and Va elements, e.g. Sm2Fe17N2
- H01F1/0596—Alloys characterised by their composition containing rare earth metals and magnetic transition metals, e.g. SmCo5 and Va elements, e.g. Sm2Fe17N2 of rhombic or rhombohedral Th2Zn17 structure or hexagonal Th2Ni17 structure
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2998/00—Supplementary information concerning processes or compositions relating to powder metallurgy
- B22F2998/10—Processes characterised by the sequence of their steps
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B22—CASTING; POWDER METALLURGY
- B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
- B22F2999/00—Aspects linked to processes or compositions used in powder metallurgy
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C2202/00—Physical properties
- C22C2202/02—Magnetic
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Power Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Hard Magnetic Materials (AREA)
Description
Tiを更に含み、かつ、
2.5原子%以下の含有量でCoを更に含む、またはCoを含まない、
サマリウム鉄窒素系磁性材料が提供される。
表1に示す組成のうち、Nを除く原料金属を該組成に対応する割合で混合し、高周波誘導加熱炉にて溶解させて母合金を準備した。
この母合金を、アルゴン雰囲気下にて、溶解させて、周速度30~100m/sで回転するMoロール上に噴射し、これにより超急冷して薄帯を得た。
この薄帯を粉砕して、最大粒径32μm以下の粉末を得た(目開き32μmのふるいを使用してふるい分けした)。
得られた粉末を、アルゴン雰囲気下にて、725~825℃にて3~30分間の熱処理に付した。
次いで、熱処理後の粉末を、窒素雰囲気下にて、460℃にて8時間の熱処理に付して窒化させた。
窒化後の粉末として、Sm-Fe-Co-Ti-N系磁性材料の試料を得た。
上記で得られた試料の組成を誘導結合プラズマ質量分析(ICP-MS)により分析した。
また、上記で得られた試料の磁気特性を評価した。評価に際して、試料(粉末)の真密度は7.6g/cm3とし、反磁界補正は行わず、振動試料型磁力計(VSM)により、保磁力Hcj、残留磁束密度Brおよび最大エネルギー積(BH)maxを測定した。
これらの結果を表1に示す。
なお、上記で得られた試料を粉末X線回折により調べたところ、いずれの試料も、TbCu7型構造および/またはTh2Zn17型構造を有する結晶相を含み、更に、α-Fe相を含んでいることが確認された。
Claims (7)
- Sm、FeおよびNを含むサマリウム鉄窒素系磁性材料であって、
Tiを更に含み、かつ、
2.5原子%以下の含有量でCoを更に含む、またはCoを含まず、
前記Nの含有量が14.0原子%以上16原子%以下であり、
前記Tiの含有量が1.1原子%以上1.5原子%以下であり、
Sm、Fe、Co、TiおよびNの合計の含有量が98.0原子%以上100原子%以下であり、
サマリウム鉄窒素系磁性材料(但し、Bを含む場合およびSiを含む場合を除く)。 - 前記Smの含有量が、7原子%以上10原子%以下であり、
前記Feの含有量が、65原子%以上80原子%以下であり、
前記Nの含有量が、14.0原子%以上16原子%以下であり、
前記含有量の合計が、100原子%を超えない、請求項1に記載のサマリウム鉄窒素系磁性材料。 - Zrを更に含む、請求項1または2に記載のサマリウム鉄窒素系磁性材料。
- 前記Zrの含有量が、0.5原子%以上1.5原子%以下である、請求項3に記載のサマリウム鉄窒素系磁性材料。
- 前記Smの含有量が、8.0原子%以上9.5原子%以下である、請求項1~4のいずれかに記載のサマリウム鉄窒素系磁性材料。
- 前記Coの含有量が、1原子%以上2.5原子%以下である、請求項1~5のいずれかに記載のサマリウム鉄窒素系磁性材料。
- TbCu7型および/またはTh2Zn17型構造を有する結晶相を含む、請求項1~6のいずれかに記載のサマリウム鉄窒素系磁性材料。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2019102696 | 2019-05-31 | ||
JP2019102696 | 2019-05-31 | ||
PCT/JP2020/019787 WO2020241380A1 (ja) | 2019-05-31 | 2020-05-19 | サマリウム鉄窒素系磁性材料 |
Publications (3)
Publication Number | Publication Date |
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JPWO2020241380A1 JPWO2020241380A1 (ja) | 2020-12-03 |
JPWO2020241380A5 JPWO2020241380A5 (ja) | 2022-03-08 |
JP7405141B2 true JP7405141B2 (ja) | 2023-12-26 |
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Country Status (5)
Country | Link |
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US (1) | US20220076865A1 (ja) |
EP (1) | EP3978164A4 (ja) |
JP (1) | JP7405141B2 (ja) |
CN (1) | CN114008728A (ja) |
WO (1) | WO2020241380A1 (ja) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN114561524B (zh) * | 2021-11-19 | 2022-10-21 | 杭州永磁集团有限公司 | 一种钐铁合金提高2:17型相含量的热处理方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1072796A (zh) | 1991-11-26 | 1993-06-02 | 北京三环新材料高技术公司 | 一种新型粘结型铁基稀土永磁体及其制造方法 |
JP2000049006A (ja) | 1998-05-26 | 2000-02-18 | Hitachi Metals Ltd | 希土類磁石材料およびそれを用いた希土類ボンド磁石 |
JP2000340422A (ja) | 1999-03-24 | 2000-12-08 | Hitachi Metals Kiko Co Ltd | マグネットロール |
JP2002057017A (ja) | 2000-05-29 | 2002-02-22 | Daido Steel Co Ltd | 等方性の粉末磁石材料、その製造方法およびボンド磁石 |
JP2013531359A (ja) | 2010-03-29 | 2013-08-01 | グリレム アドバンスド マテリアルズ カンパニー リミティッド | 希土類永久磁石粉、ボンド磁石およびボンド磁石で作られた装置 |
Family Cites Families (12)
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US5684076A (en) * | 1994-12-16 | 1997-11-04 | Matsushita Electric Industrial Co., Ltd. | Rare earth-iron-nitrogen based magnetic material and method of manufacturing the same |
JPH0913151A (ja) * | 1994-12-16 | 1997-01-14 | Matsushita Electric Ind Co Ltd | 希土類−鉄−窒素系磁性材料及びその製造方法 |
JPH091315A (ja) * | 1995-04-12 | 1997-01-07 | Asahi Tec Corp | 車両用ホイールの鋳造方法 |
JPH10241923A (ja) * | 1997-02-21 | 1998-09-11 | Hitachi Metals Ltd | 希土類磁石材料およびその製造方法ならびにそれを用いた希土類ボンド磁石 |
JP3469496B2 (ja) * | 1998-03-27 | 2003-11-25 | 株式会社東芝 | 磁石材料の製造方法 |
US6290782B1 (en) * | 1998-03-27 | 2001-09-18 | Kabushiki Kaisha Toshiba | Magnetic material and manufacturing method thereof, and bonded magnet using the same |
JPH11297518A (ja) * | 1998-04-13 | 1999-10-29 | Hitachi Metals Ltd | 希土類磁石材料 |
DE19981167T1 (de) * | 1998-05-26 | 2000-08-10 | Hitachi Metals Ltd | Seltenerd-Magnetmaterialien vom Nitrid-Typ und daraus gebildete Verbundmagnete |
CN1315679A (zh) * | 2000-03-24 | 2001-10-03 | 日立金属株式会社 | 磁辊 |
TW503409B (en) * | 2000-05-29 | 2002-09-21 | Daido Steel Co Ltd | Isotropic powdery magnet material, process for preparing and resin-bonded magnet |
CN108630371B (zh) | 2017-03-17 | 2020-03-27 | 有研稀土新材料股份有限公司 | 一种高热稳定性的稀土永磁材料、其制备方法及含有其的磁体 |
JP7040928B2 (ja) | 2017-12-05 | 2022-03-23 | Fdk株式会社 | インダクタ |
-
2020
- 2020-05-19 CN CN202080039894.9A patent/CN114008728A/zh active Pending
- 2020-05-19 WO PCT/JP2020/019787 patent/WO2020241380A1/ja unknown
- 2020-05-19 JP JP2021522251A patent/JP7405141B2/ja active Active
- 2020-05-19 EP EP20814089.7A patent/EP3978164A4/en active Pending
-
2021
- 2021-11-19 US US17/530,735 patent/US20220076865A1/en active Pending
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN1072796A (zh) | 1991-11-26 | 1993-06-02 | 北京三环新材料高技术公司 | 一种新型粘结型铁基稀土永磁体及其制造方法 |
JP2000049006A (ja) | 1998-05-26 | 2000-02-18 | Hitachi Metals Ltd | 希土類磁石材料およびそれを用いた希土類ボンド磁石 |
JP2000340422A (ja) | 1999-03-24 | 2000-12-08 | Hitachi Metals Kiko Co Ltd | マグネットロール |
JP2002057017A (ja) | 2000-05-29 | 2002-02-22 | Daido Steel Co Ltd | 等方性の粉末磁石材料、その製造方法およびボンド磁石 |
JP2013531359A (ja) | 2010-03-29 | 2013-08-01 | グリレム アドバンスド マテリアルズ カンパニー リミティッド | 希土類永久磁石粉、ボンド磁石およびボンド磁石で作られた装置 |
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CN114008728A (zh) | 2022-02-01 |
EP3978164A1 (en) | 2022-04-06 |
WO2020241380A1 (ja) | 2020-12-03 |
US20220076865A1 (en) | 2022-03-10 |
JPWO2020241380A1 (ja) | 2020-12-03 |
EP3978164A4 (en) | 2023-01-18 |
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