EP1311453B1 - Bec de remplissage a jet en parapluie et machine de remplissage munie d'un tel bec - Google Patents
Bec de remplissage a jet en parapluie et machine de remplissage munie d'un tel bec Download PDFInfo
- Publication number
- EP1311453B1 EP1311453B1 EP01956619A EP01956619A EP1311453B1 EP 1311453 B1 EP1311453 B1 EP 1311453B1 EP 01956619 A EP01956619 A EP 01956619A EP 01956619 A EP01956619 A EP 01956619A EP 1311453 B1 EP1311453 B1 EP 1311453B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- product
- filling device
- filling
- shaped jet
- annular
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Images
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
- B67C3/28—Flow-control devices, e.g. using valves
- B67C3/281—Profiled valve bodies for smoothing the flow at the outlet of the filling nozzle
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
- B67C3/26—Filling-heads; Means for engaging filling-heads with bottle necks
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
- B67C3/26—Filling-heads; Means for engaging filling-heads with bottle necks
- B67C2003/2602—Details of vent-tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
- B67C3/26—Filling-heads; Means for engaging filling-heads with bottle necks
- B67C2003/2671—Means for preventing foaming of the liquid
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B67—OPENING, CLOSING OR CLEANING BOTTLES, JARS OR SIMILAR CONTAINERS; LIQUID HANDLING
- B67C—CLEANING, FILLING WITH LIQUIDS OR SEMILIQUIDS, OR EMPTYING, OF BOTTLES, JARS, CANS, CASKS, BARRELS, OR SIMILAR CONTAINERS, NOT OTHERWISE PROVIDED FOR; FUNNELS
- B67C3/00—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus; Filling casks or barrels with liquids or semiliquids
- B67C3/02—Bottling liquids or semiliquids; Filling jars or cans with liquids or semiliquids using bottling or like apparatus
- B67C3/22—Details
- B67C3/26—Filling-heads; Means for engaging filling-heads with bottle necks
- B67C2003/2688—Means for filling containers in defined atmospheric conditions
Definitions
- the invention relates to the field of filling spouts, especially those intended for bottle filling machines.
- the invention therefore aims to propose a new design a filling spout which, while retaining the qualities specific to spouts described above, also makes it possible to greatly limit or even eliminate contact of bottled product with air.
- the invention proposes a filling spout for dispense a liquid in a container, of the type in which the spout contains a liquid distribution orifice which conditions an umbrella jet, and of the type in which the spout comprises an axial cannula provided with a conduit gas outlet which opens into the space delimited by the umbrella spray, characterized in that the cannula has a pipe gas inlet which opens into the space delimited by the jet in an umbrella and which projects a gas flow which essentially flows in parallel to the umbrella jet of the liquid, on the internal side thereof.
- the invention also relates to a machine for filling containers, characterized in that it comprises at least one filling station fitted with a filling spout incorporating any of the previous features.
- the filling spout 10 illustrated in the figures is more particularly intended for filling bottles 12 with narrow necks. he could for example be used as well for glass bottles as for plastic bottles such as polyethylene terephthalate (PET). Of course such a spout will preferably be used for the manufacture of multi-nozzle filling machines, for example of the rotary carousel type,
- the spout 10 illustrated in the figures essentially comprises a body main 14 hollow, substantially of axis A1, which is crossed axially right through by two coaxial tubes: an internal tube 16 and an outer tube 18.
- the main body 14 therefore delimits an internal volume which is axially traversed by the tubes 16, 18.
- the main body 14, which is here shown in one piece, can also be made in several pieces to facilitate manufacturing. It is capped by an upper cover 20 which seals the internal volume upwards and which supports tubes 16, 18.
- the cover 20 has a stepped internal bore which passes through it axially right through.
- the upper stage 22 of the bore which opens upwards towards the outside of the main body, is cylindrical of axis A1, substantially the same diameter as the external diameter of the tube internal 16.
- the lower stage 24, which opens down into the volume internal, is cylindrical with axis A1, substantially the same diameter as the outer diameter of the outer tube 18.
- the intermediate stage 26, which extends axially between the stages upper 22 and lower 24, is cylindrical with axis A1, substantially of same diameter as the internal diameter of the outer tube 18.
- the upper end of the outer tube 18 is axially engaged with the bottom up in the bottom stage 26 of the cover bore, up to bear against an annular abutment surface which delimits the lower stage 24 of the intermediate stage 26.
- the tube 18 is mounted with tightening and with the presence of an O-ring so as to ensure the attachment of the outer tube 18 to the cover 20, and the other the tightness of this assembly.
- the inner tube 16 is engaged, axially in the center of the outer tube 18, so as to pass entirely through the cover 20.
- the internal tube 20 is held tightly through the upper stage 22 of the bore of the cover, which again ensures the fixing of the internal tube 16.
- the inside diameter of the tube outer 18 is greater than the outer diameter of the inner tube 16 of such so that, when they are mounted coaxially on the cover 20, it between the two tubes 16, 18 remains an annular space which forms a pipe 28.
- the end upper part of this pipe 28, which is formed by the stage intermediate 26 of the bore of the cover 20, is closed due to the tight fitting of the inner tube 16 in the upper stage 22 of the bore.
- an inlet port 30 passes radially through the cover to open into the intermediate stage 24 of the bore and thus allow the communication of the pipe 28 with a source of fluid.
- the internal volume delimited by the main body 14 comprises essentially three parts: an upper rotation chamber 32, an acceleration cone 34, and an annular distribution channel 36.
- the rotation chamber 32 here has a simple ring shape arranged around the outer tube 18.
- a power inlet 38 allows introduce the product to be bottled into chamber 32 according to a orientation which is not purely radial but which, on the contrary, presents a tangential component.
- the product is introduced into the chamber with a certain pressure, the product is entrained in a spiral circulation in the room, even in case this pressure comes only from the gravity flow of the product.
- the annular distribution channel 36 through which the product to bottle flows to container 12, is formed around the part bottom of the outer tube 18. In the illustrated embodiment, it is provided that this part of the spout 10 penetrates inside the neck of the container to fill, so that the channel 36 has a smaller diameter than that of the rest of main body 14.
- Channel 36 is delimited by an element of tubular cylindrical wall.
- a connection surface 34 is provided which, for simplicity, was chosen tapered.
- the internal shapes of the main body 14 of the spout 10 can be optimized, for example as illustrated in the document US-A-5,125,441, without departing from the teaching of the invention.
- the lower end of the tube external 18 descends below the level of the lower end of the channel 36, thus delimiting an orifice 40 for the outlet of the product which is annular.
- the lower end of the outer tube 18 flares radially outward so that the outer surface of the tube external thus forms a deflector 44 which tends to project the product radially outwards so that it comes into contact with the internal wall of the container by forming an umbrella spray.
- the dimensions and the respective position of the end of the tube external 18 and the end of channel 36 are chosen so that the passage section of the outlet orifice 40 is relatively small, this in order to be able to retain the liquid contained in the spout when feeding product is cut.
- the maximum acceptable cross-section for preventing the product from dripping is determined in particular according to the intrinsic surface tension of the product.
- the lower end of the inner tube 16 protrudes axially below that of the outer tube 18 and the surface the end of the inner tube 16 flares radially towards the outside to form a deflection surface 46.
- the lower end of the pipe 28 is therefore annular and widens radially towards outside.
- the power input 38 of the chamber 32 is connected to a storage tank for the product to be bottled, with interposition of a controlled valve. Opening and closing the valve can be ordered according to different parameters. It can be a time control which determines a fixed filling time which will be applied to all containers.
- the command can be of type by weight, product dispensing being interrupted when the container has reached a predetermined weight. It can still be an order flow meter into which the value of the flow delivered by the nozzle is integrated to get an estimate of the volume of product spilled in the container. In the case of a volumetric machine, the quantity of product to be dispensed will be dosed in an intermediate volume placed between the storage tank and the filling spout.
- the inlet port 30 of the gas supply line 28 will be preferably connected to a neutral gas source for the product under consideration.
- This neutral gas could for example be carbon dioxide (CO2) or nitrogen (N2).
- central duct 42 delimited inside the central tube 16 will be connected to a gas evacuation device or simply to air free.
- the flow of product which is injected into the body of the spout is therefore rotated in chamber 32, which, in combination with the annular shape of the outlet port 40 and with the shape of the deflection surface 44, ensures that the product is distributed by the spout in the form of an umbrella spray.
- the lower part of the beak being engaged in the container or being in the immediate vicinity thereof, the product then comes into contact with the internal wall of the container and the along it to fill the container. We obtain a flow which creates very little foam, even at high flow rates.
- the line 28 is supplied with a neutral gas so that the flow of gas that flows through the lower end of the pipe 28 opens "below” the umbrella flow of product. Due to the flared shape of the detection surface 46, the flow gas flows substantially parallel to the product flow in the bottle.
- the product flow is found in some sort trapped between, on the outside, the wall of the container, and on the side internal, the neutral gas flow. In this way, the contact of the product with the air ambient is very limited, even canceled.
- the exhaust duct 42 allows the gases to escape from the container as the level of product in the container increases. This exhaust is preferably done by the center of the container, up along the axis A1. Evacuated gases can either be part of the gas initially contained in the container before filling, i.e. part of the neutral gas supplied by the pipeline 36.
- the spout according to the invention it is also possible to prolong the injection of neutral gas beyond the time required to fill the product, this in order to perfect the scanning of the head space of the container with a gas neutral to avoid trapping air in the bottle, so on contact of the product, when the bottle is capped.
Landscapes
- Filling Of Jars Or Cans And Processes For Cleaning And Sealing Jars (AREA)
- Basic Packing Technique (AREA)
- Containers And Plastic Fillers For Packaging (AREA)
- Nozzles (AREA)
- Catching Or Destruction (AREA)
- Supply Of Fluid Materials To The Packaging Location (AREA)
- Containers And Packaging Bodies Having A Special Means To Remove Contents (AREA)
- Confectionery (AREA)
Description
- la canalisation d'amenée de gaz débouche à l'intérieur de l'espace délimité par le jet en parapluie sous la forme d'une ouverture annulaire ;
- au niveau de son extrémité débouchante, la canalisation d'amenée de gaz comporte une surface de déflexion sensiblement conique ;
- le conduit d'évacuation débouche axialement au centre de l'ouverture annulaire de la canalisation d'amenée de gaz, laquelle débouche axialement au centre de l'orifice de distribution de produit qui est sensiblement annulaire ;
- la canalisation d'amenée de gaz est alimentée avec un gaz neutre vis-à-vis du produit à distribuer ;
- le jet de produit présente une composante de rotation axiale ;
- le bec comporte une chambre annulaire de mise en rotation dans laquelle le produit est injecté avec une composante de vitesse tangentielle, la chambre de mise en rotation étant prolongée axialement par un canal annulaire dont l'extrémité débouchante forme l'orifice de distribution de produit ;
- la chambre de mise en rotation est raccordée au canal annulaire par une surface en entonnoir ;
- la canule axiale traverse axialement la chambre de mise en rotation ;
- la figure 1 est une vue schématique en coupe axiale d'un bec de remplissage conforme aux enseignements de l'invention, le bec étant illustré en fonctionnement au cours du remplissage d'une bouteille ;
- la figure 2 est une vue à échelle réduite en coupe transversale selon la ligne 2-2 de la figure 1.
Claims (10)
- Bec de remplissage pour distribuer un liquide dans un récipient, du type dans lequel le bec (10) comporte un orifice de distribution (36, 40) du liquide qui conditionne un jet en parapluie, et du type dans lequel le bec comporte une canule axiale munie d'un conduit d'évacuation (42) de gaz qui débouche à l'intérieur de l'espace délimité par le jet en parapluie,
caractérisé en ce que la canule comporte une canalisation (28) d'amenée de gaz qui débouche à l'intérieur de l'espace délimité par le jet en parapluie et qui projette un flux de gaz qui s'écoule essentiellement en parallèle au jet en parapluie du liquide, du côté interne de celui-ci. - Bec de remplissage selon la revendication 1, caractérisé en ce que la canalisation d'amenée de gaz (28) débouche à l'intérieur de l'espace délimité par le jet en parapluie sous la forme d'une ouverture annulaire.
- Bec de remplissage selon la revendication 2, caractérisé en ce que, au niveau de son extrémité débouchante, la canalisation (28) d'amenée de gaz comporte une surface de déflexion (46) sensiblement conique.
- Bec de remplissage selon l'une des revendications 2 ou 3, caractérisé en ce que le conduit d'évacuation (42) débouche axialement au centre de l'ouverture annulaire de la canalisation d'amenée de gaz (28), laquelle débouche axialement au centre de l'orifice de distribution (36, 40) de produit qui est sensiblement annulaire.
- Bec de remplissage selon l'une quelconque des revendications précédentes, caractérisé en ce que la canalisation d'amenée de gaz est alimentée avec un gaz neutre vis-à-vis du produit à distribuer.
- Bec de remplissage selon l'une quelconque des revendications précédentes, caractérisé en ce que le jet de produit présente une composante de rotation axiale.
- Bec de remplissage selon la revendication 6, caractérisé en ce qu'il comporte une chambre annulaire (32) de mise en rotation dans laquelle le produit est injecté (38) avec une composante de vitesse tangentielle, la chambre de mise en rotation (32) étant prolongée axialement par un canal annulaire (36) dont l'extrémité débouchante forme l'orifice (40) de distribution de produit.
- Bec de remplissage selon la revendication 7, caractérisé en ce que la chambre de mise en rotation (32) est raccordée au canal annulaire (36) par une surface en entonnoir (34).
- Bec de remplissage selon la revendication 7, caractérisé en ce que la canule axiale (16, 18) traverse axialement la chambre de mise en rotation (32).
- Machine de remplissage de récipients, caractérisée en ce qu'elle comporte au moins un poste de remplissage muni d'un bec de remplissage conforme à l'une quelconque des revendications précédentes.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR0010642 | 2000-08-16 | ||
FR0010642A FR2813071B1 (fr) | 2000-08-16 | 2000-08-16 | Bec de remplissage a jet en parapluie et machine de remplissage munie d'un tel bec |
PCT/FR2001/002366 WO2002014207A1 (fr) | 2000-08-16 | 2001-07-20 | Bec de remplissage a jet en parapluie et machine de remplissage munie d'un tel bec |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1311453A1 EP1311453A1 (fr) | 2003-05-21 |
EP1311453B1 true EP1311453B1 (fr) | 2004-01-28 |
Family
ID=8853543
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP01956619A Expired - Lifetime EP1311453B1 (fr) | 2000-08-16 | 2001-07-20 | Bec de remplissage a jet en parapluie et machine de remplissage munie d'un tel bec |
Country Status (14)
Country | Link |
---|---|
EP (1) | EP1311453B1 (fr) |
JP (1) | JP3696592B2 (fr) |
KR (1) | KR100509091B1 (fr) |
CN (1) | CN1220620C (fr) |
AT (1) | ATE258536T1 (fr) |
AU (1) | AU2001278547A1 (fr) |
BR (1) | BR0113227B1 (fr) |
CA (1) | CA2416556C (fr) |
DE (1) | DE60101916T2 (fr) |
ES (1) | ES2215143T3 (fr) |
FR (1) | FR2813071B1 (fr) |
MX (1) | MXPA03000911A (fr) |
PT (1) | PT1311453E (fr) |
WO (1) | WO2002014207A1 (fr) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
ATE492506T1 (de) * | 2005-07-28 | 2011-01-15 | Sidel Participations | Füllventil mit einer flüssigkeitskammer, gaskammer und mediumkammer sowie dieses umfassende füllmaschine |
DE102006017706A1 (de) * | 2006-04-15 | 2007-10-25 | Khs Ag | Füllelemente sowie Füllmaschine mit einem Füllelement |
FR2911594B1 (fr) * | 2007-01-22 | 2009-04-03 | Sidel Participations | Machine de remplissage equipee d'un dispositif de nettoyage avec membrane deformable |
JP5029249B2 (ja) * | 2007-09-25 | 2012-09-19 | シブヤマシナリー株式会社 | 充填装置 |
DE102008030721A1 (de) * | 2008-07-01 | 2010-01-07 | Krones Ag | Vorrichtung zum Abfüllen von zähfließenden Medien |
BRPI0823401A2 (pt) * | 2008-12-29 | 2015-06-16 | Sidel Spa | Válvula e máquina de enchimento. |
CN103112813A (zh) * | 2013-01-25 | 2013-05-22 | 南京保立隆包装机械有限公司 | 一种含果粒易拉罐饮料的灌装阀 |
DE102013110774A1 (de) | 2013-09-30 | 2015-04-02 | Sig Technology Ag | Vorrichtung zur Veränderung der Strahlform von fließfähigen Produkten |
ITPR20130105A1 (it) * | 2013-12-27 | 2015-06-28 | Gea Procomac Spa | Dispositivo di riempimento di un recipiente e macchina di riempimento |
CN104016285A (zh) * | 2014-05-27 | 2014-09-03 | 苏州柏德纳科技有限公司 | 防气泡双管式液体灌装装置 |
KR20180047930A (ko) * | 2016-11-02 | 2018-05-10 | 엔피씨(주) | 하부주입 어댑터 |
KR101896397B1 (ko) * | 2016-11-04 | 2018-09-11 | 엔피씨(주) | 하부주입 어댑터 |
CN108264008A (zh) * | 2018-03-09 | 2018-07-10 | 惠州市环发环保科技有限公司 | 包装油漆升降管 |
CN111268623B (zh) * | 2020-04-08 | 2021-09-24 | 东阿县御颜堂阿胶制品有限公司 | 一种高效的真空灌装机 |
CN111844692A (zh) * | 2020-07-29 | 2020-10-30 | 山东新华医疗器械股份有限公司 | 一种塑料瓶连续生产灌装设备 |
CN113697747B (zh) * | 2021-09-17 | 2023-01-03 | 苏州凌耀制药设备有限公司 | 一种液态药剂灌装方法及其设备 |
Family Cites Families (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4156444A (en) * | 1977-11-14 | 1979-05-29 | Manfred Mette | Filling device for the bottling of carbonated beverages |
DE4012849A1 (de) * | 1990-04-23 | 1991-10-24 | Alfill Getraenketechnik | Vorrichtung zum fuellen von behaeltern mit einer fluessigkeit |
-
2000
- 2000-08-16 FR FR0010642A patent/FR2813071B1/fr not_active Expired - Fee Related
-
2001
- 2001-07-20 BR BRPI0113227-0A patent/BR0113227B1/pt not_active IP Right Cessation
- 2001-07-20 JP JP2002519311A patent/JP3696592B2/ja not_active Expired - Fee Related
- 2001-07-20 PT PT01956619T patent/PT1311453E/pt unknown
- 2001-07-20 MX MXPA03000911A patent/MXPA03000911A/es active IP Right Grant
- 2001-07-20 KR KR10-2003-7001340A patent/KR100509091B1/ko not_active IP Right Cessation
- 2001-07-20 EP EP01956619A patent/EP1311453B1/fr not_active Expired - Lifetime
- 2001-07-20 WO PCT/FR2001/002366 patent/WO2002014207A1/fr active IP Right Grant
- 2001-07-20 CN CNB018142028A patent/CN1220620C/zh not_active Expired - Fee Related
- 2001-07-20 CA CA002416556A patent/CA2416556C/fr not_active Expired - Fee Related
- 2001-07-20 ES ES01956619T patent/ES2215143T3/es not_active Expired - Lifetime
- 2001-07-20 AU AU2001278547A patent/AU2001278547A1/en not_active Abandoned
- 2001-07-20 DE DE60101916T patent/DE60101916T2/de not_active Expired - Lifetime
- 2001-07-20 AT AT01956619T patent/ATE258536T1/de not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
WO2002014207A9 (fr) | 2003-09-12 |
ES2215143T3 (es) | 2004-10-01 |
JP2004524221A (ja) | 2004-08-12 |
DE60101916D1 (de) | 2004-03-04 |
FR2813071A1 (fr) | 2002-02-22 |
KR100509091B1 (ko) | 2005-08-18 |
PT1311453E (pt) | 2004-06-30 |
CN1220620C (zh) | 2005-09-28 |
CA2416556A1 (fr) | 2002-02-21 |
WO2002014207A1 (fr) | 2002-02-21 |
DE60101916T2 (de) | 2004-10-28 |
MXPA03000911A (es) | 2003-09-05 |
EP1311453A1 (fr) | 2003-05-21 |
CN1447774A (zh) | 2003-10-08 |
KR20030037270A (ko) | 2003-05-12 |
FR2813071B1 (fr) | 2002-10-25 |
BR0113227B1 (pt) | 2011-05-03 |
ATE258536T1 (de) | 2004-02-15 |
CA2416556C (fr) | 2007-04-03 |
JP3696592B2 (ja) | 2005-09-21 |
BR0113227A (pt) | 2003-07-08 |
AU2001278547A1 (en) | 2002-02-25 |
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