EP0728298B1 - Verfahren zum erzeugen wenigstens einer ausnehmung in einer oberfläche eines substrats als formbett für eine membran durch trockenätzen - Google Patents
Verfahren zum erzeugen wenigstens einer ausnehmung in einer oberfläche eines substrats als formbett für eine membran durch trockenätzen Download PDFInfo
- Publication number
- EP0728298B1 EP0728298B1 EP94931495A EP94931495A EP0728298B1 EP 0728298 B1 EP0728298 B1 EP 0728298B1 EP 94931495 A EP94931495 A EP 94931495A EP 94931495 A EP94931495 A EP 94931495A EP 0728298 B1 EP0728298 B1 EP 0728298B1
- Authority
- EP
- European Patent Office
- Prior art keywords
- substrate
- recess
- etching
- opening
- screening device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
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Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L19/00—Details of, or accessories for, apparatus for measuring steady or quasi-steady pressure of a fluent medium insofar as such details or accessories are not special to particular types of pressure gauges
- G01L19/06—Means for preventing overload or deleterious influence of the measured medium on the measuring device or vice versa
- G01L19/0618—Overload protection
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01L—MEASURING FORCE, STRESS, TORQUE, WORK, MECHANICAL POWER, MECHANICAL EFFICIENCY, OR FLUID PRESSURE
- G01L9/00—Measuring steady of quasi-steady pressure of fluid or fluent solid material by electric or magnetic pressure-sensitive elements; Transmitting or indicating the displacement of mechanical pressure-sensitive elements, used to measure the steady or quasi-steady pressure of a fluid or fluent solid material, by electric or magnetic means
- G01L9/0041—Transmitting or indicating the displacement of flexible diaphragms
- G01L9/0042—Constructional details associated with semiconductive diaphragm sensors, e.g. etching, or constructional details of non-semiconductive diaphragms
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S438/00—Semiconductor device manufacturing: process
- Y10S438/942—Masking
- Y10S438/944—Shadow
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S438/00—Semiconductor device manufacturing: process
- Y10S438/977—Thinning or removal of substrate
Definitions
- the invention relates to a method for generating a Form beds for a membrane.
- Membranes are used in many technical fields. An important area of application is sensor technology, in which the deflection or vibration of a membrane for measurement a physical quantity is used. Examples of this are the pressure sensors mostly made in silicon or also sound sensors. In all applications is too note that the membrane due to excessive impact or The effects of pressure in the event of overload can be destroyed. This is particularly the case if the membrane consists of a relatively brittle material such as silicon. For overload protection the membrane is usually a shaped bed provided to which the membrane is in the event of an overload can put on.
- the (100) surface of a silicon substrate by anisotropic wet etching with Potash lye (KOH) has a recess with a trapezoidal shape Profile created.
- KOH Potash lye
- a second way of producing such shaped beds consists of several, executed one after the other Lithography steps with photoresist masks increasing Diameter in a recess with a stepped profile to produce a silicon substrate.
- the lithography steps can be the profile of the recess be approximated to a smooth course (WO 90/04701, in particular FIG. 3).
- levels always remain which are problematic because of their notch effect.
- a mold bed can also be produced with gray area lithography will.
- This third procedure is for the substrate needs a mask with a gray area that becomes lighter towards the center of the desired recess. In lithography, this is done under suitable exposure conditions a lacquer profile with decreasing towards the center Thickness. During the subsequent etching of the substrate the paint mask retreats and gives more and more substrate surfaces free.
- a disadvantage of this manufacturing process is that the retraction of the paint mask at best up to a size of 10 to 20 ⁇ m leaves. The method is therefore not applicable if the diameter of the shaped bed should be much larger than its depth.
- a fourth way to make the mold bed is mechanical processing of the substrate by turning, Milling, grinding, polishing or blasting.
- the precision this method is inadequate for profile depths of a few ⁇ m.
- etching processes are known which are referred to as dry etching.
- the characteristic feature of such dry etching processes is the chemical reaction of radicals or ions of an etching gas with the substrate surface to form a volatile reaction product.
- the chemical reaction can be spontaneous, ion-, electron- or photon-induced.
- the etching gas radicals are generally generated in a low-pressure plasma, typically between 10 -1 and 10 3 Pa. In these cases, reactive dry etching is therefore often referred to as plasma etching.
- the plasma can be generated by an electromagnetic high-frequency field, which is either applied to electrodes or supplied directly as microwaves.
- Several types of plasma reactors are known for carrying out the dry etching process.
- All types have a recipient in which the substrate to be etched is arranged and which is provided with connections for evacuating and supplying the etching gas.
- a hollow cylindrical, perforated shield is provided within a housing, which preferably consists of quartz, which forms a tunnel.
- the shield is surrounded by electrodes which are approximately semicircular in cross section. An electromagnetic high-frequency field is applied to the electrodes with the aid of a high-frequency generator.
- the substrate to be etched is arranged on the so-called boat within the shield. The shielding ensures that no charged particles (electrons, ions) reach the substrate.
- the substrate is arranged on the flat surface of an electrode arranged in the recipient.
- the electrode with the substrate can now be grounded and a further flat electrode can be arranged parallel to the electrode with the substrate in the recipient, which is electrically connected to the high-frequency generator.
- the electrode with the substrate itself is connected to the high-frequency generator and the second electrode is grounded.
- the recipient's housing can also be grounded and thus be provided as a second electrode.
- the gas radicals are generated in a plasma space by means of microwaves and passed via a feed line into an etching chamber in which the substrate to be etched is arranged.
- the invention is based on the object of a method for producing a shaped bed for a membrane specify.
- the recess should precise in their depth and in their lateral dimensions and be reproducibly adjustable and a smooth Show depth profile.
- the first step is the substrate surface to be etched the pinhole device put on or applied.
- the pinhole device covers the area of the substrate surface in which the recess is to be created.
- the pinhole device form and the substrate surface has a cavity, that only through an opening in the pinhole device is connected to the reaction space.
- the etching radicals present in the reaction space during the etching only through the opening in the pinhole device to the area of the substrate surface to be etched reach.
- this increases the etching rate in this caustic area depending on location.
- the etching rate is on, moving largely in a straight line a location within the surface area to be etched in good approximation proportional to the solid angle at which one from this place on the surface through the reaction space can see the opening of the pinhole device.
- the Etch rate is at a center of the surface area to be etched directly below the opening of the pinhole device maximum and takes outward towards the edges ever further.
- FIG. 1 shows a substrate with 8, its surface with 9, an area of the surface 9 with 90, one in this area 90 lying recess in the surface 9 with 10, a point on the bottom of this recess 10 with P, a pot-like pinhole device with 5 with a base-like Side part 5a and a cover part 5b, an opening in this pinhole device in the cover part 5b with 6, the diameter of this opening with D, that of the thickness of the cover part 5b corresponding depth of this opening 6th with b, a central axis of the opening 6 with M, the distance the opening 6 from the surface 9 of the substrate 8 with a, one of the pinhole device 5 and the substrate surface 9 enclosed cavity with 11, one beyond of the cavity 11 lying on the other side of the opening 6 Reaction space with 4 and one from point P through the opening 6 seen solid angle section designated A.
- the pinhole device 5 is up to the opening 6 closed and open at the bottom. With your the base part 5a which is closed all around is the pinhole device 5 onto the surface 9 of the substrate 8 either put on in prefabricated form or by growing up and structuring corresponding layers applied and is usually after creating the recess removed again.
- the embodiment is the substrate surface to be etched 8 flat and the opening 6 in the applied Pinhole device 5 is parallel to surface 9 directed.
- the shape of the opening 6 is now transferred to defines fuzzy shape on the shape of the generated Recess 10.
- a rectangular Opening 6, the recess 10 is substantially rectangular and with a circular opening 6 essentially also be circular.
- the surface 9 of the substrate 8 can also be arbitrarily curved.
- the pinhole device 5 is then adjust according to the surface 9.
- the opening 6 can also be inclined to the surface 9 of the substrate 8.
- An asymmetrical depth profile of the recess is then obtained 10th
- r 0 is the maximum radius of the recess 10 in relation to the central axis M of the opening 6 of the perforated aperture device 5 which has already been removed and is therefore no longer shown in FIG. 2.
- the maximum radius r 0 is dependent on the diameter D, the depth b of the opening 6 and their distance a from the surface 9 of the substrate 8.
- the lateral edge of the cavity 11, which is defined by the side walls of the pinhole device 5, is closer to the central axis M in a radial direction than the maximum radius r 0 , this breaks Depth profile at this point on the edge.
- the actual radius of the recess 10 is then only as large as the distance between the cavity edge and the center axis M denoted by R.
- the recess 10 has its maximum depth t 0 along the center axis M. This maximum depth t 0 can be set by the etching time.
- etching gas radicals react chemically the material of the substrate 8 to form a gaseous, volatile reaction product.
- Halogen compounds as etching gas due to the high reactivity halogen radicals, especially fluorine and chlorine radicals, used.
- All substrate materials can be etched, for which there are suitable etching gases.
- substrate materials such as Silicon (Si), Germanium (Ge) or silicon carbide (SiC) provided.
- substrates 8 can also be used be etched from metals or insulators.
- the etching gas radicals are particularly advantageous Embodiment generated in a low pressure plasma. Under Low pressure becomes a pressure of 0.01 to 1000 Pa and preferably understood 0.1 to 100 Pa.
- the low pressure plasma can in a separate from the reaction space 4 Plasma chamber are generated.
- the resulting etching gas radicals are then via a gas line in the reaction chamber 4 headed. In another embodiment, this is Low pressure plasma directly inside the reaction space 4 generated.
- any known plasma reactor can be used.
- FIG. 3 shows an embodiment of a device to carry out the process with a parallel plate reactor illustrated.
- a recipient 2 there are two parallel plates arranged as electrodes 30 and 31.
- the reaction space lies between the electrodes 30 and 31 4.
- the substrate 8 is on the lower electrode 30 the pinhole device 5 arranged.
- the pinhole device 5 is usually before the introduction of the Substrate 8 in the recipient 2 on the substrate 8 as Whole set up.
- the electrode 30 with the substrate 8 is via a capacitor to a high-frequency generator 23 connected, the other electrode 31 and the housing of the Recipients 2 are grounded.
- a suction port 22 the recipient 2 is evacuated and via a feed nozzle 21 charged with etching gas.
- FIG. 4 and 5 a particularly advantageous embodiment of an apparatus for carrying out the method is shown in a plan view or in cross section.
- An etching protection layer 14 is applied to the surface 9 of the substrate 8.
- This etching protection layer 14 was structured in such a way that a circular etching area 91 of the surface 9 with a radius r 1 is exposed and preferably four alignment marks 15 are produced in a radially symmetrical manner with respect to the etching area 91.
- a cylindrically symmetrical pinhole device 5 is now placed on the etching protection layer 14 like an inverted cylinder pot.
- This cylinder pot can be made of aluminum, for example, as a turned part.
- the opening 6 is provided, which is circular and whose central axis M is equal to the cylinder axis of the cylinder pot.
- the pinhole device 5 is now adjusted with the aid of the alignment marks 15, for example by hand under a microscope, in such a way that the central axis M of its opening 6 runs perpendicularly through the center of the circular etching area 91.
- the edge of the recess 10 is precisely defined by the etching area 91 formed in the etching protection layer 14.
- the etching protection layer 14 can be removed again after the pinhole device 5 has been lifted off.
- an etching protection layer 14 made of SiO 2 is suitable, for example.
- the substrate 8 can subsequently be completely stripped with buffered hydrofluoric acid.
- Typical dimensions of the recess 10 are preferably approximately 10 ⁇ m to 1 mm for their lateral dimensions, in particular r 0 or r 1 or R, and preferably approximately 5 ⁇ m to 50 ⁇ m for their maximum depth t 0 .
- a pinhole device 5 is provided with a plurality of openings will.
- the depth profile of the recess 10 results then as an overlap (folding integral) of the individual profiles for the individual openings 6 if the openings 6 are close enough together. If the distances of the Openings 6 are sufficiently large to each other, can with this pinhole device 5 has a plurality of recesses 10 with the individual depth profiles of the corresponding openings 6 are generated. It is also possible to have several Pinhole devices 5 on a surface 9 of a Place or apply substrate 8 side by side.
- metals such as aluminum (Al), iron (Fe), nickel (Ni), titanium (Ti), molybdenum (Mo) or chrome (Cr).
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- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Drying Of Semiconductors (AREA)
Abstract
Description
- FIG 1
- ein Substrat mit aufgesetzter Lochblendeneinrichtung im Querschnitt,
- FIG 2
- das Tiefenprofil eine Ausnehmung in der Substratoberfläche nach Entfernen der Lochblendeneinrichrung,
- FIG 3
- eine Ausführungsform einer Trockenätzvorrichtung zum Erzeugen einer Ausnehmung in dem Substrat und
- FIG 4 und 5
- eine Ausführungsform einer Vorrichtung mit einer zylindrischen Lochblendeneinrichtung und einer Ätzschutzschicht auf dem Substrat in der Draufsicht bzw. im Querschnitt
Claims (12)
- Verfahren zum Erzeugen eines Formbetts für eine Membran mit folgenden Merkmalen:a) In einem Reaktionsraum (4) wird ein Substrat (8) angeordnet;b) in einer Oberfläche (9) des Substrats (8) wird durch Trockenätzen eine Ausnehmung (10) erzeugt, indemb1) auf die Oberfläche (9) des Substrats (8) eine Lochblendeneinrichtung (5) mit wenigstens einer Öffnung (6) derart aufgesetzt oder aufgebracht wird, daß nach dem Aufsetzen bzw. Aufbringen zwischen dem Bereich (90) der Oberfläche (9), in dem die Ausnehmung (10) zu erzeugen ist, und der Lochblendeneinrichtung (5) ein Hohlraum (11) entsteht, der nur über die Öffnung (6) mit dem Reaktionsraum (4) verbunden ist, und fernerb2) in dem Reaktionsraum (4) Ätzgasradikale eingebracht sind, die chemisch mit dem Material des Substrats (8) unter Bildung eines flüchtigen Reaktionsprodukts reagieren können;c) das Substrat (8) mit der Ausnehmung (10) in seiner Oberfläche (9) wird als Formbett für die Membran verwendet.
- Verfahren nach Anspruch 1, bei dem auf die Oberfläche (9) des Substrats (8) eine Ätzschutzschicht (14) aufgebracht wird und diese Ätzschutzschicht (14) in einem Ätzbereich (91) der Oberfläche (9), in dem die Ausnehmung (10) zu erzeugen ist, vor dem Aufbringen der Lochblendeneinrichtung (5) wieder entfernt wird.
- Verfahren nach Anspruch 2, bei dem in der Ätzschutzschicht (14) zusätzlich Justiermarken (15) zum Justieren der Lochblendeneinrichtung (5) erzeugt werden.
- Verfahren nach einem der vcrhergehenden Ansprüche, bei dem daß ein Substrat (8) aus einem Halbleitermaterial vorgesehen wird.
- Verfahren nach einem der vorhergehenden Ansprüche, bei dem die Ätzgasradikale in einem Niederdruckplasma erzeugt werden.
- Verfahren nach einem der vorhergehenden Ansprüche, bei dem die Lochblendeneinrichtung (5) in vorgefertigter Form auf die Oberfläche (9) des Substrats (8) aufgesetzt wird.
- Verfahren nach einem der vorhergehenden Ansprüche, bei cem die Membran als Teil eines Drucksensors vorgesehen ist.
- Verfahren nach einem der vorhergehenden Ansprüche, bei dem die Öffnung (6) der Lochblendeneinrichtung (5) nach dem Aufbringen der Lochblendeneinrichtung (5) in einen vorgegebenen Abstand (a) parallel zum Bereich (90) der Oberfläche (9), in dem die Ausnehmung (10) zu erzeugen ist, angeordnet ist.
- Verfahren nach Anspruch 8, bei dem die Öffnung (6) nach dem Aufbringen der Lochblendeneinrichtung (5) über einer Mitte des Bereichs (90) zu liegen kommt.
- Verfahren nach einem der Ansprüche 8 oder 9, bei dem die Lochblendeneinrichtung (5) die Gestalt eines Zylindertopfes hat, die Öffnung (6) kreisförmig ausgebildet ist und die Mittelachse (M) der Öffnung (6) mit der Zylinderachse des Zylindertopfes zusammenfällt.
- Verfahren nach einem der Ansprüche 8 oder 9, bei dem die Öffnung (6) von rechteckiger Gestalt ist.
- Verfahren nach einem der Ansprüche 8 bis 11, bei dem eine Lochblendeneinrichtung (5) aus einem Metall verwendet wird.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE4338575A DE4338575A1 (de) | 1993-11-11 | 1993-11-11 | Verfahren zum Erzeugen wenigstens einer Ausnehmung in einer Oberfläche eines Substrats, Vorrichtung zur Durchführung des Verfahrens und Verwendung des Verfahrensprodukts |
DE4338575 | 1993-11-11 | ||
PCT/DE1994/001274 WO1995013525A1 (de) | 1993-11-11 | 1994-10-28 | Verfahren zum erzeugen wenigstens einer ausnehmung in einer oberfläche eines substrats, vorrichtung zur durchführung des verfahrens und verwendung des verfahrensprodukts |
Publications (2)
Publication Number | Publication Date |
---|---|
EP0728298A1 EP0728298A1 (de) | 1996-08-28 |
EP0728298B1 true EP0728298B1 (de) | 1998-08-26 |
Family
ID=6502393
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP94931495A Expired - Lifetime EP0728298B1 (de) | 1993-11-11 | 1994-10-28 | Verfahren zum erzeugen wenigstens einer ausnehmung in einer oberfläche eines substrats als formbett für eine membran durch trockenätzen |
Country Status (5)
Country | Link |
---|---|
US (1) | US5693234A (de) |
EP (1) | EP0728298B1 (de) |
JP (1) | JP2785231B2 (de) |
DE (2) | DE4338575A1 (de) |
WO (1) | WO1995013525A1 (de) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6555476B1 (en) * | 1997-12-23 | 2003-04-29 | Texas Instruments Incorporated | Silicon carbide as a stop layer in chemical mechanical polishing for isolation dielectric |
US6261406B1 (en) * | 1999-01-11 | 2001-07-17 | Lsi Logic Corporation | Confinement device for use in dry etching of substrate surface and method of dry etching a wafer surface |
DE10340147B4 (de) | 2002-08-27 | 2014-04-10 | Kyocera Corp. | Trockenätzverfahren und Trockenätzvorrichtung |
US7556741B2 (en) | 2002-08-28 | 2009-07-07 | Kyocera Corporation | Method for producing a solar cell |
US7459098B2 (en) | 2002-08-28 | 2008-12-02 | Kyocera Corporation | Dry etching apparatus, dry etching method, and plate and tray used therein |
US20150020974A1 (en) * | 2013-07-19 | 2015-01-22 | Psk Inc. | Baffle and apparatus for treating surface of baffle, and substrate treating apparatus |
US10458012B2 (en) * | 2016-05-03 | 2019-10-29 | Caterpillar Inc. | Method for manufacturing a component |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS61161431A (ja) * | 1985-01-11 | 1986-07-22 | Yokogawa Electric Corp | 過大圧保護ダイアフラムの製造方法 |
EP0237844A1 (de) * | 1986-03-18 | 1987-09-23 | BBC Brown Boveri AG | Verfahren zur Herstellung einer Abdeckschicht für die Halbleitertechnik sowie Verwendung der Abdeckschicht |
US4975390A (en) * | 1986-12-18 | 1990-12-04 | Nippondenso Co. Ltd. | Method of fabricating a semiconductor pressure sensor |
US4905575A (en) * | 1988-10-20 | 1990-03-06 | Rosemount Inc. | Solid state differential pressure sensor with overpressure stop and free edge construction |
US4993143A (en) * | 1989-03-06 | 1991-02-19 | Delco Electronics Corporation | Method of making a semiconductive structure useful as a pressure sensor |
US4945769A (en) * | 1989-03-06 | 1990-08-07 | Delco Electronics Corporation | Semiconductive structure useful as a pressure sensor |
FR2654016B1 (fr) * | 1989-11-06 | 1992-02-14 | Step Soc Tech Pulverisation | Poussoir melangeur doseur. |
JP3194594B2 (ja) * | 1990-09-26 | 2001-07-30 | 株式会社日立製作所 | 構造体の製造方法 |
DE4206677C1 (de) * | 1992-02-28 | 1993-09-02 | Siemens Ag, 80333 Muenchen, De | |
DE4219857A1 (de) * | 1992-06-17 | 1993-12-23 | Perfect Ventil Gmbh | Verformbarer Behälter zum Ausbringen von Flüssigkeit |
-
1993
- 1993-11-11 DE DE4338575A patent/DE4338575A1/de not_active Withdrawn
-
1994
- 1994-10-28 JP JP7513465A patent/JP2785231B2/ja not_active Expired - Lifetime
- 1994-10-28 EP EP94931495A patent/EP0728298B1/de not_active Expired - Lifetime
- 1994-10-28 DE DE59406790T patent/DE59406790D1/de not_active Expired - Fee Related
- 1994-10-28 WO PCT/DE1994/001274 patent/WO1995013525A1/de active IP Right Grant
- 1994-10-28 US US08/640,972 patent/US5693234A/en not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
EP0728298A1 (de) | 1996-08-28 |
US5693234A (en) | 1997-12-02 |
JP2785231B2 (ja) | 1998-08-13 |
DE59406790D1 (de) | 1998-10-01 |
WO1995013525A1 (de) | 1995-05-18 |
JPH09501271A (ja) | 1997-02-04 |
DE4338575A1 (de) | 1995-05-18 |
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