CN202744480U - Heat exchanger of low-bromine epoxy resin reaction kettle - Google Patents

Heat exchanger of low-bromine epoxy resin reaction kettle Download PDF

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Publication number
CN202744480U
CN202744480U CN 201220252672 CN201220252672U CN202744480U CN 202744480 U CN202744480 U CN 202744480U CN 201220252672 CN201220252672 CN 201220252672 CN 201220252672 U CN201220252672 U CN 201220252672U CN 202744480 U CN202744480 U CN 202744480U
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China
Prior art keywords
housing
tube sheet
interchanger
end part
low bromine
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Expired - Lifetime
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CN 201220252672
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Chinese (zh)
Inventor
曾宪昌
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NEW POLY CHEMICAL (GUANGZHOU) CO Ltd
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NEW POLY CHEMICAL (GUANGZHOU) CO Ltd
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Priority to CN 201220252672 priority Critical patent/CN202744480U/en
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Publication of CN202744480U publication Critical patent/CN202744480U/en
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Abstract

The utility model discloses a heat exchanger of a low-bromine epoxy resin reaction kettle, which comprises a front condenser and a rear condenser; the front condenser comprises a first housing and a first pipe plate; heat exchange pipes are arranged between the first housing and the first pipe plate; a gas phase inlet is formed at the upper end part of one side of the first housing, and a water inlet is formed at the lower end part of the same side and positioned on the inner side of the first pipe plate; a gas phase outlet is formed at the upper end part of the other side of the first housing and positioned on the outer side of the first pipe plate; a water outlet is formed on the inner side of the first pipe plate; the rear condenser comprises a second housing and a second pipe plate; heat exchange pipes are arranged between the second housing and the second pipe plate horizontally; a partition board is horizontally mounted between one end of the second housing and the second pipe plate; a chilled water inlet is formed at the lower end part of the second housing and at the position corresponding to the partition board, and a chilled water outlet is formed at the upper end part; and a gas phase inlet is formed at the upper end of one side of the second housing and on the inner side of the second pipe plate. Acetone steam is cooled twice step by step by the heat exchanger, heat is removed, and most of acetone flows back to the reaction kettle, so that not only the loss of acetone can be reduced, but also environment pollution can be prevented.

Description

The interchanger of low bromine Resins, epoxy reactor
Technical field
The utility model relates to a kind of interchanger, belongs to the chemical industry equipment field, is in particular a kind of interchanger for secondary circulating cooling acetone.
Background technology
" energy-saving and emission-reduction " are country's one of fundamental state policies aspect energy environment protection.Comply with under the megatrend of environmental protection and energy saving, Chemical Manufacture and environment protection have the relation of Sustainable development, and wherein the gas that produces of chemical process and exhaust emissions are one of key issues very.In low bromine Resins, epoxy production, also face same problem, after low bromine Resins, epoxy reaction is finished, be in the condition of high temperature, by adding the acetone hot-cold lysis, if do not carry out respective handling to acetone and namely can cause acetone steam to be overflowed in a large number this moment, so that the lossy while of acetone also pollutes the environment.Chemical Manufacture generally adopts one-level condensation meeting to cause not reaching the effect of expection condensation in the prior art, even perhaps adopt B-grade condensation also to fail well to utilize the recycle of resource or to the protection of environment.
The utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, and the interchanger that a kind of low bromine Resins, epoxy reactor is provided is to prevent overflow the in a large number technical problem of contaminate environment when solving acetone loss Datong District of acetone steam.
For reaching above-mentioned technical purpose, the utility model is achieved through the following technical solutions:
The interchanger of a kind of low bromine Resins, epoxy reactor of the present utility model, it comprises front cool condenser and rear cool condenser, described front cool condenser comprises the first housing and the first tube sheet, be provided with some heat transfer tubes between the first tube sheet in described the first housing, one side upper end of described the first housing is provided with the gas phase import, lower end part at homonymy is provided with water-in in described the first tube sheet inboard, in this first tube sheet arranged outside gaseous phase outlet is arranged at described the first housing offside upper-end part of driving, be provided with water outlet and be positioned at this first tube sheet inboard; Described rear cool condenser comprises the second housing and the second tube sheet, some heat transfer tubes have been horizontally disposed with between the second tube sheet in described the second housing, one termination of described the second housing is horizontally installed with a dividing plate between described the second tube sheet, correspondingly with described partition position be positioned at described the second housing bottom and be provided with the refrigerated water import, and the upper end is provided with chilled water outlet, and described the second housing homonymy upper-end part of driving is provided with the gas phase import in described the second tube sheet inboard.
Further, described the first housing, the second housing right-to-left end are obliquely installed from high to low.
Further, in described the first housing between the first tube sheet, all be vertically installed with traverse baffle between the second tube sheet in the second housing.
Further, the top and bottom of described the first housing, the second housing are provided with expansion joint.
Further, described the first housing bottom and this gaseous phase outlet opposite position are provided with condensate outlet.
Further, described the first tube sheet one inside bottom is provided with leakage fluid dram.
Further, the lower end part of described the second housing offside is provided with condensate outlet in this second tube sheet inboard.
Further, the upper-end part of driving of described the second housing offside is equipped with drain in these the second tube sheet both sides.
Further, described the second tube sheet one inside bottom is provided with discharging hole.
Compared with prior art, the beneficial effects of the utility model:
The utility model structurally by front cold, rear cool condenser so that acetone through twice on interchanger step by step cooling band walk heat, the overwhelming majority passes back into reactor, prevents that acetone steam from overflowing in a large number, so that the lossy while of acetone also pollutes the environment.
Description of drawings
Fig. 1 is structural representation of the present utility model.
Fig. 1: 1, front cool condenser; 10, heat transfer tube; 11, the first housing; 111 first tube sheets; 12, gas phase import; 13, water inlet; 14, gaseous phase outlet; 15, water outlet; 16, condensate outlet; 17, leakage fluid dram; 18, expansion joint; 19, traverse baffle; 2, rear cool condenser; 20, heat transfer tube; 21, the second housing; 211, the second tube sheet; 22, gas phase import; 23, refrigerated water import; 24, drain; 25, chilled water outlet; 26, condensate outlet; 27, rinse mouth; 28, expansion joint; 29, traverse baffle; 30, dividing plate; 31, discharging hole
Embodiment
As shown in Figure 1, the interchanger of a kind of low bromine Resins, epoxy reactor of the present utility model, it comprises front cool condenser 1 and rear cool condenser 2, and described the first housing 11, the second housing 21 equal right-to-left ends are obliquely installed from high to low, so that recirculated water and refrigerated water flow, make that itself and acetone steam are more abundant to be contacted.Described front cool condenser 1 comprises the first housing 11 and the first tube sheet 111, some heat transfer tubes 10 have been horizontally disposed with between the first tube sheet 111 in described the first housing 11, be vertically installed with traverse baffle 19 between described the first housing 11 interior described the first tube sheets 111, improve the shell side flow velocity with this, increase fluid shell side path, finally strengthen heat transfer effect and also play the effect of supporting heat transfer tube.Described front cool condenser 1 is positioned at described the first housing 11 top and bottom and is provided with expansion joint 18, because be that heat and mass is carried out in the lower refrigerated water heat exchange of high temperature gas phase and temperature lower recirculated water, temperature in the condenser, therefore have the phenomenon of expanding with heat and contract with cold, the described expansion joint 18 of setting strengthens interchanger heat expansion shrinkage ability to bear.One side upper end of described the first housing 11 is provided with gas phase import 12, enters for acetone steam.Lower end part at homonymy is provided with water-in 13 in described the first tube sheet 111 inboards, and recirculated water enters from this water-in 13.In these the first tube sheet 111 arranged outside gaseous phase outlet 14 is arranged at described the first housing 11 offside upper-end part of drivings, for carrying out acetone steam output after the heat exchange with recirculated water.The recirculated water that obtains heat with the acetone steam heat exchange is then exported from the water outlet 15 that is positioned at these the first tube sheet 111 inboards.The first tube sheet 111 inside bottom of described front cool condenser 1 are provided with leakage fluid dram 17.Described the first housing 11 bottoms and this gaseous phase outlet 14 opposite positions are provided with condensate outlet 16, and acetone steam is through changing the just from then on mouthful discharge of thermogenetic phlegma with recirculated water.
Described rear cool condenser 2 comprises the second housing 21 and the second tube sheet 211, has been horizontally disposed with some heat transfer tubes 20 between the second tube sheet 211 in described the second housing 21, all is vertically installed with traverse baffle 29 between described the second housing 21 the interior the described the 2 211.Described rear cool condenser 2 is positioned at described the second housing 21 upper ends, the lower end is provided with expansion joint 28.One termination of described the second housing 21 is horizontally installed with a dividing plate 30 between described the second tube sheet 211, because the second housing 21 upper and lower end parts will arrange respectively refrigerated water import and outlet in this section space.Corresponding described the second housing 21 bottoms that are positioned at described dividing plate 30 positions are provided with refrigerated water import 23, and the upper end is provided with chilled water outlet 25, and described the second housing 21 homonymy upper-end part of drivings are provided with gas phase import 22 in described the second tube sheet 211 inboards.Described the second housing 21 offside lower end parts are provided with condensate outlet 26 in this tube sheet inboard.Described the second housing 21 offside upper-end part of drivings are provided with drain 24 in these tube sheet both sides, are used for draining described the second housing 21 interior a small amount of gases, because almost all reflux in described condenser 2 at this stage acetone steam, therefore gaseous phase outlet are set no longer.The second tube sheet 211 inside bottom of described rear cool condenser 2 are provided with discharging hole 31, and it act as the foreign material in the emptying pipeline.
Utilize the lower boiling of acetone, make acetone through twice on interchanger step by step cooling band walk heat, again its overwhelming majority is passed back into reactor.In front cool condenser, amount of heat is taken away in recirculated water and acetone heat exchange, allows a large amount of acetone reflux at this.This moment, acetone steam refluxed in tube side, and recirculated water refluxes in shell side; In rear cool condenser, make refrigerated water and acetone heat exchange, deep condensation allows residue acetone almost all in this backflow, and acetone steam refluxes in shell side, and refrigerated water refluxes in tube side.By B-grade condensation, the acetone of cleaning is recovered use, has realized that the resource recycling has also reduced environmental pollution.
The utility model is not limited to above-mentioned embodiment, if various changes of the present utility model or modification are not broken away from spirit and scope of the present utility model, if these are changed and modification belongs within claim of the present utility model and the equivalent technologies scope, then the utility model also comprises these changes and modification.

Claims (9)

1. the interchanger of one kind low bromine Resins, epoxy reactor is characterized in that, described interchanger comprises front cool condenser and rear cool condenser,
Described front cool condenser comprises the first housing and the first tube sheet, be provided with some heat transfer tubes between the first tube sheet in described the first housing, one side upper end of described the first housing is provided with the gas phase import, lower end part at homonymy is provided with water-in in described the first tube sheet inboard, in this first tube sheet arranged outside gaseous phase outlet is arranged at described the first housing offside upper-end part of driving, be provided with water outlet and be positioned at this first tube sheet inboard;
Described rear cool condenser comprises the second housing and the second tube sheet, some heat transfer tubes have been horizontally disposed with between the second tube sheet in described the second housing, one termination of described the second housing is horizontally installed with a dividing plate between described the second tube sheet, correspondingly with described partition position be positioned at described the second housing bottom and be provided with the refrigerated water import, and the upper end is provided with chilled water outlet, and described the second housing homonymy upper-end part of driving is provided with the gas phase import in described the second tube sheet inboard.
2. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that described the first housing, the second housing right-to-left end are obliquely installed from high to low.
3. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that, in described the first housing between the first tube sheet, all be vertically installed with traverse baffle between the second tube sheet in the second housing.
According to claim 1 described low bromine Resins, epoxy reactor interchanger, it is characterized in that the top and bottom of described the first housing, the second housing are provided with expansion joint.
5. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that described the first housing bottom and this gaseous phase outlet opposite position are provided with condensate outlet.
6. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that described the first tube sheet one inside bottom is provided with leakage fluid dram.
7. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that the lower end part of described the second housing offside is provided with condensate outlet in this second tube sheet inboard.
8. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that the upper-end part of driving of described the second housing offside is equipped with drain in these the second tube sheet both sides.
9. the interchanger of described low bromine Resins, epoxy reactor according to claim 1 is characterized in that described the second tube sheet one inside bottom is provided with discharging hole.
CN 201220252672 2012-05-30 2012-05-30 Heat exchanger of low-bromine epoxy resin reaction kettle Expired - Lifetime CN202744480U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220252672 CN202744480U (en) 2012-05-30 2012-05-30 Heat exchanger of low-bromine epoxy resin reaction kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220252672 CN202744480U (en) 2012-05-30 2012-05-30 Heat exchanger of low-bromine epoxy resin reaction kettle

Publications (1)

Publication Number Publication Date
CN202744480U true CN202744480U (en) 2013-02-20

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105944401A (en) * 2016-06-25 2016-09-21 余林岚 Condensation tower for machining anaerobic adhesive
CN106745432A (en) * 2017-01-13 2017-05-31 华南理工大学 A kind of bubble type solar energy sea water desalination apparatus and its method for desalting seawater

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105944401A (en) * 2016-06-25 2016-09-21 余林岚 Condensation tower for machining anaerobic adhesive
CN106745432A (en) * 2017-01-13 2017-05-31 华南理工大学 A kind of bubble type solar energy sea water desalination apparatus and its method for desalting seawater

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Granted publication date: 20130220