CN1609055A - 一种钛硅碳化物粉及其以铝为反应助剂的常压合成方法 - Google Patents
一种钛硅碳化物粉及其以铝为反应助剂的常压合成方法 Download PDFInfo
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- CN1609055A CN1609055A CN 200410009589 CN200410009589A CN1609055A CN 1609055 A CN1609055 A CN 1609055A CN 200410009589 CN200410009589 CN 200410009589 CN 200410009589 A CN200410009589 A CN 200410009589A CN 1609055 A CN1609055 A CN 1609055A
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- powder
- silicon carbide
- sic
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- titanium silicon
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- 239000000843 powder Substances 0.000 title claims abstract description 34
- 238000006243 chemical reaction Methods 0.000 title claims abstract description 19
- 238000000034 method Methods 0.000 title claims description 10
- 229910004339 Ti-Si Inorganic materials 0.000 title abstract 2
- 229910010978 Ti—Si Inorganic materials 0.000 title abstract 2
- 230000015572 biosynthetic process Effects 0.000 title description 4
- 238000003786 synthesis reaction Methods 0.000 title description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000000463 material Substances 0.000 claims abstract description 12
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 8
- 229910052719 titanium Inorganic materials 0.000 claims abstract description 6
- 229910010271 silicon carbide Inorganic materials 0.000 claims description 40
- 239000010936 titanium Substances 0.000 claims description 33
- UGACIEPFGXRWCH-UHFFFAOYSA-N [Si].[Ti] Chemical compound [Si].[Ti] UGACIEPFGXRWCH-UHFFFAOYSA-N 0.000 claims description 18
- 239000002994 raw material Substances 0.000 claims description 11
- 229910002804 graphite Inorganic materials 0.000 claims description 9
- 239000010439 graphite Substances 0.000 claims description 9
- 238000002156 mixing Methods 0.000 claims description 9
- 229910052782 aluminium Inorganic materials 0.000 claims description 8
- 239000004411 aluminium Substances 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 238000009413 insulation Methods 0.000 claims description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 4
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 4
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims description 4
- 238000010438 heat treatment Methods 0.000 claims description 4
- 239000010703 silicon Substances 0.000 claims description 4
- 239000011863 silicon-based powder Substances 0.000 claims description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 2
- 238000000498 ball milling Methods 0.000 claims description 2
- 238000001354 calcination Methods 0.000 claims description 2
- 238000001816 cooling Methods 0.000 claims description 2
- 229960000935 dehydrated alcohol Drugs 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 238000007873 sieving Methods 0.000 claims description 2
- 230000002194 synthesizing effect Effects 0.000 claims description 2
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 abstract description 6
- 229910052786 argon Inorganic materials 0.000 abstract description 4
- 238000002360 preparation method Methods 0.000 description 8
- 238000010189 synthetic method Methods 0.000 description 5
- 229910018540 Si C Inorganic materials 0.000 description 3
- 239000007795 chemical reaction product Substances 0.000 description 3
- 238000007731 hot pressing Methods 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 239000011159 matrix material Substances 0.000 description 3
- 238000002441 X-ray diffraction Methods 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- DXZIFGZIQQRESB-UHFFFAOYSA-N [C].[Ti].[Si] Chemical compound [C].[Ti].[Si] DXZIFGZIQQRESB-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000013590 bulk material Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000003837 high-temperature calcination Methods 0.000 description 1
- 238000001513 hot isostatic pressing Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000001902 propagating effect Effects 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- MTPVUVINMAGMJL-UHFFFAOYSA-N trimethyl(1,1,2,2,2-pentafluoroethyl)silane Chemical compound C[Si](C)(C)C(F)(F)C(F)(F)F MTPVUVINMAGMJL-UHFFFAOYSA-N 0.000 description 1
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Abstract
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CN 200410009589 CN1251994C (zh) | 2004-09-21 | 2004-09-21 | 一种钛硅碳化物粉及其以铝为反应助剂的常压合成方法 |
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CN 200410009589 CN1251994C (zh) | 2004-09-21 | 2004-09-21 | 一种钛硅碳化物粉及其以铝为反应助剂的常压合成方法 |
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CN1609055A true CN1609055A (zh) | 2005-04-27 |
CN1251994C CN1251994C (zh) | 2006-04-19 |
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CN 200410009589 Expired - Fee Related CN1251994C (zh) | 2004-09-21 | 2004-09-21 | 一种钛硅碳化物粉及其以铝为反应助剂的常压合成方法 |
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CN (1) | CN1251994C (zh) |
Cited By (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100382918C (zh) * | 2005-11-10 | 2008-04-23 | 上海大学 | Ti3AlC2粉体的制备方法 |
CN101508591B (zh) * | 2008-11-10 | 2011-09-14 | 西北工业大学 | Ti3SiC2改性C/SiC复合材料的制备方法 |
CN102659106A (zh) * | 2011-11-28 | 2012-09-12 | 镇江中孚复合材料有限公司 | 一种无压烧结合成高纯度Ti3SiC2粉体的方法 |
CN102703161A (zh) * | 2012-05-14 | 2012-10-03 | 无锡润鹏复合新材料有限公司 | 一种自润滑铜-Ti3SiC2-NbSe2复合材料及其制备方法 |
CN103341291A (zh) * | 2013-06-30 | 2013-10-09 | 成都易态膜分离技术有限公司 | 烧结多孔材料及应用该多孔材料的过滤元件 |
CN108341670A (zh) * | 2018-02-02 | 2018-07-31 | 西南科技大学 | 单相Ti3SiC2金属陶瓷的制备方法 |
CN110128145A (zh) * | 2019-06-26 | 2019-08-16 | 辽宁工业大学 | 一种合成高纯Ti3SiC2的方法 |
CN110156018A (zh) * | 2019-06-03 | 2019-08-23 | 蚌埠学院 | 一种高纯度钛硅碳材料的制备方法 |
CN111282586A (zh) * | 2020-03-24 | 2020-06-16 | 福州大学 | 一种原位氧化铝包覆碳化钛催化剂的制备方法及其应用 |
CN112919470A (zh) * | 2021-01-21 | 2021-06-08 | 辽宁中色新材科技有限公司 | 一种碳化硅钛的生产工艺 |
-
2004
- 2004-09-21 CN CN 200410009589 patent/CN1251994C/zh not_active Expired - Fee Related
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100382918C (zh) * | 2005-11-10 | 2008-04-23 | 上海大学 | Ti3AlC2粉体的制备方法 |
CN101508591B (zh) * | 2008-11-10 | 2011-09-14 | 西北工业大学 | Ti3SiC2改性C/SiC复合材料的制备方法 |
CN102659106A (zh) * | 2011-11-28 | 2012-09-12 | 镇江中孚复合材料有限公司 | 一种无压烧结合成高纯度Ti3SiC2粉体的方法 |
CN102703161B (zh) * | 2012-05-14 | 2014-10-22 | 无锡润鹏复合新材料有限公司 | 一种自润滑铜-Ti3SiC2-NbSe2复合材料及其制备方法 |
CN102703161A (zh) * | 2012-05-14 | 2012-10-03 | 无锡润鹏复合新材料有限公司 | 一种自润滑铜-Ti3SiC2-NbSe2复合材料及其制备方法 |
CN103341291B (zh) * | 2013-06-30 | 2015-07-15 | 成都易态膜分离技术有限公司 | 烧结多孔材料及应用该多孔材料的过滤元件 |
CN103341291A (zh) * | 2013-06-30 | 2013-10-09 | 成都易态膜分离技术有限公司 | 烧结多孔材料及应用该多孔材料的过滤元件 |
CN108341670A (zh) * | 2018-02-02 | 2018-07-31 | 西南科技大学 | 单相Ti3SiC2金属陶瓷的制备方法 |
CN108341670B (zh) * | 2018-02-02 | 2020-08-04 | 西南科技大学 | 单相Ti3SiC2金属陶瓷的制备方法 |
CN110156018A (zh) * | 2019-06-03 | 2019-08-23 | 蚌埠学院 | 一种高纯度钛硅碳材料的制备方法 |
CN110128145A (zh) * | 2019-06-26 | 2019-08-16 | 辽宁工业大学 | 一种合成高纯Ti3SiC2的方法 |
CN111282586A (zh) * | 2020-03-24 | 2020-06-16 | 福州大学 | 一种原位氧化铝包覆碳化钛催化剂的制备方法及其应用 |
CN111282586B (zh) * | 2020-03-24 | 2022-07-08 | 福州大学 | 一种原位氧化铝包覆碳化钛催化剂的制备方法及其应用 |
CN112919470A (zh) * | 2021-01-21 | 2021-06-08 | 辽宁中色新材科技有限公司 | 一种碳化硅钛的生产工艺 |
Also Published As
Publication number | Publication date |
---|---|
CN1251994C (zh) | 2006-04-19 |
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