CN1275346A - 一种干馏山楂核以提取汁液的新方法及设备 - Google Patents

一种干馏山楂核以提取汁液的新方法及设备 Download PDF

Info

Publication number
CN1275346A
CN1275346A CN00109230A CN00109230A CN1275346A CN 1275346 A CN1275346 A CN 1275346A CN 00109230 A CN00109230 A CN 00109230A CN 00109230 A CN00109230 A CN 00109230A CN 1275346 A CN1275346 A CN 1275346A
Authority
CN
China
Prior art keywords
juice
chinese hawthorn
hawthorn seed
destructive distillation
extract
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN00109230A
Other languages
English (en)
Other versions
CN1149018C (zh
Inventor
石易
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Individual
Original Assignee
Individual
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Individual filed Critical Individual
Priority to CNB001092308A priority Critical patent/CN1149018C/zh
Publication of CN1275346A publication Critical patent/CN1275346A/zh
Priority to US10/311,461 priority patent/US6821394B2/en
Priority to JP2002503347A priority patent/JP3967265B2/ja
Priority to EP01951334A priority patent/EP1295603A4/en
Priority to AU2001272318A priority patent/AU2001272318A1/en
Priority to PCT/CN2001/000971 priority patent/WO2001097864A1/zh
Application granted granted Critical
Publication of CN1149018C publication Critical patent/CN1149018C/zh
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
    • A01N65/08—Magnoliopsida [dicotyledons]
    • A01N65/34—Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00—Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18—Magnoliophyta (angiosperms)
    • A61K36/185—Magnoliopsida (dicotyledons)
    • A61K36/73—Rosaceae (Rose family), e.g. strawberry, chokeberry, blackberry, pear or firethorn
    • A61K36/734—Crataegus (hawthorn)
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
    • A61P1/02—Stomatological preparations, e.g. drugs for caries, aphtae, periodontitis
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P1/00—Drugs for disorders of the alimentary tract or the digestive system
    • A61P1/16—Drugs for disorders of the alimentary tract or the digestive system for liver or gallbladder disorders, e.g. hepatoprotective agents, cholagogues, litholytics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P17/00—Drugs for dermatological disorders
    • A61P17/02—Drugs for dermatological disorders for treating wounds, ulcers, burns, scars, keloids, or the like
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P31/00—Antiinfectives, i.e. antibiotics, antiseptics, chemotherapeutics
    • A61P31/02—Local antiseptics
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61P—SPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P9/00—Drugs for disorders of the cardiovascular system
    • A61P9/10—Drugs for disorders of the cardiovascular system for treating ischaemic or atherosclerotic diseases, e.g. antianginal drugs, coronary vasodilators, drugs for myocardial infarction, retinopathy, cerebrovascula insufficiency, renal arteriosclerosis
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E50/00—Technologies for the production of fuel of non-fossil origin
    • Y02E50/10—Biofuels, e.g. bio-diesel
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/13—Spirits
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00—Distillation: processes, separatory
    • Y10S203/16—Combination

Landscapes

  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Natural Medicines & Medicinal Plants (AREA)
  • Engineering & Computer Science (AREA)
  • General Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Organic Chemistry (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • General Chemical & Material Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Biotechnology (AREA)
  • Microbiology (AREA)
  • Mycology (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Medical Informatics (AREA)
  • Agronomy & Crop Science (AREA)
  • Botany (AREA)
  • Alternative & Traditional Medicine (AREA)
  • Environmental Sciences (AREA)
  • Plant Pathology (AREA)
  • Dentistry (AREA)
  • Heart & Thoracic Surgery (AREA)
  • Urology & Nephrology (AREA)
  • Vascular Medicine (AREA)
  • Cardiology (AREA)
  • Oncology (AREA)
  • Communicable Diseases (AREA)
  • Gastroenterology & Hepatology (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Medicines Containing Plant Substances (AREA)
  • Non-Alcoholic Beverages (AREA)

Abstract

本发明为改进了的从山楂核直接提取山楂核汁液技术,采用炉内直接加热山楂核使其产生汽烟,将汽烟导入胆管然后冷凝,产出山楂核汁液,再经沉淀分离,静置比重分离,得到产品。本发明增加了入炉前将山楂核原料长时间浸泡的工艺,发明设备主要由炉体、胆管、导出管及冷凝器构成,用本发明方法和设备干馏的山楂汁液产出率高。本发明方法及设备易实施,可实现工业化批量生产,设备结构及安装均较简单,干馏工艺操作易行。

Description

一种干馏山楂核以提取汁液的新方法及设备
本发明属于果核加工技术领域，尤其涉及山楂核加工技术。
山楂是一种人们喜爱的酸味水果，我国北方许多省份均有种植，它可以做成各种食品，以满足不同口味之需要，但其果核——山楂核却大多未被利用，有的作为燃料烧掉，十分可惜。
现代科技方法已经证实，从山楂核中提取的汁液有人们预想不到的抗菌、杀菌及消毒的功效，而且已广泛应用于医药卫生、食品加工及环保各领域，例如以山楂核液为原料制成的体外皮肤杀菌剂，对皮肤粘膜无刺激，并且无任何毒副作用，用山楂核液制成蚊香，有很好的杀蚊效果，并且于人体无任何不良作用，随着科学技术不断发展，它的用途领域也会逐渐拓宽。
但目前干馏山楂核技术方法，产出率受到一定限制，如何利用合理的提取工艺，尽量简化的生产设备提高其产出率，是目前生产领域部门普遍关心的问题，这也正是本发明所要解决的问题。
本发明的目的是提供一种改进了的提取山楂核汁液的方法及设备，以便在同样的能耗下获取更高的产出率。
本发明是通过以下技术方案完成的，经过反复试验证明，山楂核在洗净入炉前，必须经过长时间水浸泡，一般约为12-14小时，而且沥水后即入炉(勿使山楂核干燥)，因此本发明方法步骤包括：
①洗净山楂核，去掉其中杂质(前面山楂加工中留下来的除核以外杂质)；
②自然凉干；
③入炉前用水浸泡；
④沥水后即入炉；
⑤两段加温，提取干馏液。
⑥两段加温干馏液混合沉淀；
⑦分离水状物；
⑧静置比重分离；
⑨虹吸分离。
以上③、④两步时间上必须连续，不可延隔。
根据上述方法步骤设计了本发明设备，它主要由炉体、胆管、导出管、冷凝管、冷凝器构成，胆管与导出管连接进而再与冷凝管连接形成山楂核汁液产出通路，即成品山楂汁液最后从冷凝管流出。
胆管为一管壁多孔的一端封闭式园管。
胆管置于炉中心，其周围则为原料山楂核包围，当然也可并行设置数路胆管，分别与数个导出管及数个冷凝管连接形成数条产出通路。
本发明有益效果：
①本发明工艺方法的山楂核汁液产出率高。
②产品用途广，可衍生产品包括：祛疣液、脚股癣液、烫伤药、褥疮药、妇女洗液、口洁液、杀菌剂、杀菌卫生香、植物型农药、食品添加剂、HIV×AIDS药、食用菌生长素、肝炎药、战地急救包(外用)。
③本发明工艺方法易于实施，适于山楂产区乡镇建厂投产。
④本发明设备，结构简单，易于制造，成本低廉。
附图说明：
图1为本发明设备示意图
图2为本发明方法流程图
以下接合附图说明实施例：
图1所示，其中1为热源(可用煤火也可用天燃气或电热)，2为炉体，3为胆管，4为导出管，5为冷凝管，6为冷凝器，7为山楂核原料入口，8为山楂核废料出口，9为温度计，10为温度表，11为山楂核汁液出口，12为冷凝水进口，13为冷凝水出口。
炉体应选碳钢，材质厚度在10-20mm，胆管上的透汽孔尺寸应小于山楂核(可选2-3mm)以免其周围的山楂核料进入胆管，设一条胆管时胆管位于炉体中心，本实施例炉体高1.8米，直径1米，胆管直径10厘米，进料口直径20厘米，出料口直径25厘米，冷凝器高80厘米，直径30厘米，冷凝管初始直径10厘米，后渐细，冷凝管可盘旋10几卷后伸出冷凝器外。
进出料口、胆管与导出管连接处，导出管与冷凝管连接处均采用法兰型连接，并夹以石棉垫密封，上述实施例干馏炉，每炉可处理约350公斤山楂核。
以下叙述动态操作过程，参见图2。
将山楂核洗净，并去掉杂质(在山楂加工时，剩下来的果肉，枝叶等)，凉干后备用。正式入炉前须浸泡12-14小时，主要为使其膨胀，核中吸纳水分，达到提高产出率之目的，同时也有进一步去土和去杂质的作用，浸泡后山楂核放入漏孔容器，自然沥掉水分，约1小时后装入炉中，入料高度约为炉体内2/3，即上部留有1/3空间。将炉封闭，然后即可点火升温，火源可用煤(炉外加垒炉灶)煤气、天燃气，或电热均可，以能达到预期温度为目的，升温速度采用逐渐为宜，且采取两段加温：当温度升至105℃时恒温/小时，此后在115、135、155、175、195℃各恒温1小时，以收取山楂核液；第二段当温度升至305℃时恒温/小时，此后325、345、365℃各恒温1小时再继续收取山楂核液。将两温度段山楂核液混合沉淀36小时，分离出上层水状物，然后于容器中静置48小时，采用物质比重分离法在常温或低于常温、常压下使产品分为两层，虹吸出上层棕红色透明液即为本发明产品。
有关本发明设备，由于高温和山楂的酸性腐蚀作用，胆管每三炉要拆下清洗，炉体也宜1个月后更换(耐温耐蚀材质可延长)。

Claims (6)

1、一种干馏山楂核以提取汁液的新方法，其特征在于按照如下流程进行：
①洗净山楂核，去掉杂质；
②自然凉干；
③入炉前用水浸泡；
④沥水后即入炉；
⑤两段加温，提取干馏液。
⑥两段加温干馏液混合沉淀；
⑦分离水状物；
⑧静置比重分离；
⑨虹吸分离。
2、如权利要求1所述的一种干馏山楂核以提取汁液的新方法，其特征在于所述以水浸泡，时间约在12-14小时。
3、如权利要求1所述的一种干馏山楂核以提取汁液的新方法，其特征在于所述的两段阶梯恒温法为第一段当温度升至105℃时恒温1小时，此后在115、135、155、175、195℃各恒温1小时，以干馏山楂核；第二段当温度升至305℃时恒温1小时，此后325、345、365℃各恒温1小时以继续高温下干馏。
4、如权利要求3所述的一种干馏山楂核以提取汁液的新方法，其特征在于升温最高不超过380℃。
5、一种干馏山楂核以提取汁液的设备，主要由炉体、胆管、导出管、冷凝管、冷凝器组成，其特征在于胆管与导出管连结，导出管与冷凝管连接形成胆管、导出管及冷凝管通路以使成品山楂核汁液直接流出。
6、如权利要求5所述的一种干馏山楂核以提取汁液的设备，其特征在于也可设置两条或两条以上的胆管、导出管及冷凝管通路，即炉体内可同时***两根或两根以上胆管，形成多路平行引出汁液通路。
CNB001092308A 2000-06-16 2000-06-16 一种干馏山楂核以提取汁液的新方法及设备 Expired - Fee Related CN1149018C (zh)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CNB001092308A CN1149018C (zh) 2000-06-16 2000-06-16 一种干馏山楂核以提取汁液的新方法及设备
US10/311,461 US6821394B2 (en) 2000-06-16 2001-06-15 Process of extracting from haw-pit by dry distillation and its device
JP2002503347A JP3967265B2 (ja) 2000-06-16 2001-06-15 乾留による山査子核からの抽出方法及びその装置
EP01951334A EP1295603A4 (en) 2000-06-16 2001-06-15 METHOD FOR EXTRACTING CELLULAR CORES BY DRY DISTILLATION AND DEVICE THEREOF
AU2001272318A AU2001272318A1 (en) 2000-06-16 2001-06-15 The process of extracting from haw-pit by dry distillation and its device
PCT/CN2001/000971 WO2001097864A1 (fr) 2000-06-16 2001-06-15 Procede d'extraction de noyaux de cenelles par distillation seche et dispositif associe

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB001092308A CN1149018C (zh) 2000-06-16 2000-06-16 一种干馏山楂核以提取汁液的新方法及设备

Publications (2)

Publication Number Publication Date
CN1275346A true CN1275346A (zh) 2000-12-06
CN1149018C CN1149018C (zh) 2004-05-12

Family

ID=4579513

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB001092308A Expired - Fee Related CN1149018C (zh) 2000-06-16 2000-06-16 一种干馏山楂核以提取汁液的新方法及设备

Country Status (6)

Country Link
US (1) US6821394B2 (zh)
EP (1) EP1295603A4 (zh)
JP (1) JP3967265B2 (zh)
CN (1) CN1149018C (zh)
AU (1) AU2001272318A1 (zh)
WO (1) WO2001097864A1 (zh)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1330332C (zh) * 2003-06-26 2007-08-08 深圳帝阳药业有限公司 治疗***炎、皮肤病的药物及其制备方法
CN106866224A (zh) * 2017-01-12 2017-06-20 山东森科尔生物药业有限公司 植物提取物、含植物提取物的植物肥料及其应用
CN107619673A (zh) * 2017-11-01 2018-01-23 承德本多宝生物科技有限公司 山楂核熏蒸汽化提取***及提取方法
CN107674759A (zh) * 2017-11-01 2018-02-09 承德本多宝生物科技有限公司 一种植物药液提取与活性炭生产加工设备及工艺
CN110923056A (zh) * 2019-12-13 2020-03-27 北京多宝德健康科技产业发展有限公司 一种干馏山楂核提取液方法及装置

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN115968915A (zh) * 2022-12-21 2023-04-18 山西巴盾环境保护技术研究所 一种全新无色低刺激性山楂核精改进制备工艺及应用

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5534280A (en) * 1987-12-04 1996-07-09 Welch; George Method for dehydration of solid foods
CN1041281A (zh) 1989-10-03 1990-04-18 华东化工学院 从山楂核中提取医用舒痛精的方法
US6613366B1 (en) * 1990-02-16 2003-09-02 The Harvest Festival Ltd. Enzyme-rich sprouted food products with limited pH drop and methods of making same
CN1102206A (zh) * 1993-10-26 1995-05-03 山东省科学院生物研究所 食用烟熏香料的提取方法
AU3163797A (en) * 1996-06-20 1998-01-07 Fuxing Gao A pure natural disinfectant and food additive product and its preparation
US5773241A (en) * 1996-09-05 1998-06-30 Ericsson; Arthur Dale Preparation of bioactive extracts
CN1059308C (zh) * 1996-11-20 2000-12-13 韩林 从山楂核中提取消毒杀菌剂的方法
US6289543B1 (en) * 1999-07-16 2001-09-18 Frans Segers Process and system for processing cherry pits

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1330332C (zh) * 2003-06-26 2007-08-08 深圳帝阳药业有限公司 治疗***炎、皮肤病的药物及其制备方法
CN106866224A (zh) * 2017-01-12 2017-06-20 山东森科尔生物药业有限公司 植物提取物、含植物提取物的植物肥料及其应用
CN107619673A (zh) * 2017-11-01 2018-01-23 承德本多宝生物科技有限公司 山楂核熏蒸汽化提取***及提取方法
CN107674759A (zh) * 2017-11-01 2018-02-09 承德本多宝生物科技有限公司 一种植物药液提取与活性炭生产加工设备及工艺
CN107619673B (zh) * 2017-11-01 2024-01-30 承德本多宝生物科技有限公司 山楂核熏蒸汽化提取***及提取方法
CN110923056A (zh) * 2019-12-13 2020-03-27 北京多宝德健康科技产业发展有限公司 一种干馏山楂核提取液方法及装置

Also Published As

Publication number Publication date
US6821394B2 (en) 2004-11-23
JP2003535914A (ja) 2003-12-02
US20030159914A1 (en) 2003-08-28
WO2001097864A1 (fr) 2001-12-27
JP3967265B2 (ja) 2007-08-29
EP1295603A4 (en) 2009-05-27
CN1149018C (zh) 2004-05-12
AU2001272318A1 (en) 2002-01-02
EP1295603A1 (en) 2003-03-26

Similar Documents

Publication Publication Date Title
CN102851120A (zh) 一种艾纳香油的提取方法
CN103451022A (zh) 一种从江香薷中综合提取挥发油、多糖和黄酮的方法
CN105001992B (zh) 一种利用卡箍快装的小型精油及纯露提取设备
CN1149018C (zh) 一种干馏山楂核以提取汁液的新方法及设备
CN105733809A (zh) 一种低温蒸馏生产茉莉花纯露的方法及其设备
CN104258594A (zh) 一种高效萃取植物有效成分的方法
CN2427978Y (zh) 一种干馏山楂核以提取汁液的设备
CN211532065U (zh) 一种马铃薯育种用栽培装置
CN216457025U (zh) 茶叶低温萃取***
CN1742636B (zh) 一种无公害液体香烟的生产工艺
CN204951680U (zh) 艾纳香的加工提取设备
CN205995829U (zh) 一种用于溪黄草的清洗烘干装置
CN106810591B (zh) 一种从甘草中提取甘草酸的设备
CN101519607A (zh) 一种利用制炭废气采集分离提纯清洁新能源的方法及装置
CN210419888U (zh) 一种植物精油提取装置
CN204841026U (zh) 中药提取罐
CN207918781U (zh) 一种用于油脂提炼的脱酸脱臭塔
CN2745367Y (zh) 山楂果核原液提取的新技术设备
CN205389385U (zh) 一种便携式蔬菜种子催芽装置
CN104906161B (zh) 艾纳香的加工提取设备
CN107969732B (zh) 生物组合物及其制备方法
CN110721210A (zh) 一种刺五加茎皮黄酮提取工艺及其应用
CN205586665U (zh) 一种生物医药提取装置
CN215232151U (zh) 一种节能环保香料浓缩罐
CN216890852U (zh) 一种用于天然香料生产的蒸汽回收装置

Legal Events

Date Code Title Description
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C06 Publication
PB01 Publication
C57 Notification of unclear or unknown address
DD01 Delivery of document by public notice

Addressee: Shi Yi

Document name: Notice of first review

C14 Grant of patent or utility model
GR01 Patent grant
C57 Notification of unclear or unknown address
DD01 Delivery of document by public notice

Addressee: Shi Yi

Document name: Notification of Termination of Patent Right

C19 Lapse of patent right due to non-payment of the annual fee
CF01 Termination of patent right due to non-payment of annual fee
REG Reference to a national code

Ref country code: HK

Ref legal event code: GR

Ref document number: 1043442

Country of ref document: HK