CN110117422A - A kind of formula and extraction process of the orange pigment of composite natral - Google Patents
A kind of formula and extraction process of the orange pigment of composite natral Download PDFInfo
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- CN110117422A CN110117422A CN201810116242.5A CN201810116242A CN110117422A CN 110117422 A CN110117422 A CN 110117422A CN 201810116242 A CN201810116242 A CN 201810116242A CN 110117422 A CN110117422 A CN 110117422A
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- pigment
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Classifications
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L5/00—Preparation or treatment of foods or foodstuffs, in general; Food or foodstuffs obtained thereby; Materials therefor
- A23L5/40—Colouring or decolouring of foods
- A23L5/42—Addition of dyes or pigments, e.g. in combination with optical brighteners
- A23L5/43—Addition of dyes or pigments, e.g. in combination with optical brighteners using naturally occurring organic dyes or pigments, their artificial duplicates or their derivatives
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0033—Blends of pigments; Mixtured crystals; Solid solutions
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0083—Solutions of dyes
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The invention discloses a kind of formulas of the orange pigment of composite natral, are made of following material composition: 250 grams of beet root, 100 grams of Yellow Fructus Gardeniae, peeling 25 grams of lemon, 1500 grams of water；Normal juice weight: beet root 45%-47%, Yellow Fructus Gardeniae 55%-59%；Weight after concentration: beet root 25%, Yellow Fructus Gardeniae 24%.Formula is scientific and reasonable for this, does not add pigment, all using natural food materials, and draws materials conveniently.Comprise the steps of: beet root cleans silt, and without peeling, 100 mesh dusting covers of squeezing the juice together with the lemon of peeling after drying are put into after being boiled by fire in pot and are concentrated into recipe requirements weight with small fire, take the top net portion spare after natural sedimentation；Yellow Fructus Gardeniae adds 7 times of water of own wt, is boiled with soft fire after being boiled by fire 10 minutes, bored 20 minutes be sieved, continue to be boiled with soft fire after boiling to the 1/3 of original volume to thick state with high fire, take within last natural sedimentation at least 60 minutes above net portion it is spare.The beet red pigment extracted is uniformly mixed with Gardenia Yellow be packed into the dark Ethereal oil bottle sterilized orange natural pigment.
Description
Technical field
The present invention relates to edible pigment field, more specifically for, in particular to a kind of orange pigment of composite natral is matched
Side and extraction process.
Background technique
Natural pigment is the edible pigment obtained by natural resources.Mainly from animal and plant tissue and microorganism (culture)
The pigment of middle extraction, wherein vegetalitas colorant occupies the majority.Natural pigment not only has the function of to food color, moreover, phase
When part natural pigment has physiological activity.
It is edible from the natural pigment of the root of natural plants, stem, leaf, flower, fruit and animal, microorganism etc.
Pigment is known as edible natural pigment, the ratio very little accounted in food from edible pigment from additive amount, generally product, drink
The some thousandths of of material, drinks, cake, candy, medicine etc., ten thousand/it is several even 100,000/several.Although natural pigment is extensive
It is allowed as edible pigment, but various countries are not identical to the definition of natural food colour and license situation, some substances are recognized
It is set to fragrance and non-pigmented, therefore many spices are not identified as pigment.By taking Sweden as an example, which assert turmeric, capsicum, hiding
Safflower and sandalwood not instead of pigment, spice.The alimentary codex of other such as Italy, Holland, Switzerland and states, Norway is all
There is similar regulation.
The exploitation of natural pigment (NaturalPigments) becomes every profession and trade scientific worker common concern with using oneself
Project.Be attempted to obtain natural pigment from various animal and plant resources, while exploring its physiological activity, come alleviate and solve by
Various problems brought by synthetic dyestuff.But since natural pigment color is unstable, it is easy in its use process by various
The influence of factor (such as illumination, temperature, oxidation, pH value, medium polarity, metal ion, additive) and occur fade, discoloration etc.
The variation of aspect, and its coloring effect is influenced, seriously constrain the process that natural pigment replaces synthetic food color.
Natural pigment is typically derived from natural component, such as beet red, grape and capsicum, these food have been obtained extensively
Therefore the recognition and acceptance of big consumer can more obtain the favor of consumer using the natural pigment of these food sources, use
Get up also more safer.It is most of to derive from phytochrome.
For some products due to using natural pigment, appearance has just lacked some artificial factors, therefore closer to natural
Form, to attract more consumers.Nowadays in European Union, natural pigment not only robs the market for accounting for synthetic dyestuff, but also
Also the market for accounting for some pigment extracts is robbed.
Natural food colour can be artificial synthesized by directly extracting, biotechnology production, but it is artificial synthesized with it is biological
Technology production has certain limitation in production application, so current natural food colour is produced with direct extraction method
Based on.Natural food colour need to be extracted in a manner of extracting by different solvents when extracting natural food colour, or
Natural pigment is extracted with the mode of enzymatic hydrolysis, also the method for useful supercritical fluid extraction extracts natural pigment, more useful ultrasonic wave
Extraction method extracts natural pigment.The mode of the natural pigment purifying extracted has a macroreticular resin absorbing method, gel chromatography partition method,
Membrane technology partition method, high-speed countercurrent chromatography.Although there are many extract natural food colour and purifying natural edible pigment
Mode, but not can avoid the work for needing that extraction and purification could be completed by very more chemical reagent auxiliary.Not only set
It is standby to take up a large area at high cost and strongly professional, all unusual height of the human cost and time cost spent.
Alternative edible pigment is very more on the market, not only have it is domestic also have import, but with consumer
Gradually the understanding of diet and healthy relationship is deepened, food-safe attention degree is continuously improved, and follows for more and more
It is naturally no added to like close to for the crowd of the Nature, it is vivid to want to purchase or oneself extract really no added
Natural food colour, to make health delicious food.The formula and extraction process for the compound orange pigment that the present invention announces be
A method of no added natural food colour being extracted from natural food materials with the mode of physics, at the same also disclose extraction after
The use reference quantity of natural food colour, the application data in practical baked product.It can not only produce various in riotous profusion more
Color food, more healthy bonus point.
Summary of the invention
To solve above directly to extract that orange pigment needs chemical reagent and artificial synthesized orange pigment and biotechnology are raw
The problems such as producing the limitation of orange pigment, the invention discloses the formulas and extraction process of a kind of orange pigment of composite natral, no
The method for adding any chemical substance physics extracts the orange pigment of composite natral by medium of clear water from raw material, and solves
It has determined the problem of citraurin cannot be directly extracted from food materials.
To achieve the goals above, the invention discloses a kind of formula of the orange pigment of composite natral, by following raw material at
It is grouped as: 250 grams of beet root, 100 grams of Yellow Fructus Gardeniae, peeling 25 grams of lemon, 1500 grams of water；
Normal juice weight: beet root 45%-47%, Yellow Fructus Gardeniae 55%-59%；
Weight after concentration: beet root 25%, Yellow Fructus Gardeniae 24%.
Formula is scientific and reasonable for this, does not add pigment, all using natural food materials, and draws materials conveniently.
The invention also discloses a kind of extraction processes of the orange pigment of composite natral, comprise the steps of:
Pretreatment: sterilizing dark Ethereal oil bottle, after cleaning up Ethereal oil bottle, bottleneck drain well and cleaned downward
Bottle cap of dropper, which is put into togerther in 80 degree of disinfection cabinet, to be sterilized at least 60 minutes, it is ensured that all moisture content evaporating completelies in Ethereal oil bottle.
1) beet root cleans silt, and without peeling, 100 mesh dusting covers of squeezing the juice together with the lemon of peeling after drying are put into
It is concentrated into recipe requirements weight with small fire after being boiled by fire in pot, takes the top net portion spare after natural sedimentation；
2) Yellow Fructus Gardeniae adds 7 times of water of own wt, is boiled with soft fire after being boiled by fire 10 minutes, is sieved within bored 20 minutes, uses high fire
Continue to be boiled with soft fire after boiling to the 1/3 of original volume to thick state, take within last natural sedimentation at least 60 minutes above net portion it is standby
With.
3) the beet red pigment extracted is uniformly mixed to the dark Ethereal oil bottle for being packed into and sterilizing with Gardenia Yellow i.e.
At orange natural pigment.
Post-processing: bottleneck, which is wrapped tinfoil and is put into 80 DEG C preheated of oven, sterilize 30 minutes, is covered after cooling down completely
Bottle cap is put into seal box and is finished in stored refrigerated 30 days.Health is paid attention to during use, and trickle irrigation be not infected with any
Raw material, especially cream etc. have the raw material of grease, using finish be immediately placed in refrigerator cold-storage save, especially day heat when
It waits, if it find that having mildew on the silica gel cover expansion of Ethereal oil bottle or dropper, all not be further continued for washing using natural pigment
Clean bottle does disinfection again, extracts the orange pigment of composite natral again, sterilizes again, guarantee the quality of pigment.
Points for attention: the Yellow Fructus Gardeniae place of production is Bozhou, and the beet root place of production is the north.The selection of raw material please in regular pharmacy or
Person shop purchase, to guarantee the fresh and quality of food materials.Also colour-fast during high-temperature baking；If answered in cold production
With with good stability.
The extraction process does not add artificial chemistry preparation, does not need professional equipment, simple, easy to learn, practical.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the beet root
Juice drains the juice in root when being sieved, to guarantee the concentration of beet root juice.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the container boiled is used
Material be stainless steel, glass, ceramics, do not glue, cannot with aluminium, iron material because metal ion will affect pigment in food materials
Stablize generate color change.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: do not add any
The method of chemical substance physics is extracted from raw material using clear water as medium.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the invention is created
Orange pigment be not illuminated by the light and caused by air oxidation colour fading and discoloration problem.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: because making
In the process without addition artificial chemistry preparation, the original flavor of food materials is remained.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the invention is created
Orange pigment can avoid because high-temperature heating caused by color change, it is with good stability.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the invention is created
Orange pigment preserving type must be 3-5 DEG C stored refrigerated, and using finishing in one month.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: if bored 20
Discovery moisture content did not have food materials before minute, then we are just again plus a part of water, guarantee allows more pigmentolysis to water
In, it is boiled by fire again, and bored 20 minutes.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the weight after sieving
Data are measured less than theoretical weight, when needing to check separation dry and wet food materials, if completely squeeze out Normal juice, or bored
Forget to close fire in the process, continuous heating causes water loss excessive.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the liquid in pot
When body is concentrated to the 1/3 of only original volume, the duration and degree of heating is needed to be grasped, if fire temperature is very high and leaves tens seconds, having very much can
It will can cause to be sticking because of evaporation is too fast.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: in the mistake of precipitating
Preservative film or lid are not covered in journey, prevent the vapor generated in cooling procedure from falling into bowl.
A kind of formula and extraction process of the orange pigment of composite natral as described above, it is characterised in that: the invention is created
Orange pigment based on the Gardenia Yellow class and betanin of the crocin of terpene and flavonoids.
Compared with the existing technology, the beneficial effects of the present invention are:
Without using synthetic food color, the safety of food is improved, the production method is simple, easy to learn, practical, materials side
Just, production of being in may be implemented.The method for not adding any chemical substance physics is extracted from raw material using clear water as medium
The technique of the orange pigment of composite natral solves the problems, such as directly extract citraurin from food materials.
Specific embodiment
Embodiment
Dark Ethereal oil bottle is sterilized, after cleaning up Ethereal oil bottle, bottleneck drain well and cleaned bottle cap of dropper downward
It is put into togerther in 80 degree of disinfection cabinet and sterilizes at least 60 minutes, it is ensured that all moisture content evaporating completelies in Ethereal oil bottle.
Beet root cleans silt, without peeling, filter soy-bean milk gauze 100 of squeezing the juice together with the lemon of peeling after drying
Mesh dusting cover is put into after being boiled by fire in stainless-steel pan and is concentrated into recipe requirements weight with small fire, takes after natural sedimentation pure topmost
Net part is spare；
Yellow Fructus Gardeniae adds 7 times of water of own wt, is put into after being boiled by fire in stainless-steel pan and is boiled with soft fire 10 minutes, and bored 20 minutes
Sieving, continues to be boiled with soft fire after boiling to the 1/3 of original volume to thick state, take above within last natural sedimentation at least 60 minutes with high fire
Net portion is spare；
The beet red pigment extracted is uniformly mixed with Gardenia Yellow be packed into sterilized dark Ethereal oil bottle orange
Color natural pigment.
Using finish be immediately placed in refrigerator cold-storage save, especially day heat when, if it find that the silica gel lid of Ethereal oil bottle
There is mildew on son expansion or dropper, all not be further continued for using natural pigment, wash clean bottle does disinfection again, weight
It is new to extract the orange pigment of composite natral, it sterilizes again, guarantees the quality of pigment.
The embodiment of the present invention is explained in detail above, but the invention is not limited to above-mentioned embodiment party
Formula, in the knowledge of one skilled in the relevant art, the present invention can also make many variations.It is all for of the invention special
Inside the protection scope of benefit.
Claims (5)
1. a kind of formula and extraction process of the orange pigment of composite natral, it is characterised in that: be made of following material composition: beet
250 grams of root, 100 grams of Yellow Fructus Gardeniae, peeling 25 grams of lemon, 1500 grams of water.
2. a kind of formula and extraction process of the orange pigment of composite natral, which is characterized in that comprise the steps of:
1) beet root cleans silt, and without peeling, 100 mesh dusting covers of squeezing the juice together with the lemon of peeling after drying are put into pot
It is concentrated into recipe requirements weight with small fire after being boiled by fire, takes the top net portion spare after natural sedimentation；
2) Yellow Fructus Gardeniae adds 7 times of water of own wt, is boiled with soft fire after being boiled by fire 10 minutes, is sieved within bored 20 minutes, is continued with high fire
Be boiled with soft fire after boiling to the 1/3 of original volume to thick state, take within last natural sedimentation at least 60 minutes above net portion it is spare.
3) the beet red pigment extracted is uniformly mixed with Gardenia Yellow be packed into the dark Ethereal oil bottle sterilized orange
Color natural pigment.
3. the formula and extraction process of the orange pigment of a kind of composite natral according to claim 1, which is characterized in that described
The material of container is stainless steel, glass, ceramics, does not glue, and the material of aluminium, iron cannot be used, because metal ion will affect food materials
Stablizing for middle pigment generates color change.
4. the formula and extraction process of the orange pigment of a kind of composite natral according to claim 1, which is characterized in that described
The method for not adding any chemical substance physics in formula is extracted from raw material using clear water as medium.
5. the formula and extraction process of the orange pigment of a kind of composite natral according to claim 1, which is characterized in that described
Color change caused by orange pigment can avoid because of high-temperature heating, it is with good stability.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810116242.5A CN110117422A (en) | 2018-02-06 | 2018-02-06 | A kind of formula and extraction process of the orange pigment of composite natral |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810116242.5A CN110117422A (en) | 2018-02-06 | 2018-02-06 | A kind of formula and extraction process of the orange pigment of composite natral |
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| Publication Number | Publication Date |
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| CN110117422A true CN110117422A (en) | 2019-08-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810116242.5A Pending CN110117422A (en) | 2018-02-06 | 2018-02-06 | A kind of formula and extraction process of the orange pigment of composite natral |
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Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101020788A (en) * | 2007-03-09 | 2007-08-22 | 陈义 | Prepn process of natural botanic food color |
| EP2096146A1 (en) * | 2008-02-29 | 2009-09-02 | San-Ei Gen F.F.I., Inc. | Deodorized plant pigment derived from Ipomoea Batatas |
| CN101838478A (en) * | 2010-05-27 | 2010-09-22 | 河南中大生物工程有限公司 | Natural pigment composition and preparation method thereof |
| CN102993769A (en) * | 2012-12-24 | 2013-03-27 | 晨光生物科技集团股份有限公司 | Method for improving color tone of beet red pigment |
| CN104320979A (en) * | 2012-04-19 | 2015-01-28 | 伊比西(北京)植物药物技术有限公司 | Compositions comprising a combination of at least one colorant and at least one polysaccharide |
| CN104327133A (en) * | 2014-10-15 | 2015-02-04 | 浙江天露生物科技有限公司 | Gardenia jasminoides effective component comprehensive extraction technology |
| CN104448924A (en) * | 2013-09-22 | 2015-03-25 | 青岛中人智业生物科技有限公司 | Natural pigment composition |
| CN105255214A (en) * | 2014-07-18 | 2016-01-20 | 周子童 | Natural pigment composition |
-
2018
- 2018-02-06 CN CN201810116242.5A patent/CN110117422A/en active Pending
Patent Citations (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101020788A (en) * | 2007-03-09 | 2007-08-22 | 陈义 | Prepn process of natural botanic food color |
| EP2096146A1 (en) * | 2008-02-29 | 2009-09-02 | San-Ei Gen F.F.I., Inc. | Deodorized plant pigment derived from Ipomoea Batatas |
| CN101838478A (en) * | 2010-05-27 | 2010-09-22 | 河南中大生物工程有限公司 | Natural pigment composition and preparation method thereof |
| CN104320979A (en) * | 2012-04-19 | 2015-01-28 | 伊比西(北京)植物药物技术有限公司 | Compositions comprising a combination of at least one colorant and at least one polysaccharide |
| CN102993769A (en) * | 2012-12-24 | 2013-03-27 | 晨光生物科技集团股份有限公司 | Method for improving color tone of beet red pigment |
| CN104448924A (en) * | 2013-09-22 | 2015-03-25 | 青岛中人智业生物科技有限公司 | Natural pigment composition |
| CN105255214A (en) * | 2014-07-18 | 2016-01-20 | 周子童 | Natural pigment composition |
| CN104327133A (en) * | 2014-10-15 | 2015-02-04 | 浙江天露生物科技有限公司 | Gardenia jasminoides effective component comprehensive extraction technology |
Non-Patent Citations (1)
| Title |
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| 王威: "常用天然色素抗氧活性的研究 ", 《食品科学》 * |
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Application publication date: 20190813 |