CN109157443B - Tremella mask - Google Patents
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- CN109157443B CN109157443B CN201811260145.XA CN201811260145A CN109157443B CN 109157443 B CN109157443 B CN 109157443B CN 201811260145 A CN201811260145 A CN 201811260145A CN 109157443 B CN109157443 B CN 109157443B
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9728—Fungi, e.g. yeasts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0212—Face masks
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/64—Proteins; Peptides; Derivatives or degradation products thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/676—Ascorbic acid, i.e. vitamin C
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/67—Vitamins
- A61K8/678—Tocopherol, i.e. vitamin E
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9771—Ginkgophyta, e.g. Ginkgoaceae [Ginkgo family]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9789—Magnoliopsida [dicotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9783—Angiosperms [Magnoliophyta]
- A61K8/9794—Liliopsida [monocotyledons]
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/004—Aftersun preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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Abstract
The invention relates to the technical field of daily chemical masks, and particularly relates to a tremella mask. The tremella mask comprises a mask paper carrier and a mask liquid, wherein the mask paper carrier is prepared from tremella superfine powder and alcohol-soluble protein; the mask liquid is prepared from potato powder, honeysuckle extract, vitamin C, vitamin E, ginkgo leaf extract, aloe extract, preservative, water-soluble essence and deionized water. The facial mask paper carrier of the tremella facial mask is environment-friendly and degradable, has good affinity with skin and good pasting performance, has high moisture retention and excellent adsorption performance, and also has the beautifying effect of tremella; the facial mask liquid of the tremella facial mask has the remarkable effects of moisturizing, whitening, resisting aging and preventing radiation, has excellent adsorption performance, is matched with a facial mask paper carrier, can well lock the facial mask liquid, and is convenient to use.
Description
Technical Field
The invention relates to the technical field of daily chemical masks, and particularly relates to a tremella mask.
Background
With the increase of income level of female consumers in China, the concept of skin care is more and more rich and mature, the consumption concept of the facial mask is changed day by night, and the frequency of using the facial mask is increased. As analyzed by many experts in the industry, the improvement of consumer's ability, the transformation of consumer concept, the increase of skin care demand, and the considerable profit of facial masks, etc. all become catalysts for the rapid development of the industry. In recent years, with the new concept of a cheap single mask, the positioning of high-grade skin care products of the mask is broken, the product subdivision is accelerated, and new brands are continuously appeared. The mask is known to be the fourth major cosmetic consumer product, and from 2001 to 2009, the mask is the highest one of the sub-categories of skin care products, and the sales of the mask market from 2010 to 2015 show a trend of continuous increase. Compared with the essence skin care products with more functions, the facial mask emphasizes intensive care, and the requirements of moisturizing, whitening and freckle removing are the greatest requirements, particularly the requirements of moisturizing exist every day. Due to this consumer environment, mask products are gradually being targeted as daily necessities in skin care products, with great market potential.
The facial mask paper is a carrier of facial mask functional components, the quality of the facial mask paper is very important, the beauty and skin care facial masks in the current market are basically manufactured by adopting chemical synthetic fiber non-woven fabrics or artificial fiber non-woven fabrics through the working procedures of folding, bagging, injecting soak solution, sealing and the like, the complex operation of a soft film is greatly simplified, customers can conveniently care at home, the price is close to the people and is easier to accept by users, the cloth facial masks bring certain beauty and skin care effects to consumers, but the facial mask paper has the defects in beauty, and the problems are as follows: (1) synthetic fiber non-woven fabrics or artificial fiber non-woven fabrics all generally have the degradation problem, and can not recycle, easily cause environmental pollution after the consumer uses. (2) The synthetic fiber non-woven fabric or artificial fiber non-woven fabric substrate facial mask reduces the using effect of the facial mask and is easy to cause the allergic phenomenon of consumers because the fiber of the non-woven fabric and the adhesive are partially dissolved after being soaked in the soaking solution for a long time. (3) The mask with the synthetic fiber non-woven fabric or the artificial fiber non-woven fabric substrate is characterized in that the soaking solution is thickened by the high molecular synthetic resin, so that a consumer feels tight after using the mask, and feels comfortable after cleaning. (4) The mask with the synthetic fiber non-woven fabric or artificial fiber non-woven fabric substrate has the advantages that nutrient substances and a large amount of moisture exist in the soak solution, and microorganisms and bacteria are easily generated, so the shelf life of the mask is directly influenced, and particularly the effective period of bioactivity is directly influenced. (5) The non-woven fabric mask has poor affinity with skin, is only a carrier of essence, has a high transdermal absorption rate of nutrient components in the essence, and is not ideal in effect, and the non-woven fabric mask has a 'back absorption' phenomenon. (6) The mask paper made of terylene and blended non-woven fabrics has good tensile property, but poor hygroscopicity, is difficult to lock a large amount of nutrient water, and the nutrient water seeps out and flows down greatly when being stuck on the face, thereby causing serious waste and reducing the using effect of the mask.
Disclosure of Invention
In order to overcome the defects, the invention aims to provide the tremella mask, the mask paper carrier of the tremella mask is environment-friendly and degradable, the affinity with skin is good, the face pasting performance is good, the tremella mask has high moisture retention and excellent adsorption performance, and in addition, the tremella mask also has the beautifying effect; the facial mask liquid of the tremella facial mask has the remarkable effects of moisturizing, whitening, resisting aging and preventing radiation, has excellent adsorption performance, is matched with a facial mask paper carrier, can well lock the facial mask liquid, and is convenient to use.
In order to achieve the purpose, the technical scheme of the invention is as follows:
a tremella mask comprises a mask paper carrier and a mask liquid, wherein the mask paper carrier is prepared from tremella superfine powder and prolamin; the mask liquid is prepared from potato powder, honeysuckle extract, vitamin C, vitamin E, ginkgo leaf extract, aloe extract, preservative, water-soluble essence and deionized water.
The tremella polysaccharide is the most important medicinal component of tremella, and is an important bioactive substance, and modern science proves that the tremella polysaccharide can improve the immunologic function of a human body, enhance the macrophage function, and also has the function of improving leucocytes, and the tremella polysaccharide can reduce blood pressure and blood fat, prevent arteriosclerosis, inhibit tumors, enhance the immunologic function of an organism, and has the effects of delaying senility and protecting skin after being taken for a long time. Research shows that the tremella polysaccharide has certain capacity of eliminating hydroxyl free radicals and can be used as an anti-aging component to be applied to cosmetics; the tremella polysaccharide has better moisturizing effect than glycerin and trehalose, and can be used as a moisturizing component to be applied to cosmetics; the tremella polysaccharide has radioprotective effect, and the number of nucleated cells in bone marrow of patients treated with Co60 radiation is 186% more than that of control group without tremella polysaccharide. At present, the tremella polysaccharide is added into a plurality of high-grade cosmetics at home and abroad as an effective component. The invention adopts the tremella superfine powder, does not destroy the effective ingredients in the tremella, and improves the bioavailability of the tremella.
Prolamin is one of the components of plant seed storage protein, is insoluble in water and soluble in 50% -90% ethanol. Prolamins have been discovered as early as the end of the 18 th century, and their presence has been found in plant seeds such as corn and wheat. The alcohol soluble protein has rich sources and relatively low market price. Because the protein is composed of amino acid sequences, the fabric has skin-friendly property equivalent to cotton cloth, is biodegradable, has the functions of oxidation resistance, ultraviolet resistance, fragrance retention, oil impermeability, bacteriostasis and the like, and the alcohol soluble protein has elasticity and can realize better veneering after being spun into a non-woven film.
The tremella facial mask is prepared from potato powder, honeysuckle extract, vitamin C, vitamin E, ginkgo leaf extract, aloe extract, preservative, water-soluble essence and deionized water.
The potato has rich sources and low price, has good effects of caring skin and maintaining beauty, has obvious whitening effect, has good effect of removing color spots on the skin such as sunburn, suntan and the like, and has no side effect. Meanwhile, the content of vitamins in the potatoes is the most abundant in all food crops, and the potatoes contain a substance called polyphenol, so that the substances can inhibit the damage of free radicals to elastic fibers of skin, and the skin which is dark, yellow and lack of vitality is full of elasticity and healthy luster again. The potato flour of the present invention may be obtained commercially or prepared by itself by methods known in the art.
Modern researches prove that the honeysuckle extract contains pharmacological active ingredients such as chlorogenic acid and luteolin glycoside, and the chlorogenic acid and derivatives thereof have stronger free radical scavenging effect than ascorbic acid (vitamin C), caffeic acid and tocopherol (vitamin E), can effectively scavenge DPPH free radicals, hydroxyl free radicals and superoxide anion free radicals, and can inhibit the oxidation of low-density lipoprotein. Chlorogenic acid has important effects in effectively scavenging free radicals in vivo, maintaining normal structure and function of body cells, and preventing and delaying tumor mutation and aging. The eucommia chlorogenic acid contains a special component which can promote the synthesis and decomposition of collagen in skin, bones and muscles of a human body, and has the functions of promoting metabolism and preventing decline. Therefore, chlorogenic acid is often used as a raw material for medicines, health products and cosmetics. The honeysuckle extract of the present invention can be obtained commercially or extracted by itself by methods of the prior art that have been disclosed.
Vitamin C, which is a component added in most whitening products, is considered to have the whitening effect because the vitamin C can help the skin to resist the ultraviolet ray and avoid the generation of black spots and freckles.
The vitamin E can eliminate free radicals, protect skin tissues and care the skin, so that the skin does not have the condition of fine lines and looseness in the early stage. Can also promote the circulation of skin micro-vessels, so that the blood in the skin is always bright and clean, and the face looks natural, ruddy and active.
Folium Ginkgo contains natural active flavone and ginkgolide, has effects of dissolving cholesterol, dilating blood vessel, and improving brain function disorder, arteriosclerosis, hypertension, giddiness, tinnitus, headache, senile dementia, hypomnesis, etc. Ginkgo was listed as royal tribute in ancient times. The flavonoid glycoside and amino acid components in folium Ginkgo can inhibit melanin growth, and keep skin luster and elasticity. The folium Ginkgo extractive solution is also an antioxidant, and can reduce free radical damage to skin, reduce lipid peroxidation level, reduce freckle, moisten skin, and care skin. Meanwhile, the skin microcirculation can be improved, the skin is prevented from being dry and yellow, and the skin can be made tender and white. The ginkgo leaf extract contains a plurality of flavonoid compounds, and the current research shows that the ginkgo leaf extract has a certain radiation resistance effect. The ginkgo leaf extract can be obtained commercially or extracted by the methods disclosed in the prior art, such as the method disclosed in the patent with the application number of 201110185794. X.
Aloe is called Luhui, Liliaceae, Aloe genus. Perennial evergreen plants, large and thick leaves, outgrowth, and clumping. The juice extracted from the leaves can be used as the medicine. Aloe is bitter in taste and cold in nature. The aloe contains anthraquinone derivatives, aloe rhubarb, saponin, amino acids and polysaccharide. Aloe has effects of nourishing, moisturizing and preventing sunburn, so it is widely used in moisturizing and wrinkle removing cosmetics such as cream, milky lotion, facial cleanser, facial mask, etc. The current research proves that aloe polysaccharide and aloe anthraquinone substances which are functional components of aloe have obvious radiation protection effect, and animal living body experiments prove that the aloe polysaccharide can relieve the discomfort symptoms of animal living bodies after receiving radiation irradiation, and obviously improve the tolerance capability and survival rate of the aloe polysaccharide to the radiation. The aloe anthraquinone has effects of resisting oxidation, scavenging free radical, diminishing inflammation, killing bacteria, and regulating cytokine secretion. The radiation protection principle of aloe anthraquinone substances is mainly related to the capabilities of diminishing inflammation, resisting oxidation, inhibiting inflammatory reaction and the like. The aloe vera extract of the present invention may be obtained commercially or may be extracted by itself using methods known in the art, such as the method disclosed in the referenced application No. 200910184679.3.
Further, the tremella facial mask is characterized in that the facial mask paper carrier is prepared from, by weight, 3-7 parts of tremella superfine powder and 10-15 parts of alcohol-soluble protein.
Further, the tremella facial mask is characterized in that the facial mask paper carrier is prepared from 5 parts by weight of tremella superfine powder and 12 parts by weight of prolamin.
Further, the particle size of the tremella ultra-fine powder is 1000-2000 meshes.
Further, in the tremella facial mask, the alcohol-soluble protein is wheat alcohol-soluble protein and/or zein.
Further, the preparation method of the tremella superfine powder comprises the following steps: removing the culture medium from fresh tremella fuciformis, cleaning, drying the cleaned tremella fuciformis to enable the water content of the tremella fuciformis to be less than 15%, and crushing the tremella fuciformis for 10-30 minutes by using an ultrafine crusher to obtain tremella fuciformis ultrafine powder.
Further, the tremella facial mask is prepared by one or more of hot air drying at 50-60 ℃, microwave drying and infrared drying.
Further, the tremella facial mask is prepared from, by weight, 10-15 parts of potato powder, 3-11 parts of honeysuckle extract, 5-10 parts of vitamin C, 3-5 parts of vitamin E, 3-7 parts of ginkgo leaf extract, 3-5 parts of aloe extract, 1-5 parts of preservative, 1-5 parts of water-soluble essence and 60-80 parts of deionized water.
The invention also provides a preparation method of the tremella mask, and in order to achieve the purpose, the technical scheme of the invention is as follows:
the preparation method of the tremella mask comprises the following steps:
(1) preparation of facial mask paper carrier
Dissolving prolamin in an ethanol water solution to prepare a prolamin ethanol solution with the mass percent of prolamin being 10-20%, adding tremella superfine powder into the prolamin ethanol solution, and stirring until the tremella superfine powder is fully dissolved to obtain a mixed solution; preparing the obtained mixed solution into a nano-scale electrospun membrane by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain a tremella facial mask paper carrier;
(2) mixing potato powder with deionized water, gelatinizing in water bath, cooling, adding flos Lonicerae extract, vitamin C, vitamin E, folium Ginkgo extract, Aloe extract, antiseptic, and water soluble essence, and stirring to obtain facial mask solution;
(3) and (3) putting the facial mask paper carrier obtained in the step (1) into the facial mask liquid obtained in the step (2), soaking for 10-30 minutes, and making the facial mask liquid adsorb and/or permeate onto the facial mask paper carrier under the liquid absorption characteristic of the facial mask paper carrier to prepare the tremella facial mask.
Further, in the preparation method of the tremella mask, in the step (1), the volume fraction of the ethanol water solution is 50% -70%.
Further, in the preparation method of the tremella mask, in the step (1), a plasticizer with the mass fraction of 0.5-1.5% is added into the mixed solution.
Further, in the preparation method of the tremella mask, the plasticizer is glycerol.
The invention has the beneficial effects that: 1) the tremella mask has the advantages that the mask paper carrier is environment-friendly and degradable, the affinity with skin is good, the pasting performance is good, and the tremella mask has high moisture retention and excellent adsorption performance. 2) The tremella superfine powder and alcohol soluble protein used as raw materials for preparing the mask paper carrier are rich in sources, low in price and biodegradable, and cannot bring too much pressure to the environment after being used. 3) The alcohol soluble protein has the same skin-friendly property as cotton cloth, also has the functions of oxidation resistance, ultraviolet resistance, fragrance protection, oil impermeability, bacteriostasis and the like, and can realize better veneering after being spun into a non-woven film. 4) Tremella polysaccharide contained in Tremella is an important bioactive substance, has hydrophilicity, can be well adhered to skin, and has remarkable effects of moisturizing, whitening, resisting aging and preventing radiation. 5) The facial mask liquid of the tremella facial mask has the remarkable effects of moisturizing, whitening, resisting aging and preventing radiation, has excellent adsorption performance, is matched with a facial mask paper carrier, can well lock the facial mask liquid, and is convenient to use.
Detailed Description
The preferred embodiments of the present invention will be described in detail below with reference to specific embodiments. The examples are provided for better illustration of the present invention, but the present invention is not limited to the examples. Therefore, those skilled in the art should make insubstantial modifications and adaptations to the embodiments of the present invention in light of the above teachings and remain within the scope of the invention. Experimental methods without specific conditions noted in the examples or conditions as recommended by the manufacturer.
In the following specific examples of the present invention, the test materials used were:
the alcohol soluble protein is prepared by taking zein (Assay:morethan or equal to 92.0%) as an example: nanjing Tolya Biotechnology Ltd; absolute ethanol was analytically pure.
The preparation method of the tremella submicron powder comprises the following steps: removing the culture medium from fresh tremella fuciformis, cleaning, drying the cleaned tremella fuciformis to enable the water content of the tremella fuciformis to be less than 15%, and crushing the tremella fuciformis for 10-30 minutes by using an ultrafine crusher to obtain tremella fuciformis ultrafine powder.
In the following examples, potato flour, honeysuckle extract, vitamin C, vitamin E, ginkgo leaf extract and aloe extract were purchased commercially.
EXAMPLE 1 preparation of facial mask paper support
Preparing an ethanol solution with the volume fraction of 55%; and then adding 120g of zein into a certain amount of 55% ethanol solution, stirring until the zein is completely dissolved, preparing 15% zein ethanol solution by mass percent, adding 50g of tremella superfine powder with the particle size of 1500 meshes into the zein ethanol solution, stirring until the tremella superfine powder is completely dissolved, obtaining mixed solution, preparing the obtained mixed solution into a nano-scale electrospun membrane with the thickness of 0.05mm by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain the tremella facial mask paper carrier.
Example 2 preparation of a facial mask paper support
Preparing an ethanol solution with the volume fraction of 60%; adding 150g of zein into a certain amount of 55% ethanol solution, stirring until the zein is completely dissolved, preparing 15% zein ethanol solution by mass percent, adding 30g of tremella fuciformis ultra-fine powder with the particle size of 1500 meshes into the zein ethanol solution, stirring until the tremella fuciformis ultra-fine powder is completely dissolved, obtaining mixed solution, preparing the obtained mixed solution into a nano-scale electrospun membrane with the thickness of 0.05mm by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain the tremella fuciformis facial mask paper carrier.
EXAMPLE 3 preparation of facial mask paper support
Preparing an ethanol solution with the volume fraction of 70%; and then adding 100g of zein into a certain amount of 55% ethanol solution, stirring until the zein is completely dissolved, preparing 15% zein ethanol solution by mass percent, adding 70g of tremella superfine powder with the particle size of 1500 meshes into the zein ethanol solution, stirring until the tremella superfine powder is completely dissolved, obtaining a mixed solution, preparing the obtained mixed solution into a nano-scale electrospun membrane with the thickness of 0.05mm by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain the tremella facial mask paper carrier.
EXAMPLE 4 preparation of facial mask paper support
Preparing an ethanol solution with the volume fraction of 55%; adding 150g of zein into a certain amount of 55% ethanol solution, stirring until the zein is completely dissolved, preparing 15% zein ethanol solution by mass percent, adding 20g of tremella fuciformis ultra-fine powder with the particle size of 1500 meshes into the zein ethanol solution, stirring until the tremella fuciformis ultra-fine powder is completely dissolved, obtaining mixed solution, preparing the obtained mixed solution into a nano-scale electrospun membrane with the thickness of 0.05mm by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain the tremella fuciformis facial mask paper carrier.
EXAMPLE 5 preparation of facial mask paper support
Preparing an ethanol solution with the volume fraction of 55%; and adding 90g of zein into a certain amount of 55% ethanol solution, stirring until the zein is completely dissolved, preparing 15% zein ethanol solution by mass percent, adding 70g of tremella superfine powder with the particle size of 1500 meshes into the zein ethanol solution, stirring until the tremella superfine powder is completely dissolved to obtain mixed solution, preparing the obtained mixed solution into a nano-scale electrospun membrane with the thickness of 0.05mm by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain the tremella facial mask paper carrier.
EXAMPLE 6 preparation of facial mask paper support
Preparing an ethanol solution with the volume fraction of 55%; and then adding 120g of zein into a certain amount of 55% ethanol solution, stirring until the zein is completely dissolved, preparing 15% zein ethanol solution by mass percent, adding 50g of tremella ultrafine powder with the particle size of 1500 meshes into the zein ethanol solution, stirring until the tremella ultrafine powder is completely dissolved, obtaining mixed solution, adding 1% of glycerol by mass percent into the mixed solution, stirring and mixing uniformly, preparing a nano-scale electrospun membrane with the thickness of 0.05mm by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain the tremella facial mask paper carrier.
Example 7 efficacy verification of facial mask paper Carrier
The tremella facial mask paper carriers of examples 1-6 were respectively taken for the following efficacy verification.
(1) Adsorption experiment and elasticity experiment
Weighing the tremella facial mask paper carrier with the same weight, putting the tremella facial mask paper carrier into water, taking out the tremella facial mask paper carrier after 5 minutes, and weighing. Then the absorbed facial mask paper carrier is pulled with uniform force, and the deformation degree of the facial mask paper carrier is judged.
And (4) conclusion: the tremella facial mask paper carrier of example 5 had the best water absorption, followed by the tremella facial mask paper carriers of examples 1-3 and example 6, and the tremella facial mask paper carrier of example 4 had the worst water absorption. However, the tremella facial mask paper carrier of example 5, although having good water absorption, was easily deformed by pulling and was not easy to use. The tremella facial mask paper carrier of example 4 was not easily deformed, but had poor water absorption. The tremella facial mask paper carriers of examples 1-3 and example 6 have good water absorption and are not easy to deform after being pulled. In example 6, the glycerol serving as a plasticizer is added, so that the tremella facial mask paper carrier prepared in example 6 is higher in tensile resistance.
(2) Water retention test
Water retention test: the same weight of the tremella facial mask paper carrier after water absorption is weighed, and the change of the weight of the facial mask paper carrier along with time is measured (fixed condition: 25 ℃, 50% relative humidity).
And (4) conclusion: the evaporation rate of water in the tremella facial mask paper carrier of example 6 was the slowest, followed by the relatively fastest evaporation rates of water in the tremella facial mask paper carriers of examples 3, 1, 2, 5, and 4 in that order.
Therefore, the tremella mask paper carrier is not easy to shrink along with the change of humidity, so that the tremella mask paper carrier does not have a tight feeling when being applied to skin care products.
(3) Face-pasting property
Preparing facial mask liquid, wherein the facial mask liquid is prepared from 12g of potato powder, 8g of honeysuckle extract, 8g of vitamin C, 4g of vitamin E, 5g of ginkgo leaf extract, 4g of aloe extract, 3g of preservative, 2g of water-soluble essence and 70g of deionized water. Mixing potato powder with deionized water, gelatinizing in water bath, cooling, adding flos Lonicerae extract, vitamin C, vitamin E, folium Ginkgo extract, Aloe extract, antiseptic, and water soluble essence, and stirring to obtain facial mask liquid. And (3) respectively putting the facial mask paper carriers of the embodiments 1-6 into facial mask liquid, and soaking for 20 minutes to obtain the tremella facial mask.
The facial mask with good face-pasting property has good sealing property, and can further promote the absorption of nutrient components. The key points for detecting the fit of the mask are at the alar, chin and ear area. We chose 60 female subjects over 5 years old, age 28-42 years, using the mask. Groups were randomized into 6 groups of 10 people each. The tremella mask obtained as described above was used for 6 groups, and the fit at the side of the nose, chin, and ear area was evaluated to be very satisfactory 9-10, substantially satisfactory 7-9 (excluding 9), and less than unsatisfactory 7, and the results were averaged for each group as shown in table 1 below.
TABLE 1 results of evaluation of the adhesion
Group of | Face pack | Scoring |
Group 1 | Example 1 | 9.76 |
2 groups of | Example 2 | 9.58 |
Group 3 | Example 3 | 9.64 |
4 groups of | Example 4 | 6.88 |
5 groups of | Example 5 | 7.94 |
6 groups of | Example 6 | 9.87 |
(4) Evaluation of combination of facial mask paper carrier and facial mask liquid
According to the formula of each mask liquid in table 2, mask liquid A, B, C, D is prepared, and the preparation method comprises the following steps: mixing potato powder with deionized water, gelatinizing in water bath, cooling, adding flos Lonicerae extract, vitamin C, vitamin E, folium Ginkgo extract, Aloe extract, antiseptic, and water soluble essence, and stirring to obtain facial mask liquid.
And (3) taking 4 parts of the facial mask paper carrier in the example 1, respectively putting the facial mask paper carrier into the facial mask liquid A, B, C, D, and soaking for 20 minutes to obtain the tremella facial mask A, B, C, D. We chose 60 female subjects over 5 years old, age 28-42 years, using the mask. Randomized into 4 groups of 15 people each. And 4, respectively using the tremella mask A, B, C, D to observe whether the tremella mask is stuck on the face and whether a large amount of nutrient solution seeps out and flows down, so as to evaluate whether the mask paper carrier can well lock the mask solution after the combination of the mask paper carrier and the mask solution. No nutrient solution oozed out and flowed down for 9 to 10 minutes, a small amount of nutrient solution oozed out and flowed down for 7 to 9 minutes (excluding 9 minutes), and a large amount of nutrient solution oozed out and flowed down for 7 minutes or less, and then the groups were averaged, and the results are shown in table 3 below.
TABLE 2 formulation of each mask liquid
Facial mask liquid A | Mask liquid B | Mask liquid C | Facial mask liquid D | |
Dried potato powder | 10 | 13 | 20 | 8 |
Honeysuckle extract | 10 | 5 | 8 | 8 |
Vitamin C | 6 | 8 | 8 | 8 |
Vitamin E | 5 | 4 | 4 | 4 |
Ginkgo leaf extract | 4 | 6 | 5 | 5 |
Aloe extract | 3 | 5 | 4 | 4 |
Preservative | 2 | 1 | 3 | 3 |
Water-soluble essence | 2 | 2 | 2 | 2 |
Deionized water | 70 | 80 | 70 | 70 |
TABLE 3 evaluation results of the combination of facial mask paper carrier and facial mask liquid
Tremella face mask | Facial mask liquid | Scoring |
A | A | 9.96 |
B | B | 9.92 |
C | C | 6.64 |
D | D | 7.88 |
Finally, the above embodiments are only for illustrating the technical solutions of the present invention and not for limiting, although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that modifications or equivalent substitutions may be made to the technical solutions of the present invention without departing from the spirit and scope of the technical solutions of the present invention, and all of them should be covered in the claims of the present invention.
Claims (7)
1. The tremella mask is characterized by comprising a mask paper carrier and a mask liquid, wherein the mask paper carrier is prepared from 5 parts by weight of tremella superfine powder and 12 parts by weight of prolamin; the mask liquid is prepared from 10-15 parts of potato powder, 3-11 parts of honeysuckle extract, 5-10 parts of vitamin C, 3-5 parts of vitamin E, 3-7 parts of ginkgo leaf extract, 3-5 parts of aloe extract, 1-5 parts of preservative, 1-5 parts of water-soluble essence and 60-80 parts of deionized water.
2. The tremella mask as claimed in claim 1, wherein the particle size of the tremella ultra-fine powder is 1000-2000 mesh.
3. The tremella mask as claimed in claim 1, wherein the prolamin is wheat prolamin and/or zein.
4. The method for preparing the tremella mask as claimed in any one of claims 1 to 3, comprising the steps of:
(1) preparation of facial mask paper carrier
Dissolving prolamin in an ethanol water solution to prepare a prolamin ethanol solution with the mass percent of prolamin being 10-20%, adding tremella superfine powder into the prolamin ethanol solution, and stirring until the tremella superfine powder is fully dissolved to obtain a mixed solution; preparing the obtained mixed solution into a nano-scale electrospun membrane by using an electrostatic spinning technology, rinsing with water to remove ethanol, and drying to obtain a tremella facial mask paper carrier;
(2) mixing potato powder with deionized water, gelatinizing in water bath, cooling, adding flos Lonicerae extract, vitamin C, vitamin E, folium Ginkgo extract, Aloe extract, antiseptic, and water soluble essence, and stirring to obtain facial mask solution;
(3) and (3) putting the facial mask paper carrier obtained in the step (1) into the facial mask liquid obtained in the step (2), soaking for 10-30 minutes, and making the facial mask liquid adsorb and/or permeate onto the facial mask paper carrier under the liquid absorption characteristic of the facial mask paper carrier to prepare the tremella facial mask.
5. The preparation method of the tremella mask as claimed in claim 4, wherein in the step (1), the volume fraction of the ethanol aqueous solution is 50% -70%.
6. The preparation method of the tremella mask as claimed in claim 4, wherein in the step (1), a plasticizer is further added into the mixed solution, wherein the plasticizer is added into the mixed solution, and the mass fraction of the plasticizer is 0.5-1.5%.
7. The method for preparing the tremella mask as claimed in claim 6, wherein the plasticizer is glycerin.
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CN103405380A (en) * | 2013-09-06 | 2013-11-27 | 重庆市中药研究院 | White fungus skin-care composition and application thereof |
CN104983624A (en) * | 2015-06-29 | 2015-10-21 | 南阳市汇博生物技术有限公司 | Repairing skin-protecting nourishing mask impregnation liquid and preparation method thereof |
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CN103099761A (en) * | 2011-11-14 | 2013-05-15 | 廖琦 | Acne removal mask and preparation method thereof |
CN106880552A (en) * | 2017-03-07 | 2017-06-23 | 中山市帝芙尼美容美发有限公司 | Beauty mask and preparation method thereof |
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CN103405380A (en) * | 2013-09-06 | 2013-11-27 | 重庆市中药研究院 | White fungus skin-care composition and application thereof |
CN104983624A (en) * | 2015-06-29 | 2015-10-21 | 南阳市汇博生物技术有限公司 | Repairing skin-protecting nourishing mask impregnation liquid and preparation method thereof |
CN106361615A (en) * | 2016-09-26 | 2017-02-01 | 重庆市中药研究院 | White fungus mask tissue |
CN108514544A (en) * | 2018-07-04 | 2018-09-11 | 合肥丰瑞隆生物科技有限公司 | Face's moisturizing liquid and preparation method thereof |
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