CN108221181B - 异形碳化硅纤维毡的制备方法 - Google Patents
异形碳化硅纤维毡的制备方法 Download PDFInfo
- Publication number
- CN108221181B CN108221181B CN201810005453.1A CN201810005453A CN108221181B CN 108221181 B CN108221181 B CN 108221181B CN 201810005453 A CN201810005453 A CN 201810005453A CN 108221181 B CN108221181 B CN 108221181B
- Authority
- CN
- China
- Prior art keywords
- fiber
- special
- polycarbosilane
- silicon carbide
- carbide fibre
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 239000000835 fiber Substances 0.000 title claims abstract description 122
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 title claims abstract description 40
- 229910010271 silicon carbide Inorganic materials 0.000 title claims abstract description 40
- 238000002360 preparation method Methods 0.000 title claims abstract description 19
- 229920003257 polycarbosilane Polymers 0.000 claims abstract description 58
- 230000003647 oxidation Effects 0.000 claims abstract description 20
- 238000007254 oxidation reaction Methods 0.000 claims abstract description 20
- 239000002243 precursor Substances 0.000 claims abstract description 17
- 239000004642 Polyimide Substances 0.000 claims abstract description 11
- 229920001721 polyimide Polymers 0.000 claims abstract description 11
- 230000008021 deposition Effects 0.000 claims abstract description 10
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 claims description 28
- 238000010792 warming Methods 0.000 claims description 17
- 229910052786 argon Inorganic materials 0.000 claims description 14
- 239000007789 gas Substances 0.000 claims description 14
- 238000000034 method Methods 0.000 claims description 9
- QABCGOSYZHCPGN-UHFFFAOYSA-N chloro(dimethyl)silicon Chemical compound C[Si](C)Cl QABCGOSYZHCPGN-UHFFFAOYSA-N 0.000 claims description 6
- 238000004132 cross linking Methods 0.000 claims description 6
- 230000005251 gamma ray Effects 0.000 claims description 6
- 238000010438 heat treatment Methods 0.000 claims description 5
- 238000006073 displacement reaction Methods 0.000 claims description 4
- 235000004035 Cryptotaenia japonica Nutrition 0.000 claims description 2
- 102000007641 Trefoil Factors Human genes 0.000 claims description 2
- 235000015724 Trifolium pratense Nutrition 0.000 claims description 2
- 238000001035 drying Methods 0.000 claims description 2
- 238000004886 process control Methods 0.000 claims 1
- 238000005260 corrosion Methods 0.000 abstract description 11
- 230000007797 corrosion Effects 0.000 abstract description 11
- 230000009286 beneficial effect Effects 0.000 abstract description 3
- 239000011230 binding agent Substances 0.000 abstract description 3
- 230000000052 comparative effect Effects 0.000 description 5
- 239000000463 material Substances 0.000 description 3
- 239000000919 ceramic Substances 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000011261 inert gas Substances 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- 229910003978 SiClx Inorganic materials 0.000 description 1
- IKXDEFIEGAVNOZ-UHFFFAOYSA-N [SiH4].[C] Chemical compound [SiH4].[C] IKXDEFIEGAVNOZ-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 239000002657 fibrous material Substances 0.000 description 1
- 229920006253 high performance fiber Polymers 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 238000012113 quantitative test Methods 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
Classifications
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/58—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives
- D04H1/587—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties by applying, incorporating or activating chemical or thermoplastic bonding agents, e.g. adhesives characterised by the bonding agents used
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
- D01F9/10—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material by decomposition of organic substances
-
- D—TEXTILES; PAPER
- D04—BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
- D04H—MAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
- D04H1/00—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres
- D04H1/40—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties
- D04H1/42—Non-woven fabrics formed wholly or mainly of staple fibres or like relatively short fibres from fleeces or layers composed of fibres without existing or potential cohesive properties characterised by the use of certain kinds of fibres insofar as this use has no preponderant influence on the consolidation of the fleece
- D04H1/4382—Stretched reticular film fibres; Composite fibres; Mixed fibres; Ultrafine fibres; Fibres for artificial leather
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06C—FINISHING, DRESSING, TENTERING OR STRETCHING TEXTILE FABRICS
- D06C7/00—Heating or cooling textile fabrics
- D06C7/04—Carbonising or oxidising
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Fibers (AREA)
- Nonwoven Fabrics (AREA)
Abstract
Description
组别 | 年腐蚀延伸率 |
实施例一 | 50% |
实施例二 | 55% |
对比例一 | 74% |
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810005453.1A CN108221181B (zh) | 2018-01-03 | 2018-01-03 | 异形碳化硅纤维毡的制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201810005453.1A CN108221181B (zh) | 2018-01-03 | 2018-01-03 | 异形碳化硅纤维毡的制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN108221181A CN108221181A (zh) | 2018-06-29 |
CN108221181B true CN108221181B (zh) | 2019-10-01 |
Family
ID=62645195
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201810005453.1A Active CN108221181B (zh) | 2018-01-03 | 2018-01-03 | 异形碳化硅纤维毡的制备方法 |
Country Status (1)
Country | Link |
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CN (1) | CN108221181B (zh) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN109837611B (zh) * | 2019-01-28 | 2021-09-24 | 江西嘉捷信达新材料科技有限公司 | C形HfC纳米片增强碳化硅纤维毡及其制备方法 |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5218972A (en) * | 1975-07-29 | 1977-02-12 | Tohoku Daigaku Kinzoku Zairyo | Silicon carbide fiber laminate and its manufacture |
JPS63312926A (ja) * | 1987-06-15 | 1988-12-21 | Honda Motor Co Ltd | 繊維強化複合材料の製造方法 |
CN1878898A (zh) * | 2003-11-10 | 2006-12-13 | 帝人株式会社 | 碳纤维无纺布、其制造方法及用途 |
CN102877218A (zh) * | 2012-10-24 | 2013-01-16 | 厦门大学 | 一种疏水吸油碳化硅陶瓷纤维毡的制备方法 |
CN103451852A (zh) * | 2013-08-31 | 2013-12-18 | 中国人民解放军国防科学技术大学 | 一种TiO2纳米棒/SiC复合纤维毡的制备方法 |
CN105386237A (zh) * | 2015-12-24 | 2016-03-09 | 南通大学 | 一种碳化硅纤维毡的制备方法及制备用湿法沉积装置 |
CN106835497A (zh) * | 2017-02-14 | 2017-06-13 | 中国人民解放军国防科学技术大学 | 多级纳米结构碳化硅或氮化硅纤维毡及其制备方法 |
-
2018
- 2018-01-03 CN CN201810005453.1A patent/CN108221181B/zh active Active
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5218972A (en) * | 1975-07-29 | 1977-02-12 | Tohoku Daigaku Kinzoku Zairyo | Silicon carbide fiber laminate and its manufacture |
JPS63312926A (ja) * | 1987-06-15 | 1988-12-21 | Honda Motor Co Ltd | 繊維強化複合材料の製造方法 |
CN1878898A (zh) * | 2003-11-10 | 2006-12-13 | 帝人株式会社 | 碳纤维无纺布、其制造方法及用途 |
CN102877218A (zh) * | 2012-10-24 | 2013-01-16 | 厦门大学 | 一种疏水吸油碳化硅陶瓷纤维毡的制备方法 |
CN103451852A (zh) * | 2013-08-31 | 2013-12-18 | 中国人民解放军国防科学技术大学 | 一种TiO2纳米棒/SiC复合纤维毡的制备方法 |
CN105386237A (zh) * | 2015-12-24 | 2016-03-09 | 南通大学 | 一种碳化硅纤维毡的制备方法及制备用湿法沉积装置 |
CN106835497A (zh) * | 2017-02-14 | 2017-06-13 | 中国人民解放军国防科学技术大学 | 多级纳米结构碳化硅或氮化硅纤维毡及其制备方法 |
Non-Patent Citations (1)
Title |
---|
具备吸收雷达波功能的三叶型碳化硅纤维研制;王应德等;《复合材料学报》;20100228;第18卷(第1期);第42-45页 * |
Also Published As
Publication number | Publication date |
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CN108221181A (zh) | 2018-06-29 |
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Effective date of registration: 20240122 Address after: 330513 Hongshan Avenue, Industrial Park, Anyi County, Nanchang City, Jiangxi Province Patentee after: Jiangxi Xinda Hangke New Material Technology Co.,Ltd. Country or region after: China Address before: Room 502, Venture Building No. 18, High-tech Second Road, Nanchang High-tech Industrial Development Zone, Nanchang City, Jiangxi Province Patentee before: JIANGXI JIAJIE XINDA NEW MATERIAL TECHNOLOGY CO.,LTD. Country or region before: China |