CN108103441A - A kind of anti-dazzle lens coating method - Google Patents
A kind of anti-dazzle lens coating method Download PDFInfo
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- CN108103441A CN108103441A CN201711353480.XA CN201711353480A CN108103441A CN 108103441 A CN108103441 A CN 108103441A CN 201711353480 A CN201711353480 A CN 201711353480A CN 108103441 A CN108103441 A CN 108103441A
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/10—Glass or silica
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/06—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the coating material
- C23C14/08—Oxides
- C23C14/083—Oxides of refractory metals or yttrium
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C14/00—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material
- C23C14/22—Coating by vacuum evaporation, by sputtering or by ion implantation of the coating forming material characterised by the process of coating
- C23C14/24—Vacuum evaporation
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
- G02B1/10—Optical coatings produced by application to, or surface treatment of, optical elements
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- G—PHYSICS
- G02—OPTICS
- G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
- G02B5/00—Optical elements other than lenses
- G02B5/20—Filters
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- General Physics & Mathematics (AREA)
- Optics & Photonics (AREA)
- Physical Vapour Deposition (AREA)
Abstract
The present invention relates to a kind of anti-dazzle lens coating methods, comprise the following steps:1)Substrate is cleaned, is dried;2)Plated film is carried out to inside and outside two surfaces of substrate respectively:Respectively to two-sided the first film layer of plating, respectively to two-sided the second film layer of plating, respectively to two-sided plating third membrane layer, respectively to two-sided the 4th film layer of plating, respectively to two-sided the 5th film layer of plating, respectively to two-sided the 6th film layer of plating and respectively to two-sided the 7th film layer of plating.Multiple film layers for being coated with of eyeglass of the present invention can effective anti-dazzle, metal layer can effectively promote clarity and anti-blue light effect simultaneously, so as to improve the whole clarity of eyeglass, clarity and authenticity for vision have good contribution, can effectively alleviate visual fatigue to the filtering for being harmful to glare, blue light.
Description
Technical field
The present invention relates to a kind of lens technology field, more particularly, to a kind of anti-dazzle lens coating method.
Background technology
With people's culture, the continuous improvement of living standard, the development of sight protection work, glasses as correcting defects of vision or
Protect eyes and the simple optical device made, played an important role in people's sphere of life.Glasses are typically by mirror
Piece and mirror holder composition, from functionally saying for eyeglass, it has the light quantity adjusted into eyes, increases eyesight, protect eyes safety
The effects that with clinical treatment eye disease.
The species of eyeglass is various at present, such as common TAC polarized lenses at present, can the harmful light of 100% barrier, therefore
Quite favored by consumer, used particularly suitable for outdoor sports, however, eyeglass inevitably scrapes during the motion, therefore
The rub proofness of eyeglass is also the Consideration that consumer chooses, presently commercially available TAC polarized lenses, surface it is hard
Degree can only achieve H, and wearability is 1.5 grades, it is easy to and it is scratched or is broken by hard object, influence the effect that user observes things,
Both made troubles, but also need to often replace to user, and increased use cost, have much room for improvement.
During driving at night, if opposite driving vehicle uses powerful car light in violation of rules and regulations, driver will generate dazzling sensation,
And vision is difficult to recover normal condition in longer period of time, easily causes traffic accident.People in the case, dazzle by generation
Purpose mechanism is:When people enters dark place or from dark place to daylight under strong light environment, eyes are required for one section of adaptation time of experience
Surrounding objects can just be seen clearly, correspondingly referred to as dark adaptation and light adaptation.Related scientific information shows this time met the needs of
About 5-10min, and new lightness environment needs 20 are adapted to completely-30min.During driving at night, when opposite, vehicle heads on
It sails when coming, driver will be there are one the process of light adaptation, and when vehicle crosses, and there are one the process of dark adaptation, easily causes
Human eye fatigue.To solve the brilliant prestige mirror of this security risk, the method that people's generally use electronics is combined with optics, such as ADS,
This product is the upgraded product of automotive sunshade panel, can effectively prevent dazzling, and is had saturating with extraneous light intensity adjust automatically
The advantages of penetrating rate, but it matches with vehicle, if other vehicles are want separately install using this product, greatly reduces
Its versatility, and such product is on the high side.
In view of the above-mentioned problems, with reference to the glasses that people often wear, research and development are a kind of to prevent that dazzling eyeglass from being most important
's.
The content of the invention
In view of the above-mentioned deficiencies in the prior art, it is an object of the present invention to provide it is a kind of have the function of anti-glare, make suitable for night
Anti-dazzle lens coating method.
To achieve the above object, the present invention uses following technical scheme:
A kind of anti-dazzle lens coating method, the eyeglass are included by resin or the molding substrate of glass, the substrate it is inside and outside
Two surfaces are symmetrical from the inside to surface to be sequentially equipped with the first film layer, the second film layer, third membrane layer, the 4th film layer, the 5th film layer, the 6th
Film layer and the 7th film layer;First film layer, third membrane layer and the 5th film layer are silicon dioxide layer, and thickness is 60-90nm;
Second film layer, the 4th film layer and the 6th film layer are five oxidations, three titanium layer, and thickness is 20-80nm;7th film layer
For metal layer, thickness 25-40nm;When the substrate is by resin forming, the film plating process specifically includes following steps:
1)Substrate is cleaned, is dried;
2)Plated film is carried out to inside and outside two surfaces of substrate respectively;
A, respectively to two-sided the first film layer of plating:
Vacuum degree in vacuum coating cabin is adjusted to less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin
It spends for 50-70 DEG C, the membrane material of the first film layer is bombarded using electron gun, after the membrane material evaporation of the first film layer in the form of nanoscale molecular
Be deposited on the outer surface of substrate, while control the rate that the first film layer is deposited as 7/S, the first film layer ultimately form after thickness
For 60-90nm;Wherein, the membrane material of first film layer is silica, forms silicon dioxide layer;
B, respectively to two-sided the second film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the second film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the second film layer in the form of nanoscale molecular
The surface of product first film layer in above-mentioned steps A, while the rate that the second film layer is controlled to be deposited is 2.5/S, the second film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of second film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
C, respectively to two-sided plating third membrane layer:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
It 50-70 DEG C, using the membrane material of electron gun bombardment third membrane layer, is deposited after the membrane material evaporation of third membrane layer in the form of nanoscale molecular
The surface of the second film layer in above-mentioned steps B, while the rate that third membrane layer is controlled to be deposited is 7/S, third membrane layer ultimately forms
Thickness afterwards is 60-90nm;Wherein, the membrane material of the third membrane layer is silica, forms silicon dioxide layer;
D, respectively to two-sided the 4th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the 4th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 4th film layer in the form of nanoscale molecular
The surface of product third membrane layer in above-mentioned steps C, while the rate that the 4th film layer is controlled to be deposited is 2.5/S, the 4th film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of the 4th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
E, respectively to two-sided the 5th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the 5th film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the 5th film layer in the form of nanoscale molecular
The surface of the 4th film layer in above-mentioned steps D, while the rate that the 5th film layer is controlled to be deposited is 7/S, the 5th film layer ultimately forms
Thickness afterwards is 60-90nm;Wherein, the membrane material of the 5th film layer is silica, forms silicon dioxide layer;
F, respectively to two-sided the 6th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the 6th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 6th film layer in the form of nanoscale molecular
The surface of product the 5th film layer in above-mentioned steps E, while the rate that the 6th film layer is controlled to be deposited is 2.5/S, the 6th film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of the 6th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
G, respectively to two-sided the 7th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the 7th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 7th film layer in the form of nanoscale molecular
The surface of product the 6th film layer in above-mentioned steps F, while the rate that the 7th film layer is deposited is controlled as 1/S, the 7th film layer most end form
Thickness after is 25-40nm;Wherein, the membrane material of the 7th film layer is gold, silver, platinum, neodymium, copper, zinc, nickel, billon, silver conjunction
Gold, platinum alloy, neodymium alloy, copper alloy, kirsite or nickel alloy form metal layer.
When the substrate is molded by glass, the film plating process specifically includes following steps:
1)Substrate is cleaned, is dried;
2)Plated film is carried out to inside and outside two surfaces of substrate respectively;
A, respectively to two-sided the first film layer of plating:
Vacuum degree in vacuum coating cabin is adjusted to less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin
It spends for 200-300 DEG C, the membrane material of the first film layer is bombarded using electron gun, with nanoscale molecular shape after the membrane material evaporation of the first film layer
Formula is deposited on the outer surface of substrate, while controls the rate that the first film layer is deposited as 7/S, the first film layer ultimately form after thickness
It spends for 60-90nm;Wherein, the membrane material of first film layer is silica, forms silicon dioxide layer;
B, respectively to two-sided the second film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the second film layer is bombarded using electron gun, after the membrane material evaporation of the second film layer in the form of nanoscale molecular
The surface of the first film layer in above-mentioned steps A is deposited on, while the rate that the second film layer is controlled to be deposited is 2.5/S, the second film layer is most
Thickness of the end form after is 20-80nm;Wherein, the membrane material of second film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
C, respectively to two-sided plating third membrane layer:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
It 200-300 DEG C, using the membrane material of electron gun bombardment third membrane layer, is sunk after the membrane material evaporation of third membrane layer in the form of nanoscale molecular
The surface of product second film layer in above-mentioned steps B, while the rate that third membrane layer is deposited is controlled as 7/S, third membrane layer most end form
Thickness after is 60-90nm;Wherein, the membrane material of the third membrane layer is silica, forms silicon dioxide layer;
D, respectively to two-sided the 4th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the 4th film layer is bombarded using electron gun, after the membrane material evaporation of the 4th film layer in the form of nanoscale molecular
The surface of third membrane layer in above-mentioned steps C is deposited on, while the rate that the 4th film layer is controlled to be deposited is 2.5/S, the 4th film layer is most
Thickness of the end form after is 20-80nm;Wherein, the membrane material of the 4th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
E, respectively to two-sided the 5th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the 5th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 5th film layer in the form of nanoscale molecular
The surface of product the 4th film layer in above-mentioned steps D, while the rate that the 5th film layer is deposited is controlled as 7/S, the 5th film layer most end form
Thickness after is 60-90nm;Wherein, the membrane material of the 5th film layer is silica, forms silicon dioxide layer;
F, respectively to two-sided the 6th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the 6th film layer is bombarded using electron gun, after the membrane material evaporation of the 6th film layer in the form of nanoscale molecular
The surface of the 5th film layer in above-mentioned steps E is deposited on, while the rate that the 6th film layer is controlled to be deposited is 2.5/S, the 6th film layer is most
Thickness of the end form after is 20-80nm;Wherein, the membrane material of the 6th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
G, respectively to two-sided the 7th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the 7th film layer is bombarded using electron gun, after the membrane material evaporation of the 7th film layer in the form of nanoscale molecular
The surface of the 6th film layer in above-mentioned steps F is deposited on, while the rate that the 7th film layer is controlled to be deposited is 1/S, the 7th film layer is final
Thickness after formation is 25-40nm;Wherein, the membrane material of the 7th film layer is gold, silver, platinum, neodymium, copper, zinc, nickel, billon, silver
Alloy, platinum alloy, neodymium alloy, copper alloy, kirsite or nickel alloy form metal layer.
The step 1)In substrate is cleaned, dry and be as follows:Using organic cleaning solvent pair
Substrate carries out first wash, and aids in cleaning with ultrasonic wave, is dried using isopropanol;Before substrate coating, substrate is placed on very
In empty cabin, with being cleaned again for outer surface 2-3 minutes for ion gun bombardment substrate.
The present invention uses the principle of electron beam vacuum evaporation, has after being accelerated in the electric field using electrically charged particle certain
Ion is guided into and is intended to the electrode made of the substrate of plated film by the characteristics of kinetic energy, and is bombarded by electron gun with high temperature and there is simple substance
High purity metal, metal alloy or other oxides, the nano molecular being evaporated makes it be moved to along certain direction
Substrate and the method finally to form a film in deposition on substrate.This invention technology is combined in the special distributed controll electric field in magnetic field
Trajectory of electron motion, the technique that plated film is improved with this so that coating film thickness and uniformity are controllable, and prepare film layer compactness
It gets well, cohesive force is strong and high purity.
If present invention vacuum evaporation on substrate has dried layer five to aoxidize three titanium layers, five oxidations, three titanium crystal material is taken full advantage of
The performances such as material coating operation is good, and film layer is intensive, uniformly, stablizes, and stress is small and five oxidation Tritanium/Trititanium crystalline materials are in visible ray
There is the advantages that highest refractive index, good crystallinity, vapor deposition stabilization, no deflation and splash so as to fit in eyeglass base in wave band
On piece is coated with the good multilayer film of anti-reflection property.
If present invention vacuum evaporation on substrate has dried layer silicon dioxide layer, main rise increases film adhesion, wearability
And the effect of impact resistance, while harmful light can be absorbed.
Several five three titanium layers of oxidation being arranged alternately and silicon dioxide layer are deposited in eyeglass substrate inner and outer surfaces in the present invention,
Most purple lights and blue light have not only effectively been filtered off, but also can effectively reflect harmful light, Qiang Guang, dazzling light wave, flash light by force
Ripple reduces the stimulation of the injury and shortwave dazzle to human eye retina;The metal layer of the present invention not only improves anti-blue light effect
Fruit and clarity, and harmful light, dazzling light wave can also be reflected, flash light wave etc. by force;The present invention is mutual by above-mentioned film layer
Cooperation plays absorption, reflection, conversion, filtering and other effects, is the core technology of glasses lens plated anti-glazing, while has filter blue light
Function;The present invention is by adjusting the thickness of above-mentioned each film layer so that longer wavelengths of visible ray generates coherent interference, so as into one
Step generates antiglare effect.
When the eyeglass substrate of the present invention is by resin forming, by each film layer of eyeglass made from preparation method of the present invention subzero
Adhesive force at 20 DEG C is 2-4hrs, and the adhesive force at 80 DEG C is 2-4hrs;When the eyeglass substrate of the present invention is molded by glass,
It is 6-9hrs by adhesive force of each film layer of eyeglass made from preparation method of the present invention at subzero 20 DEG C, the attachment at 80 DEG C
Power is 6-9hrs;Multiple film layers for being coated with of eyeglass of the present invention can effective anti-dazzle, while metal layer can be promoted effectively clearly
Clear degree and anti-blue light effect, so as to improve the whole clarity of eyeglass, clarity and authenticity for vision have well
Contribution can effectively alleviate visual fatigue to the filtering for being harmful to glare, blue light.
Description of the drawings
The present invention is described in further details below in conjunction with the drawings and specific embodiments:
Fig. 1 is the exploded view of anti-dazzle lens coating method of the present invention.
Specific embodiment
As shown in Figure 1, the anti-dazzle lens coating method of the present invention, the eyeglass is included by resin or the molding base of glass
Piece 1, inside and outside two surfaces of the substrate 1 are symmetrical from the inside to surface to be sequentially equipped with the first film layer 2, the second film layer 3, third membrane layer
4th, the 4th film layer 5, the 5th film layer 6, the 6th film layer 7 and the 7th film layer 8;First film layer 2,4 and the 5th film layer 6 of third membrane layer
It is silicon dioxide layer, thickness is 60-90nm;Second film layer 3, the 4th film layer 5 and the 6th film layer 7 are five oxidations three
Titanium layer, thickness are 20-80nm;7th film layer 8 be metal layer, thickness 25-40nm;The substrate 1 is by resin forming
When, the film plating process specifically includes following steps:
1)Substrate is cleaned, is dried;
2)Plated film is carried out to inside and outside two surfaces of substrate respectively;
A, respectively to two-sided the first film layer of plating:
Vacuum degree in vacuum coating cabin is adjusted to less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin
It spends for 50-70 DEG C, the membrane material of the first film layer is bombarded using electron gun, after the membrane material evaporation of the first film layer in the form of nanoscale molecular
Be deposited on the outer surface of substrate, while control the rate that the first film layer is deposited as 7/S, the first film layer ultimately form after thickness
For 60-90nm;Wherein, the membrane material of first film layer is silica, forms silicon dioxide layer;
B, respectively to two-sided the second film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the second film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the second film layer in the form of nanoscale molecular
The surface of product first film layer in above-mentioned steps A, while the rate that the second film layer is controlled to be deposited is 2.5/S, the second film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of second film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
C, respectively to two-sided plating third membrane layer:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
It 50-70 DEG C, using the membrane material of electron gun bombardment third membrane layer, is deposited after the membrane material evaporation of third membrane layer in the form of nanoscale molecular
The surface of the second film layer in above-mentioned steps B, while the rate that third membrane layer is controlled to be deposited is 7/S, third membrane layer ultimately forms
Thickness afterwards is 60-90nm;Wherein, the membrane material of the third membrane layer is silica, forms silicon dioxide layer;
D, respectively to two-sided the 4th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the 4th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 4th film layer in the form of nanoscale molecular
The surface of product third membrane layer in above-mentioned steps C, while the rate that the 4th film layer is controlled to be deposited is 2.5/S, the 4th film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of the 4th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
E, respectively to two-sided the 5th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the 5th film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the 5th film layer in the form of nanoscale molecular
The surface of the 4th film layer in above-mentioned steps D, while the rate that the 5th film layer is controlled to be deposited is 7/S, the 5th film layer ultimately forms
Thickness afterwards is 60-90nm;Wherein, the membrane material of the 5th film layer is silica, forms silicon dioxide layer;
F, respectively to two-sided the 6th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the 6th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 6th film layer in the form of nanoscale molecular
The surface of product the 5th film layer in above-mentioned steps E, while the rate that the 6th film layer is controlled to be deposited is 2.5/S, the 6th film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of the 6th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
G, respectively to two-sided the 7th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the 7th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 7th film layer in the form of nanoscale molecular
The surface of product the 6th film layer in above-mentioned steps F, while the rate that the 7th film layer is deposited is controlled as 1/S, the 7th film layer most end form
Thickness after is 25-40nm;Wherein, the membrane material of the 7th film layer is gold, silver, platinum, neodymium, copper, zinc, nickel, billon, silver conjunction
Gold, platinum alloy, neodymium alloy, copper alloy, kirsite or nickel alloy form metal layer.
When the substrate is molded by glass, the film plating process specifically includes following steps:
1)Substrate is cleaned, is dried;
2)Plated film is carried out to inside and outside two surfaces of substrate respectively;
A, respectively to two-sided the first film layer of plating:
Vacuum degree in vacuum coating cabin is adjusted to less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin
It spends for 200-300 DEG C, the membrane material of the first film layer is bombarded using electron gun, with nanoscale molecular shape after the membrane material evaporation of the first film layer
Formula is deposited on the outer surface of substrate, while controls the rate that the first film layer is deposited as 7/S, the first film layer ultimately form after thickness
It spends for 60-90nm;Wherein, the membrane material of first film layer is silica, forms silicon dioxide layer;
B, respectively to two-sided the second film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the second film layer is bombarded using electron gun, after the membrane material evaporation of the second film layer in the form of nanoscale molecular
The surface of the first film layer in above-mentioned steps A is deposited on, while the rate that the second film layer is controlled to be deposited is 2.5/S, the second film layer is most
Thickness of the end form after is 20-80nm;Wherein, the membrane material of second film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
C, respectively to two-sided plating third membrane layer:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
It 200-300 DEG C, using the membrane material of electron gun bombardment third membrane layer, is sunk after the membrane material evaporation of third membrane layer in the form of nanoscale molecular
The surface of product second film layer in above-mentioned steps B, while the rate that third membrane layer is deposited is controlled as 7/S, third membrane layer most end form
Thickness after is 60-90nm;Wherein, the membrane material of the third membrane layer is silica, forms silicon dioxide layer;
D, respectively to two-sided the 4th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the 4th film layer is bombarded using electron gun, after the membrane material evaporation of the 4th film layer in the form of nanoscale molecular
The surface of third membrane layer in above-mentioned steps C is deposited on, while the rate that the 4th film layer is controlled to be deposited is 2.5/S, the 4th film layer is most
Thickness of the end form after is 20-80nm;Wherein, the membrane material of the 4th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
E, respectively to two-sided the 5th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the 5th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 5th film layer in the form of nanoscale molecular
The surface of product the 4th film layer in above-mentioned steps D, while the rate that the 5th film layer is deposited is controlled as 7/S, the 5th film layer most end form
Thickness after is 60-90nm;Wherein, the membrane material of the 5th film layer is silica, forms silicon dioxide layer;
F, respectively to two-sided the 6th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the 6th film layer is bombarded using electron gun, after the membrane material evaporation of the 6th film layer in the form of nanoscale molecular
The surface of the 5th film layer in above-mentioned steps E is deposited on, while the rate that the 6th film layer is controlled to be deposited is 2.5/S, the 6th film layer is most
Thickness of the end form after is 20-80nm;Wherein, the membrane material of the 6th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
G, respectively to two-sided the 7th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the 7th film layer is bombarded using electron gun, after the membrane material evaporation of the 7th film layer in the form of nanoscale molecular
The surface of the 6th film layer in above-mentioned steps F is deposited on, while the rate that the 7th film layer is controlled to be deposited is 1/S, the 7th film layer is final
Thickness after formation is 25-40nm;Wherein, the membrane material of the 7th film layer is gold, silver, platinum, neodymium, copper, zinc, nickel, billon, silver
Alloy, platinum alloy, neodymium alloy, copper alloy, kirsite or nickel alloy form metal layer.
The step 1)In substrate is cleaned, dry and be as follows:Using organic cleaning solvent pair
Substrate carries out first wash, and aids in cleaning with ultrasonic wave, is dried using isopropanol;Before substrate coating, substrate is placed on very
In empty cabin, with being cleaned again for outer surface 2-3 minutes for ion gun bombardment substrate.
The present invention uses the principle of electron beam vacuum evaporation, has after being accelerated in the electric field using electrically charged particle certain
Ion is guided into and is intended to the electrode made of the substrate of plated film by the characteristics of kinetic energy, and is bombarded by electron gun with high temperature and there is simple substance
High purity metal, metal alloy or other oxides, the nano molecular being evaporated makes it be moved to along certain direction
Substrate and the method finally to form a film in deposition on substrate.This invention technology is combined in the special distributed controll electric field in magnetic field
Trajectory of electron motion, the technique that plated film is improved with this so that coating film thickness and uniformity are controllable, and prepare film layer compactness
It gets well, cohesive force is strong and high purity.
If present invention vacuum evaporation on substrate has dried layer five to aoxidize three titanium layers, five oxidations, three titanium crystal material is taken full advantage of
The performances such as material coating operation is good, and film layer is intensive, uniformly, stablizes, and stress is small and five oxidation Tritanium/Trititanium crystalline materials are in visible ray
There is the advantages that highest refractive index, good crystallinity, vapor deposition stabilization, no deflation and splash so as to fit in eyeglass base in wave band
On piece is coated with the good multilayer film of anti-reflection property.
If present invention vacuum evaporation on substrate has dried layer silicon dioxide layer, main rise increases film adhesion, wearability
And the effect of impact resistance, while harmful light can be absorbed.
Several five three titanium layers of oxidation being arranged alternately and silicon dioxide layer are deposited in eyeglass substrate inner and outer surfaces in the present invention,
Most purple lights and blue light have not only effectively been filtered off, but also can effectively reflect harmful light, Qiang Guang, dazzling light wave, flash light by force
Ripple reduces the stimulation of the injury and shortwave dazzle to human eye retina;The metal layer of the present invention not only improves anti-blue light effect
Fruit and clarity, and harmful light, dazzling light wave can also be reflected, flash light wave etc. by force;The present invention is mutual by above-mentioned film layer
Cooperation plays absorption, reflection, conversion, filtering and other effects, is the core technology of glasses lens plated anti-glazing, while has filter blue light
Function;The present invention is by adjusting the thickness of above-mentioned each film layer so that longer wavelengths of visible ray generates coherent interference, so as into one
Step generates antiglare effect.
When the eyeglass substrate of the present invention is by resin forming, by each film layer of eyeglass made from preparation method of the present invention subzero
Adhesive force at 20 DEG C is 2-4hrs, and the adhesive force at 80 DEG C is 2-4hrs;When the eyeglass substrate of the present invention is molded by glass,
It is 6-9hrs by adhesive force of each film layer of eyeglass made from preparation method of the present invention at subzero 20 DEG C, the attachment at 80 DEG C
Power is 6-9hrs;Multiple film layers for being coated with of eyeglass of the present invention can effective anti-dazzle, while metal layer can be promoted effectively clearly
Clear degree and anti-blue light effect, so as to improve the whole clarity of eyeglass, clarity and authenticity for vision have well
Contribution can effectively alleviate visual fatigue to the filtering for being harmful to glare, blue light.
Above description should not have protection scope of the present invention any restriction.
Claims (3)
1. a kind of anti-dazzle lens coating method, the eyeglass is included by resin or the molding substrate of glass, the substrate it is interior,
Outer two surfaces are symmetrical from the inside to surface to be sequentially equipped with the first film layer, the second film layer, third membrane layer, the 4th film layer, the 5th film layer, the
Six film layers and the 7th film layer;First film layer, third membrane layer and the 5th film layer are silicon dioxide layer, and thickness is 60-
90nm;Second film layer, the 4th film layer and the 6th film layer are five oxidations, three titanium layer, and thickness is 20-80nm;Described 7th
Film layer is metal layer, thickness 25-40nm, it is characterised in that:When the substrate is by resin forming, the film plating process specifically wraps
Include following steps:
1)Substrate is cleaned, is dried;
2)Plated film is carried out to inside and outside two surfaces of substrate respectively;
A, respectively to two-sided the first film layer of plating:
Vacuum degree in vacuum coating cabin is adjusted to less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin
For 50-70 DEG C, the membrane material of the first film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the first film layer in the form of nanoscale molecular
Product is in the outer surface of substrate, while the rate that the first film layer is controlled to be deposited is 7/S, and the thickness after the first film layer ultimately forms is
60-90nm;Wherein, the membrane material of first film layer is silica, forms silicon dioxide layer;
B, respectively to two-sided the second film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the second film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the second film layer in the form of nanoscale molecular
The surface of the first film layer in above-mentioned steps A, while the rate that the second film layer is deposited is controlled as 2.5/S, the second film layer most end form
Thickness after is 20-80nm;Wherein, the membrane material of second film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
C, respectively to two-sided plating third membrane layer:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
It 50-70 DEG C, using the membrane material of electron gun bombardment third membrane layer, is deposited after the membrane material evaporation of third membrane layer in the form of nanoscale molecular
The surface of the second film layer in above-mentioned steps B, while the rate that third membrane layer is controlled to be deposited is 7/S, third membrane layer ultimately forms
Thickness afterwards is 60-90nm;Wherein, the membrane material of the third membrane layer is silica, forms silicon dioxide layer;
D, respectively to two-sided the 4th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the 4th film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the 4th film layer in the form of nanoscale molecular
The surface of third membrane layer in above-mentioned steps C, while the rate that the 4th film layer is deposited is controlled as 2.5/S, the 4th film layer most end form
Thickness after is 20-80nm;Wherein, the membrane material of the 4th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
E, respectively to two-sided the 5th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the 5th film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the 5th film layer in the form of nanoscale molecular
The surface of the 4th film layer in above-mentioned steps D, while the rate that the 5th film layer is controlled to be deposited is 7/S, the 5th film layer ultimately forms
Thickness afterwards is 60-90nm;Wherein, the membrane material of the 5th film layer is silica, forms silicon dioxide layer;
F, respectively to two-sided the 6th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the 6th film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the 6th film layer in the form of nanoscale molecular
The surface of the 5th film layer in above-mentioned steps E, while the rate that the 6th film layer is deposited is controlled as 2.5/S, the 6th film layer most end form
Thickness after is 20-80nm;Wherein, the membrane material of the 6th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
G, respectively to two-sided the 7th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
50-70 DEG C, the membrane material of the 7th film layer is bombarded using electron gun, is deposited after the membrane material evaporation of the 7th film layer in the form of nanoscale molecular
The surface of the 6th film layer in above-mentioned steps F, while the rate that the 7th film layer is controlled to be deposited is 1/S, the 7th film layer ultimately forms
Thickness afterwards is 25-40nm;Wherein, the membrane material of the 7th film layer is gold, silver, platinum, neodymium, copper, zinc, nickel, billon, silver conjunction
Gold, platinum alloy, neodymium alloy, copper alloy, kirsite or nickel alloy form metal layer.
2. a kind of anti-dazzle lens coating method according to claim 1, it is characterised in that:The substrate is molded by glass
When, the film plating process specifically includes following steps:
1)Substrate is cleaned, is dried;
2)Plated film is carried out to inside and outside two surfaces of substrate respectively;
A, respectively to two-sided the first film layer of plating:
Vacuum degree in vacuum coating cabin is adjusted to less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin
For 200-300 DEG C, the membrane material of the first film layer is bombarded using electron gun, after the membrane material evaporation of the first film layer in the form of nanoscale molecular
Be deposited on the outer surface of substrate, while control the rate that the first film layer is deposited as 7/S, the first film layer ultimately form after thickness
For 60-90nm;Wherein, the membrane material of first film layer is silica, forms silicon dioxide layer;
B, respectively to two-sided the second film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the second film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the second film layer in the form of nanoscale molecular
The surface of product first film layer in above-mentioned steps A, while the rate that the second film layer is controlled to be deposited is 2.5/S, the second film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of second film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
C, respectively to two-sided plating third membrane layer:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
It 200-300 DEG C, using the membrane material of electron gun bombardment third membrane layer, is sunk after the membrane material evaporation of third membrane layer in the form of nanoscale molecular
The surface of product second film layer in above-mentioned steps B, while the rate that third membrane layer is deposited is controlled as 7/S, third membrane layer most end form
Thickness after is 60-90nm;Wherein, the membrane material of the third membrane layer is silica, forms silicon dioxide layer;
D, respectively to two-sided the 4th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the 4th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 4th film layer in the form of nanoscale molecular
The surface of product third membrane layer in above-mentioned steps C, while the rate that the 4th film layer is controlled to be deposited is 2.5/S, the 4th film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of the 4th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
E, respectively to two-sided the 5th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, and control the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the 5th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 5th film layer in the form of nanoscale molecular
The surface of product the 4th film layer in above-mentioned steps D, while the rate that the 5th film layer is deposited is controlled as 7/S, the 5th film layer most end form
Thickness after is 60-90nm;Wherein, the membrane material of the 5th film layer is silica, forms silicon dioxide layer;
F, respectively to two-sided the 6th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the 6th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 6th film layer in the form of nanoscale molecular
The surface of product the 5th film layer in above-mentioned steps E, while the rate that the 6th film layer is controlled to be deposited is 2.5/S, the 6th film layer is final
Thickness after formation is 20-80nm;Wherein, the membrane material of the 6th film layer is five oxidation Tritanium/Trititaniums, forms five three titanium layers of oxidation;
G, respectively to two-sided the 7th film layer of plating:
The vacuum degree in vacuum coating cabin is kept to be less than or equal to 5.0 × 10-3Pa, while keep the temperature in vacuum coating cabin to be
200-300 DEG C, the membrane material of the 7th film layer is bombarded using electron gun, is sunk after the membrane material evaporation of the 7th film layer in the form of nanoscale molecular
The surface of product the 6th film layer in above-mentioned steps F, while the rate that the 7th film layer is deposited is controlled as 1/S, the 7th film layer most end form
Thickness after is 25-40nm;Wherein, the membrane material of the 7th film layer is gold, silver, platinum, neodymium, copper, zinc, nickel, billon, silver conjunction
Gold, platinum alloy, neodymium alloy, copper alloy, kirsite or nickel alloy form metal layer.
3. according to a kind of anti-dazzle lens coating method described in claims 1 or 2, it is characterised in that:The step 1)
In substrate is cleaned, dry and be as follows:Using organic cleaning solvent to substrate progress first wash, and with
Ultrasonic wave auxiliary cleaning, is dried using isopropanol;Before substrate coating, substrate is placed in vacuum chamber, bombards base with ion gun
Outer surface 2-3 minutes of piece is cleaned again.
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN109437582A (en) * | 2018-12-03 | 2019-03-08 | 仙游县元生智汇科技有限公司 | A kind of production method of the 3D glass with anti-glare |
CN109455942A (en) * | 2018-12-03 | 2019-03-12 | 仙游县元生智汇科技有限公司 | A kind of anti-blue light resists dizzy 3D glass making procedures |
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CN105425414A (en) * | 2015-12-31 | 2016-03-23 | 奥特路(漳州)光学科技有限公司 | Blue light filtering lens and preparation method thereof |
CN105445960A (en) * | 2015-12-31 | 2016-03-30 | 奥特路(漳州)光学科技有限公司 | Anti-reflection and wear-proof lens capable of filtering blue light and preparation method of anti-reflection and wear-proof lens |
CN105441879A (en) * | 2015-12-31 | 2016-03-30 | 奥特路(漳州)光学科技有限公司 | Lampshade capable of filtering blue light and preventing glare and manufacturing method for lampshade |
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CN105425419A (en) * | 2015-12-31 | 2016-03-23 | 奥特路(漳州)光学科技有限公司 | Blue light filtering and wear resisting lens and preparation method thereof |
CN105425414A (en) * | 2015-12-31 | 2016-03-23 | 奥特路(漳州)光学科技有限公司 | Blue light filtering lens and preparation method thereof |
CN105445960A (en) * | 2015-12-31 | 2016-03-30 | 奥特路(漳州)光学科技有限公司 | Anti-reflection and wear-proof lens capable of filtering blue light and preparation method of anti-reflection and wear-proof lens |
CN105441879A (en) * | 2015-12-31 | 2016-03-30 | 奥特路(漳州)光学科技有限公司 | Lampshade capable of filtering blue light and preventing glare and manufacturing method for lampshade |
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CN109455942A (en) * | 2018-12-03 | 2019-03-12 | 仙游县元生智汇科技有限公司 | A kind of anti-blue light resists dizzy 3D glass making procedures |
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