CN107739825B - 一种利用含钒浸出液制备钒产品的方法 - Google Patents
一种利用含钒浸出液制备钒产品的方法 Download PDFInfo
- Publication number
- CN107739825B CN107739825B CN201711045681.3A CN201711045681A CN107739825B CN 107739825 B CN107739825 B CN 107739825B CN 201711045681 A CN201711045681 A CN 201711045681A CN 107739825 B CN107739825 B CN 107739825B
- Authority
- CN
- China
- Prior art keywords
- vanadium
- leachate
- boiling
- hydrochloric acid
- filter cake
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Links
- 229910052720 vanadium Inorganic materials 0.000 title claims abstract description 101
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 title claims abstract description 101
- 238000000034 method Methods 0.000 title claims abstract description 51
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims abstract description 45
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 claims abstract description 26
- 238000009835 boiling Methods 0.000 claims abstract description 24
- 239000012065 filter cake Substances 0.000 claims abstract description 24
- 239000000047 product Substances 0.000 claims abstract description 22
- 239000006228 supernatant Substances 0.000 claims abstract description 22
- 238000001816 cooling Methods 0.000 claims abstract description 12
- 238000005406 washing Methods 0.000 claims description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 9
- 239000008367 deionised water Substances 0.000 claims description 9
- 229910021641 deionized water Inorganic materials 0.000 claims description 9
- 238000002791 soaking Methods 0.000 claims description 9
- 229910052710 silicon Inorganic materials 0.000 abstract description 7
- 238000003756 stirring Methods 0.000 abstract description 7
- 239000010703 silicon Substances 0.000 abstract description 3
- 238000005272 metallurgy Methods 0.000 abstract description 2
- 239000012535 impurity Substances 0.000 description 8
- 239000011734 sodium Substances 0.000 description 8
- 238000004519 manufacturing process Methods 0.000 description 7
- 229910052708 sodium Inorganic materials 0.000 description 7
- 238000002360 preparation method Methods 0.000 description 5
- 238000000746 purification Methods 0.000 description 5
- 229910052804 chromium Inorganic materials 0.000 description 4
- 238000001035 drying Methods 0.000 description 4
- 238000005516 engineering process Methods 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 229910052700 potassium Inorganic materials 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 3
- 238000000605 extraction Methods 0.000 description 3
- 238000007689 inspection Methods 0.000 description 3
- 239000002994 raw material Substances 0.000 description 3
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 238000005265 energy consumption Methods 0.000 description 2
- 239000000413 hydrolysate Substances 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- 229910052742 iron Inorganic materials 0.000 description 2
- SZVJSHCCFOBDDC-UHFFFAOYSA-N iron(II,III) oxide Inorganic materials O=[Fe]O[Fe]O[Fe]=O SZVJSHCCFOBDDC-UHFFFAOYSA-N 0.000 description 2
- 238000011031 large-scale manufacturing process Methods 0.000 description 2
- 238000002386 leaching Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000001698 pyrogenic effect Effects 0.000 description 2
- 238000000638 solvent extraction Methods 0.000 description 2
- 229910001456 vanadium ion Inorganic materials 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- UNTBPXHCXVWYOI-UHFFFAOYSA-O azanium;oxido(dioxo)vanadium Chemical compound [NH4+].[O-][V](=O)=O UNTBPXHCXVWYOI-UHFFFAOYSA-O 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000009388 chemical precipitation Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- LPUQAYUQRXPFSQ-DFWYDOINSA-M monosodium L-glutamate Chemical compound [Na+].[O-]C(=O)[C@@H](N)CCC(O)=O LPUQAYUQRXPFSQ-DFWYDOINSA-M 0.000 description 1
- 235000013923 monosodium glutamate Nutrition 0.000 description 1
- 239000004223 monosodium glutamate Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- -1 sodium vanadates Chemical class 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 239000004575 stone Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical group [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 description 1
- WQEVDHBJGNOKKO-UHFFFAOYSA-K vanadic acid Chemical compound O[V](O)(O)=O WQEVDHBJGNOKKO-UHFFFAOYSA-K 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/22—Treatment or purification of solutions, e.g. obtained by leaching by physical processes, e.g. by filtration, by magnetic means, or by thermal decomposition
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B34/00—Obtaining refractory metals
- C22B34/20—Obtaining niobium, tantalum or vanadium
- C22B34/22—Obtaining vanadium
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Geochemistry & Mineralogy (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
Claims (4)
Priority Applications (1)
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CN201711045681.3A CN107739825B (zh) | 2017-10-31 | 2017-10-31 | 一种利用含钒浸出液制备钒产品的方法 |
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CN201711045681.3A CN107739825B (zh) | 2017-10-31 | 2017-10-31 | 一种利用含钒浸出液制备钒产品的方法 |
Publications (2)
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CN107739825A CN107739825A (zh) | 2018-02-27 |
CN107739825B true CN107739825B (zh) | 2019-05-17 |
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Families Citing this family (3)
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CN109292817A (zh) * | 2018-12-07 | 2019-02-01 | 攀钢集团攀枝花钢铁研究院有限公司 | 制备偏钒酸铵的方法 |
CN109279653A (zh) * | 2018-12-07 | 2019-01-29 | 攀钢集团攀枝花钢铁研究院有限公司 | 制备高纯五氧化二钒的方法 |
CN110010208B (zh) * | 2019-04-22 | 2023-02-28 | 东北大学 | V2O5-CaO-Cr2O3三元系相图的建立方法 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2175990C1 (ru) * | 2000-04-05 | 2001-11-20 | Открытое акционерное общество "АВИСМА титано-магниевый комбинат" | Способ получения пентаоксида ванадия |
CN102167400A (zh) * | 2011-03-18 | 2011-08-31 | 中南大学 | 一种含钒溶液生产五氧化二钒的方法 |
CN102897834A (zh) * | 2011-07-29 | 2013-01-30 | 攀钢集团钢铁钒钛股份有限公司 | 一种沉钒的方法和五氧化二钒的制备方法 |
CN102923775A (zh) * | 2012-11-27 | 2013-02-13 | 攀钢集团攀枝花钢铁研究院有限公司 | 一种高纯度五氧化二钒的制备方法 |
CN104099483A (zh) * | 2013-04-11 | 2014-10-15 | 陕西五洲矿业股份有限公司 | 一种高纯五氧化二钒的制备方法 |
-
2017
- 2017-10-31 CN CN201711045681.3A patent/CN107739825B/zh active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
RU2175990C1 (ru) * | 2000-04-05 | 2001-11-20 | Открытое акционерное общество "АВИСМА титано-магниевый комбинат" | Способ получения пентаоксида ванадия |
CN102167400A (zh) * | 2011-03-18 | 2011-08-31 | 中南大学 | 一种含钒溶液生产五氧化二钒的方法 |
CN102897834A (zh) * | 2011-07-29 | 2013-01-30 | 攀钢集团钢铁钒钛股份有限公司 | 一种沉钒的方法和五氧化二钒的制备方法 |
CN102923775A (zh) * | 2012-11-27 | 2013-02-13 | 攀钢集团攀枝花钢铁研究院有限公司 | 一种高纯度五氧化二钒的制备方法 |
CN104099483A (zh) * | 2013-04-11 | 2014-10-15 | 陕西五洲矿业股份有限公司 | 一种高纯五氧化二钒的制备方法 |
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Address after: 610306 Chengdu City, Chengdu, Sichuan, China (Sichuan) free trade test zone, Chengdu City, Qingbaijiang District, xiangdao Boulevard, Chengxiang Town, No. 1509 (room 13, A District, railway port mansion), room 1319 Patentee after: Chengdu advanced metal material industry technology Research Institute Co.,Ltd. Address before: 610306 Chengdu City, Chengdu, Sichuan, China (Sichuan) free trade test zone, Chengdu City, Qingbaijiang District, xiangdao Boulevard, Chengxiang Town, No. 1509 (room 13, A District, railway port mansion), room 1319 Patentee before: CHENGDU ADVANCED METAL MATERIAL INDUSTRIAL TECHNOLOGY RESEARCH INSTITUTE Co.,Ltd. |
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CP01 | Change in the name or title of a patent holder | ||
EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20180227 Assignee: SICHUAN PAN YAN TECHNOLOGY Co.,Ltd. Assignor: Chengdu advanced metal material industry technology Research Institute Co.,Ltd. Contract record no.: X2024980003062 Denomination of invention: A method for preparing vanadium products using vanadium containing leaching solution Granted publication date: 20190517 License type: Exclusive License Record date: 20240322 |
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EE01 | Entry into force of recordation of patent licensing contract |