CN106983697A - It is a kind of that there is shampoo of hair care effect and preparation method thereof - Google Patents
It is a kind of that there is shampoo of hair care effect and preparation method thereof Download PDFInfo
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/463—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfuric acid derivatives, e.g. sodium lauryl sulfate
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q5/02—Preparations for cleaning the hair
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
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Abstract
The invention provides a kind of shampoo with hair care effect and preparation method thereof, the shampoo is made up of shield hair composition, lauryl sodium sulfate, sodium lauryl tri(oxyethyl) sulfate, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and water, prepared by hybrid mode；The shampoo with hair care effect, each component synergy has effect of hair nourishing, submissive hair, lifting hair gloss and elasticity concurrently；Its preparation method is simple, the need for being adapted to scale industrial production.
Description
Technical field
The present invention relates to a kind of hair products and preparation method thereof, especially a kind of shampoo with hair care effect and its
Preparation method.
Background technology
Hair nursing technology is a kind of wide variety of technology in China's cosmetic field.In recent years, with cosmetics circle
Natural plant product is advocated, the correlative study using plant essence nursing hair, conditioning skin is also more and more.
Hair is the accessory organ of skin, stretches the hair outside skin and claims hair shaft, the long title hair root in skin.Hair root bag
In the hair follicle being made up of skin and connective tissue.All cell proliferations of hair and development and differentiation occur under skin surface
In hair follicle, once growing skin surface, most of metabolic activity has stopped, and is completely exposed to the external world, so as to keep physics complete
It is whole.Hair shaft is interior or endogenic repair process seldom occurs for surface.By taking hair as an example, though hair does not have to individual survival to pass
Important evolution effect, but when being grown in hair from the beginning skin, it more or less can produce influence to individual itself.Hair can
Pre- uv blocking, and in many species, hair (or fur) can provide heat-blocking action.In addition, although the hair style of people can occur
Change, but some social class crowds seem length hair in always thirsting for, and it is desirable that hair can flexible and gloss.So
And, hair can undergo the extensive infringement of environment, mainly UV irradiation, daily cleaning and with hair-dryer dry up caused by low humidity damage
Wound, various hairdressings and " anti-aging " treatment damage as caused by decolourizing, dye, persistently perm, stretch etc..Because hair can not be very
Protect oneself well, can not self-regeneration, be highly desirable to provide these nursing roles with product used in everyday.
Therefore, exploitation has the plant extraction elite of total care function to hair and skin, for cosmetics new product
Research and development are significant.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of shampoo with hair care effect.
Another technical problem to be solved by this invention is the preparation method for providing above-mentioned shampoo.
In order to solve the above technical problems, the technical scheme is that：
A kind of shampoo with hair care effect, by shield hair composition, lauryl sodium sulfate, lauryl ether sulfuric acid
Sodium, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and water composition, respectively
Weight percentages of components is as follows：
Surplus is water；Wherein,
The functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, is pressed
Its 2-10 parts of 1-5 parts of parts by weight meter Semen sesami nigrum dregs of rice, 1-3 parts of rye, 1-3 parts of black rice, 3-10 parts of the black soya bean dregs of rice and fleece-flower root.
It is preferred that, the above-mentioned shampoo with hair care effect, the shield hair composition is prepared by following methods
's：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg 40-55 DEG C water in a kettle., then with 10%
Salt acid for adjusting pH value adds 0.2-1kg composite plant hydrolases and dissolved to 3-5, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its quality percentage in the solution
Concentration is 0.3-0.5%, and in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation is by alkali protease, neutral protein
Enzyme and papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-
5：1-3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
Detection water-soluble protein content >=60% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
It is preferred that, the above-mentioned shampoo with hair care effect, shield hair composition Semen sesami nigrum based on its parts by weight
4 parts of 4 parts of the dregs of rice, 1 part of rye, 2 parts of black rice, 6 parts of the black soya bean dregs of rice and the fleece-flower root.
The preparation method of the above-mentioned shampoo with hair care effect, specific preparation process is as follows：
I prepares shield hair composition：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg 40-55 DEG C water in a kettle., then with 10%
Salt acid for adjusting pH value adds 0.2-1kg composite plant hydrolases and dissolved to 3-5, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its quality percentage in the solution
Concentration is 0.3-0.5%, and in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation is by alkali protease, neutral protein
Enzyme and papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-
5：1-3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced；
II prepares shampoo product according to conventional shampoo production technology.
It is preferred that, the preparation method of the above-mentioned shampoo with hair care effect, shampoo production technology in the step II
Step is as follows：
(1) solution that hair composition is diluted to 10% will be protected, gained 10% hair composition dilute solution is protected into standby；
(2) by formula material lauryl sodium sulfate, sodium lauryl tri(oxyethyl) sulfate, disodium ethylene diamine tetraacetate, propane diols,
Glycerine, Cocoamidopropyl betaine and lauric acid amide of ethanol are sequentially added in reactor by prescription amount after filter pipeline
It is stirred continuously, is heated to being completely dissolved under the conditions of 90 DEG C, then cools；
(3) formula material mixed adds 10% when being cooled to 45-55 DEG C and protects hair composition dilute solution and anti-corrosion
Agent, was mixed slowly after 40 minutes, was discharged when temperature drops to 40 DEG C.
It is preferred that, the preparation method of the above-mentioned shampoo with hair care effect, preservative is benzoic acid in the step (3)
Sodium, Phenoxyethanol, Sensiva SC50 or MIT.
It is preferred that, it is above-mentioned have hair care effect shampoo preparation method, step I (3) the neutral and alkali protease, in
Property protease and papain weight ratio be 4：3：1.
The beneficial effects of the invention are as follows：
The above-mentioned shampoo with hair care effect, each component synergy, has hair nourishing, submissive hair, poppet concurrently
Luminous pool and effect of elasticity；Its preparation method is simple, the need for being adapted to scale industrial production.
Embodiment
Technical scheme of the present invention is further described with reference to specific embodiment.
Embodiment 1
A kind of shampoo with hair care effect, by shield hair composition, lauryl sodium sulfate, lauryl ether sulfuric acid
Sodium, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and water composition, respectively
Weight percentages of components is as follows：
Surplus is water；Wherein,
The functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 4kg, rye 1kg, black rice 2kg, black soya bean dregs of rice 6kg and fleece-flower root 4kg.
The shield hair composition is prepared by following methods：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50 DEG C of water of 80kg in a kettle., then adjusted with 10% hydrochloric acid
PH value adds 0.7kg composite plant hydrolases and dissolved to 4,6 hours reaction time；
(3) adjust pH value to 7.5 with sodium hydroxide solution, add complex enzyme formulation, make its in the solution quality percentage it is dense
Spend for 0.4%, hydrolyzed 8 hours in temperature 45 C；The complex enzyme formulation is by alkali protease, neutral proteinase and Papain
Enzyme compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 4：3：1；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
Detection water-soluble protein content 67% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
The preparation method of the above-mentioned shampoo with hair care effect, specific preparation process is as follows：
(1) solution that hair composition is diluted to 10% will be protected, gained 10% hair composition dilute solution is protected into standby；
(2) by formula material lauryl sodium sulfate, sodium lauryl tri(oxyethyl) sulfate, disodium ethylene diamine tetraacetate, propane diols,
Glycerine, Cocoamidopropyl betaine and lauric acid amide of ethanol are sequentially added in reactor by prescription amount after filter pipeline
It is stirred continuously, is heated to being completely dissolved under the conditions of 90 DEG C, then cools；
(3) formula material mixed adds 10% when being cooled to 50 DEG C and protects hair composition dilute solution and benzoic acid
Sodium, was mixed slowly after 40 minutes, was discharged when temperature drops to 40 DEG C.
Embodiment 2
A kind of shampoo with hair care effect, by shield hair composition, lauryl sodium sulfate, lauryl ether sulfuric acid
Sodium, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and water composition, respectively
Weight percentages of components is as follows：
Surplus is water；Wherein,
The functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 5kg, rye 1kg, black rice 1kg, black soya bean dregs of rice 10kg and fleece-flower root 2kg.
The preparation method be the same as Example 1 of the shield hair composition.
The preparation method be the same as Example 1 of the above-mentioned shampoo with hair care effect.
Embodiment 3
A kind of shampoo with hair care effect, by shield hair composition, lauryl sodium sulfate, lauryl ether sulfuric acid
Sodium, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and water composition, respectively
Weight percentages of components is as follows：
Surplus is water；Wherein,
The functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 1kg, rye 3kg, black rice 3kg, black soya bean dregs of rice 3kg and fleece-flower root 10kg.
The preparation method be the same as Example 1 of the shield hair composition.
The preparation method be the same as Example 1 of the above-mentioned shampoo with hair care effect.
Embodiment 4
A kind of shampoo with hair care effect, by shield hair composition, lauryl sodium sulfate, lauryl ether sulfuric acid
Sodium, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and water composition, respectively
Weight percentages of components is as follows：
Surplus is water；Wherein,
The functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 4kg, rye 2kg, black rice 1.5kg, black soya bean dregs of rice 7kg and fleece-flower root 7kg.
The preparation method be the same as Example 1 of the shield hair composition.
The preparation method be the same as Example 1 of the above-mentioned shampoo with hair care effect.
Related test results：
Shampoo is according to GB/T 29679-2013 shampoos, hair cream national standard index pair obtained by above-described embodiment 1-4
Product is detected, including heat-resisting, cold-resistant, pH (25 DEG C), substance content, total number of bacterial colonies, excrement colibacillus group, golden yellow
Staphylococcus, pseudomonas aeruginosa, yeast and mold total plate count project.Each embodiment testing result is entirely reached：It is heat-resisting
Required with the cold-resistant regulation that meets, pH (25 DEG C) scope 6.5-7.5, substance content >=10%, total number of bacterial colonies≤
1000CFU/ml, excrement colibacillus group are not detected, staphylococcus aureus does not detect, pseudomonas aeruginosa does not detect, mould and ferment
Female bacterium total plate count total number of bacterial colonies≤100CFU/ml.Meet regulation requirement.
One of the embodiment 1-4 each components are commercially available prod, wherein, composite plant hydrolase is believed purchased from Novi of Denmark
(China) Investment Co., Ltd, enzyme activity is 100FGB/g；Alkali protease is purchased from lucky precious (Qingdao) bio tech ltd,
Its activity is 18000U/ml；Neutral proteinase is purchased from Beijing east prosperous and powerful Bioisystech Co., Ltd of China, and its activity is
20000U/ml；Papain is purchased from Zhengzhou De Xin chemical industry Industrial Co., Ltd., and its activity is 16000U/ml.Each component is used
Amount is increased or decreased according to same ratio, and the parts by weight relation of gained each component belongs to protection scope of the present invention.
Using effect is tested：
Using effect experiment (the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice, the fleece-flower root are carried out to the gained shampoo of embodiment 1
By weight 4:1:2:6:4 compoundings), wherein,
Contrast groups, replace protecting hair composition using formula with reference to embodiment 1, with purified water.
Example 1, using formula with reference to embodiment 1, with rye, black rice, the fleece-flower root by weight 1：2：4 compoundings replace hair care
With composition, water-soluble protein content is 47% (being performed by GB/T5511 appendix As).
Example 2, using formula with reference to embodiment 1, with the Semen sesami nigrum dregs of rice, the black soya bean dregs of rice, the fleece-flower root by weight 4：6：4 compounding generations
For shield hair composition, water-soluble protein content is 55% (being performed by GB/T5511 appendix As).
Example 3, using formula with reference to embodiment 1, with the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice by weight 4：1：2：6
Compounding replaces shield hair composition, and water-soluble protein content is 65% (being performed by GB/T5511 appendix As).
About 100 subjects, have participated in 2 weeks use researchs by a definite date.When research starts, the hair for recording all subjects is equal
For drying, fragility, not submissive and " wanting help ".100 subjects are divided into 5 groups, and 20 people/group use shampoo rinse in every 4 days
Hair, is during which had one's hair wash to subject and daily nursing is instructed, and laboratory is returned to after 12 days.Subject's hair quality is commented
Estimate, the results are shown in Table 1.
Table 1
The evaluation method of above-mentioned every detection parameter is as follows：
All parameters are evaluated according to 0 to 10 points, 10 points represent most probable situation.
1st, the aqueous weight testing method of hair
Use instrument：Sensitivity is 0.01mg electronic balances；Constant temperature and humidity incubator.
Topknot sample：5cm length, example weight 5g
Experimentation：Hair swatch is placed in room temperature, the constant temperature and humidity incubators of relative humidity ＜ 5% through combing rear overhang, is put
Put and taken out after 2 hours, weigh hair weight.The constant temperature and humidity culture between room temperature, relative humidity 40%-50% is suspended in again
In case, taken out after placing 2 hours, weigh hair weight.The difference divided by example weight of weight are hair water content twice.
2nd, hair intensity and elastomeric check method
Use instrument：Hair tensile strength detector
Topknot sample：20cm length
Experimentation：Using hair tensile strength detector, the fracture strength of hair is measured.Using linear variable power/away from
Hair elongation during increase strength is recorded from sensor.Hair extends, until fracture.The fracture strength of traction is typically smaller than
100 grams.Tractive force is with about 3 grams per second of speed increase.Coefficient of elasticity can be calculated according to these measurements.For comparing hair
Elasticity.With hair normal diameter, 70 μm all ultimate strength values are normalized.Detect individual's with standard microscopy
Hair diameter, calculates hairs break intensity level, for comparing hair intensity.
3rd, hair gloss is measured
Use instrument：Measurement of luster instrument
Topknot sample：Topknot length 20cm, weight 7.5g topknot
Experimentation：In the black box that hair is placed in measurement of luster instrument, Hair setting is allowed to comb equably to arrange
Into the straight line that width is 2.5cm.Using measurement of luster instrument, it is measured according to BNT gloss formula.
LBNT=gloss number
SinIntegrated in=reflectance curves in reflection peak
SoutPeak both wings are integrated in=reflectance curves
Integrated in D=diffusion curve maps
Wvisual=the average value by true picture along area-of-interest bandwidth
4th, hair drying comb rationality and wet hair comb rationality
Use instrument：Tensiometer；Constant temperature and humidity incubator
Topknot sample：Topknot length 50cm, weight 16g
Experimentation：
(1) hair drying comb rationality, topknot is placed in the constant temperature and humidity incubator of room temperature, relative humidity less than 5% 2 hours,
Take out and determine hair drying comb rationality.
(2) wet hair comb rationality, topknot is placed in the constant temperature and humidity incubator of room temperature, relative humidity more than 95% 2 hours,
Take out and determine wet hair comb rationality.
Tension tester is a kind of tester dedicated for Hair setting performance evaluation, passes through a standard comb mould
Apery combing hair is acted, and wisp of hair is combed and recorded by terminal.Sent out during test with 300mm/min speed tensile
Beam, displacement 200mm, the load value (unit that fetch bit is moved between 100-200mm：Gf) evaluated.
5th, compliance sensory evaluation standard
10 points, without tangling phenomenon, easily comb, no combing resistance hair soft such as silk, very smooth；
9 points, without obvious tangling phenomenon, easily comb, and slightly sense combs resistance hair soft, and smooth feeling is preferable；
7 separately begin slightly has tangling phenomenon when combing, and easily combs later, slightly combs resistance hair soft, there is certain smooth
Sense；
5 separately begin has tangling phenomenon when combing, and is easier to comb later, has certain resistance hair that combs relatively soft, smooth feeling
It is unobvious；
3 points have stronger tangling phenomenon when combing, and are difficult to comb later, have stronger combing resistance hair harder, not smooth；
There is very strong tangling phenomenon during 1 point of combing, hardly possible is combed, there is very strong combing resistance hair coarse, it is very hard and dry.
Shampoo of the present invention is elastic, wet to hair water content, lifting hair gloss, hair it can be seen from upper table 1
Hair comb rationality, hair drying comb rationality, hair compliance have clear improvement.
The above-mentioned detailed description carried out with reference to embodiment to a kind of shampoo with hair care effect and preparation method thereof,
It is illustrative rather than limited, several embodiments can be included according to limited scope, therefore do not departing from this hair
Changing and modifications under bright general plotting, should belong within protection scope of the present invention.
Claims (7)
1. a kind of shampoo with hair care effect, it is characterised in that：By shield hair composition, lauryl sodium sulfate, 12
Sodium alkylether sulphate, propane diols, glycerine, cocamidopropyl propyl amide hydroxyl sulfo betaine, lauric acid amide of ethanol, preservative and
Water is constituted, and each component percentage by weight is as follows：
Surplus is water；Wherein,
The functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, heavy by its
Measure 2-10 parts of 1-5 parts of the number meter Semen sesami nigrum dregs of rice, 1-3 parts of rye, 1-3 parts of black rice, 3-10 parts of the black soya bean dregs of rice and the fleece-flower root.
2. the shampoo according to claim 1 with hair care effect, it is characterised in that：It is described shield hair composition be by
What following methods were prepared：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicinal material powder
End, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg40-55 DEG C of water in a kettle., then adjusted with 10% hydrochloric acid
PH value is saved to 3-5,0.2-1kg composite plant hydrolases is added and is dissolved, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.3-0.5%, in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation by alkali protease, neutral proteinase and
Papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-5：1-
3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT, leaving air temp 95 are used after collecting supernatant, concentration
DEG C, homogenization pressure 30MPa is spray-dried, and is produced.
3. the shampoo according to claim 1 with hair care effect, it is characterised in that：The shield hair composition presses it
4 parts of 4 parts of the parts by weight meter Semen sesami nigrum dregs of rice, 1 part of rye, 2 parts of black rice, 6 parts of the black soya bean dregs of rice and the fleece-flower root.
4. there is the preparation method of the shampoo of hair care effect described in claim 1, it is characterised in that：Specific preparation process is such as
Under：
I prepares shield hair composition：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicinal material powder
End, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg40-55 DEG C of water in a kettle., then adjusted with 10% hydrochloric acid
PH value is saved to 3-5,0.2-1kg composite plant hydrolases is added and is dissolved, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.3-0.5%, in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation by alkali protease, neutral proteinase and
Papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-5：1-
3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT, leaving air temp 95 are used after collecting supernatant, concentration
DEG C, homogenization pressure 30MPa is spray-dried, and is produced；
II prepares shampoo product according to conventional shampoo production technology.
5. the preparation method of the shampoo according to claim 4 with hair care effect, it is characterised in that：The step II
Middle shampoo production craft step is as follows：
(1) solution that hair composition is diluted to 10% will be protected, gained 10% hair composition dilute solution is protected into standby；
(2) by formula material lauryl sodium sulfate, sodium lauryl tri(oxyethyl) sulfate, disodium ethylene diamine tetraacetate, propane diols, sweet
Oil, Cocoamidopropyl betaine and lauric acid amide of ethanol are sequentially added in reactor not by prescription amount after filter pipeline
It is disconnected to stir, it is heated to being completely dissolved under the conditions of 90 DEG C, then cools；
(3) formula material mixed adds 10% when being cooled to 45-55 DEG C and protects hair composition dilute solution and preservative, slowly
After speed stirring 40 minutes, discharged when temperature drops to 40 DEG C.
6. the preparation method of the shampoo according to claim 5 with hair care effect, it is characterised in that：The step
(3) preservative is sodium benzoate, Phenoxyethanol, Sensiva SC50 or MIT in.
7. the preparation method of the shampoo according to claim 4 with hair care effect, it is characterised in that：The step I
(3) the weight ratio of neutral and alkali protease, neutral proteinase and papain is 4：3：1.
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| CN101721634A (en) * | 2009-12-15 | 2010-06-09 | 王洪亮 | Black corn extraction liquid |
| CN102784074A (en) * | 2012-07-19 | 2012-11-21 | 东华大学 | Functional hair washing shampoo and its preparation method |
| CN104288005A (en) * | 2014-09-20 | 2015-01-21 | 青岛点石文具用品有限公司 | Shampoo and preparation method thereof |
| CN105168074A (en) * | 2015-07-15 | 2015-12-23 | 碌柚葉（香港）有限公司 | Antidandruff and antipruritic traditional Chinese medicine composition and application and preparation method thereof |
| WO2016171464A1 (en) * | 2015-04-20 | 2016-10-27 | (주)이지희컴퍼니 | Composition for scalp and hair, containing green tea water |
| CN106616306A (en) * | 2017-02-10 | 2017-05-10 | 江西谷物源食品有限公司 | Instant hair blackening cereal staple food material and making method thereof |
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2017
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Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101721634A (en) * | 2009-12-15 | 2010-06-09 | 王洪亮 | Black corn extraction liquid |
| CN102784074A (en) * | 2012-07-19 | 2012-11-21 | 东华大学 | Functional hair washing shampoo and its preparation method |
| CN104288005A (en) * | 2014-09-20 | 2015-01-21 | 青岛点石文具用品有限公司 | Shampoo and preparation method thereof |
| WO2016171464A1 (en) * | 2015-04-20 | 2016-10-27 | (주)이지희컴퍼니 | Composition for scalp and hair, containing green tea water |
| CN105168074A (en) * | 2015-07-15 | 2015-12-23 | 碌柚葉（香港）有限公司 | Antidandruff and antipruritic traditional Chinese medicine composition and application and preparation method thereof |
| CN106616306A (en) * | 2017-02-10 | 2017-05-10 | 江西谷物源食品有限公司 | Instant hair blackening cereal staple food material and making method thereof |
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