CN106757263A - 一种金属表面纳秒脉冲等离子体制备纳米颗粒的溶液及制备方法 - Google Patents
一种金属表面纳秒脉冲等离子体制备纳米颗粒的溶液及制备方法 Download PDFInfo
- Publication number
- CN106757263A CN106757263A CN201611157802.9A CN201611157802A CN106757263A CN 106757263 A CN106757263 A CN 106757263A CN 201611157802 A CN201611157802 A CN 201611157802A CN 106757263 A CN106757263 A CN 106757263A
- Authority
- CN
- China
- Prior art keywords
- nano particle
- metal surface
- nanosecond pulse
- solution
- prepares
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000002105 nanoparticle Substances 0.000 title claims abstract description 43
- 229910052751 metal Inorganic materials 0.000 title claims abstract description 33
- 239000002184 metal Substances 0.000 title claims abstract description 33
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 238000000034 method Methods 0.000 claims abstract description 21
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 6
- 229910002804 graphite Inorganic materials 0.000 claims abstract description 6
- 239000010439 graphite Substances 0.000 claims abstract description 6
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims abstract description 5
- 239000011368 organic material Substances 0.000 claims abstract description 5
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical group [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 6
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Chemical compound [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 6
- QDZRBIRIPNZRSG-UHFFFAOYSA-N titanium nitrate Chemical compound [O-][N+](=O)O[Ti](O[N+]([O-])=O)(O[N+]([O-])=O)O[N+]([O-])=O QDZRBIRIPNZRSG-UHFFFAOYSA-N 0.000 claims description 5
- GSEJCLTVZPLZKY-UHFFFAOYSA-N Triethanolamine Chemical compound OCCN(CCO)CCO GSEJCLTVZPLZKY-UHFFFAOYSA-N 0.000 claims description 4
- 239000012153 distilled water Substances 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 239000008367 deionised water Substances 0.000 claims description 3
- 229910021641 deionized water Inorganic materials 0.000 claims description 3
- 235000011187 glycerol Nutrition 0.000 claims description 3
- 229910000027 potassium carbonate Inorganic materials 0.000 claims description 3
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical group [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 claims description 2
- 229910001388 sodium aluminate Inorganic materials 0.000 claims description 2
- 238000000926 separation method Methods 0.000 abstract description 2
- 239000003792 electrolyte Substances 0.000 description 9
- 229910052782 aluminium Inorganic materials 0.000 description 7
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 6
- 229910000883 Ti6Al4V Inorganic materials 0.000 description 5
- 235000013339 cereals Nutrition 0.000 description 4
- 239000004411 aluminium Substances 0.000 description 3
- 210000001367 artery Anatomy 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 210000003462 vein Anatomy 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 238000004070 electrodeposition Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 2
- 238000011020 pilot scale process Methods 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- -1 sodium aluminates Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 238000002679 ablation Methods 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000001354 calcination Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000007797 corrosion Effects 0.000 description 1
- 238000005260 corrosion Methods 0.000 description 1
- 230000008878 coupling Effects 0.000 description 1
- 238000010168 coupling process Methods 0.000 description 1
- 238000005859 coupling reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 238000003487 electrochemical reaction Methods 0.000 description 1
- 230000005518 electrochemistry Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000002071 nanotube Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000004544 sputter deposition Methods 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/024—Anodisation under pulsed or modulated current or potential
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/04—Anodisation of aluminium or alloys based thereon
- C25D11/06—Anodisation of aluminium or alloys based thereon characterised by the electrolytes used
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D11/00—Electrolytic coating by surface reaction, i.e. forming conversion layers
- C25D11/02—Anodisation
- C25D11/26—Anodisation of refractory metals or alloys based thereon
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Nanotechnology (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Manufacturing & Machinery (AREA)
- Crystallography & Structural Chemistry (AREA)
- Powder Metallurgy (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
Abstract
Description
Claims (8)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611157802.9A CN106757263B (zh) | 2016-12-15 | 2016-12-15 | 一种金属表面纳秒脉冲等离子体制备纳米颗粒的溶液及制备方法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201611157802.9A CN106757263B (zh) | 2016-12-15 | 2016-12-15 | 一种金属表面纳秒脉冲等离子体制备纳米颗粒的溶液及制备方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN106757263A true CN106757263A (zh) | 2017-05-31 |
CN106757263B CN106757263B (zh) | 2018-12-18 |
Family
ID=58888355
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201611157802.9A Active CN106757263B (zh) | 2016-12-15 | 2016-12-15 | 一种金属表面纳秒脉冲等离子体制备纳米颗粒的溶液及制备方法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN106757263B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108588789A (zh) * | 2018-04-26 | 2018-09-28 | 河海大学常州校区 | 一种制备硼钛化合物膜层的处理溶液及硼钛化合物的制备方法 |
CN108754579A (zh) * | 2018-06-19 | 2018-11-06 | 河海大学常州校区 | 一种钢防腐蚀环境友好型反渗透薄膜的制备溶液及其制备方法 |
CN110512265A (zh) * | 2019-10-12 | 2019-11-29 | 河海大学常州校区 | 一种镁合金表面复合膜及其制备方法 |
Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1884630A (zh) * | 2006-06-01 | 2006-12-27 | 厦门大学 | 一种高长径比二氧化钛纳米管阵列的制备方法 |
CN101280450A (zh) * | 2008-05-08 | 2008-10-08 | 南昌航空大学 | 一种减少钛合金表面摩擦系数的微弧氧化工艺 |
CN101311326A (zh) * | 2007-05-25 | 2008-11-26 | 比亚迪股份有限公司 | 一种用于轻金属微弧氧化的电解液及微弧氧化方法 |
CN101348932A (zh) * | 2008-08-27 | 2009-01-21 | 哈尔滨工程大学 | Mg-Li合金的等离子体电解氧化方法 |
CN102199785A (zh) * | 2011-06-29 | 2011-09-28 | 上海理工大学 | 一种钛合金耐磨涂层的微弧氧化溶液及其应用 |
CN102575357A (zh) * | 2009-07-02 | 2012-07-11 | 日本帕卡濑精株式会社 | 不含铬和氟的金属表面用化学转化处理液、金属表面处理方法及金属表面涂装方法 |
US20150275387A1 (en) * | 2012-11-22 | 2015-10-01 | Eads Deutschland Gmbh | Method for the Nanostructuring and Anodization of a Metal Surface |
WO2016086914A2 (de) * | 2014-12-04 | 2016-06-09 | Meotec GmbH & Co. KG | Bauteil einer turboeinrichtung, brennkraftmaschine mit einer turboeinrichtung und verfahren zum herstellen eines turboeinrichtungsbauteils |
-
2016
- 2016-12-15 CN CN201611157802.9A patent/CN106757263B/zh active Active
Patent Citations (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1884630A (zh) * | 2006-06-01 | 2006-12-27 | 厦门大学 | 一种高长径比二氧化钛纳米管阵列的制备方法 |
CN101311326A (zh) * | 2007-05-25 | 2008-11-26 | 比亚迪股份有限公司 | 一种用于轻金属微弧氧化的电解液及微弧氧化方法 |
CN101280450A (zh) * | 2008-05-08 | 2008-10-08 | 南昌航空大学 | 一种减少钛合金表面摩擦系数的微弧氧化工艺 |
CN101348932A (zh) * | 2008-08-27 | 2009-01-21 | 哈尔滨工程大学 | Mg-Li合金的等离子体电解氧化方法 |
CN102575357A (zh) * | 2009-07-02 | 2012-07-11 | 日本帕卡濑精株式会社 | 不含铬和氟的金属表面用化学转化处理液、金属表面处理方法及金属表面涂装方法 |
CN102199785A (zh) * | 2011-06-29 | 2011-09-28 | 上海理工大学 | 一种钛合金耐磨涂层的微弧氧化溶液及其应用 |
US20150275387A1 (en) * | 2012-11-22 | 2015-10-01 | Eads Deutschland Gmbh | Method for the Nanostructuring and Anodization of a Metal Surface |
WO2016086914A2 (de) * | 2014-12-04 | 2016-06-09 | Meotec GmbH & Co. KG | Bauteil einer turboeinrichtung, brennkraftmaschine mit einer turboeinrichtung und verfahren zum herstellen eines turboeinrichtungsbauteils |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN108588789A (zh) * | 2018-04-26 | 2018-09-28 | 河海大学常州校区 | 一种制备硼钛化合物膜层的处理溶液及硼钛化合物的制备方法 |
CN108754579A (zh) * | 2018-06-19 | 2018-11-06 | 河海大学常州校区 | 一种钢防腐蚀环境友好型反渗透薄膜的制备溶液及其制备方法 |
CN110512265A (zh) * | 2019-10-12 | 2019-11-29 | 河海大学常州校区 | 一种镁合金表面复合膜及其制备方法 |
CN110512265B (zh) * | 2019-10-12 | 2021-07-27 | 河海大学常州校区 | 一种镁合金表面复合膜及其制备方法 |
Also Published As
Publication number | Publication date |
---|---|
CN106757263B (zh) | 2018-12-18 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
Kashapov et al. | Research of the impact acidity of electrolytic cathode on the course of the plasma-electrolytic process | |
CN106757263A (zh) | 一种金属表面纳秒脉冲等离子体制备纳米颗粒的溶液及制备方法 | |
Taylor et al. | Electrochemical surface finishing | |
DE1515323A1 (de) | Verfahren zum Erzeugen eines Schutzfilmes auf einer festen Unterlage | |
CN104291328B (zh) | 石墨烯材料的分级分离方法 | |
CN103695980A (zh) | 一种铝合金表面单层微弧氧化陶瓷膜的制备方法 | |
CN112276097A (zh) | 一种3d打印钛合金复杂零部件的表面抛光方法 | |
Wang et al. | Analytical study on mechanism of electrolysis and plasma polishing | |
CN111515480B (zh) | 一种微粒辅助掩膜电解加工的装置及方法 | |
CN104894628A (zh) | 阶段升压制备镁合金微弧氧化陶瓷层的方法 | |
CN105127525B (zh) | 一种微电解放电加工工作液及微电解放电加工方法 | |
CN104532320A (zh) | 一种铝、钛合金微弧陶瓷膜的制备方法 | |
Wang et al. | Study on energy consumption of Al2O3 coating prepared by cathode plasma electrolytic deposition | |
WO2006078338A3 (en) | Process and apparatus for cleaning and/or coating conductive metal surfaces using electro-plasma processing | |
KR20130028856A (ko) | 산화 피막 형성방법 | |
Di et al. | Preparation of copper nanoparticles using dielectric barrier discharge at atmospheric pressure and its mechanism | |
CN104108053A (zh) | 大型复杂金属表面等离子体与脉冲放电复合抛光加工方法 | |
CN108545784A (zh) | 一种小尺寸金属氧化物纳米片及其制备方法 | |
KR20170112026A (ko) | 그래핀의 제조 방법 | |
CN103572348A (zh) | 一种铝型材表面微弧氧化处理的方法 | |
CN103103593B (zh) | 一种铝、镁、钛或其合金的表面陶瓷氧化方法 | |
Arakawa et al. | Novel charge/discharge method for lead acid battery by high-pressure crystallization | |
CN102995097A (zh) | 镁合金表面蚀刻电解质溶液及其蚀刻方法 | |
CN105525325A (zh) | 一种金属合金的表面处理方法 | |
CN105112981A (zh) | 阶段升压制备镁合金微弧氧化陶瓷层的方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
GR01 | Patent grant | ||
GR01 | Patent grant | ||
TR01 | Transfer of patent right | ||
TR01 | Transfer of patent right |
Effective date of registration: 20201218 Address after: 213000 Zhenxi Industrial Park, Henglin Town, Wujin District, Changzhou City, Jiangsu Province Patentee after: Changzhou Shengxiang Intelligent Technology Co.,Ltd. Address before: 213022, No. 200 Jinling North Road, Jiangsu, Changzhou Patentee before: CHANGZHOU CAMPUS OF HOHAI University |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: A solution and preparation method for nanosecond pulse plasma preparation of nanoparticles on metal surfaces Granted publication date: 20181218 Pledgee: Bank of China Limited Changzhou Economic Development Zone sub branch Pledgor: Changzhou Shengxiang Intelligent Technology Co.,Ltd. Registration number: Y2024980025172 |