CN104818114A - Preparation method and applications of indigofera stachyodes extract - Google Patents
Preparation method and applications of indigofera stachyodes extract Download PDFInfo
- Publication number
- CN104818114A CN104818114A CN201510097843.2A CN201510097843A CN104818114A CN 104818114 A CN104818114 A CN 104818114A CN 201510097843 A CN201510097843 A CN 201510097843A CN 104818114 A CN104818114 A CN 104818114A
- Authority
- CN
- China
- Prior art keywords
- conopsea extraction
- stachyodes
- indigofera
- snow
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Cosmetics (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention provides a preparation method and applications of an indigofera stachyodes extract. The preparation method comprises: 1) crushing indigofera stachyodes, adding ethanol with the amount 5-20 time the mass, and carrying out heating extraction 1-3 times at a temperature of 60-100 DEG C, wherein each extraction time is 1-3 h; 2) filtering the extraction solutions, combining, concentrating, and adding an ester solvent having the amount of 3-10 times the mass of the paste when concentrating the combined filtrate to achieve the mass of 2-5 times the mass of the raw material; and 3) filtering the mixing solution so as to obtain the indigofera stachyodes extract. According to the present invention, the indigofera stachyodes extract is used for flavoring the cigarette holder rod, the preparation method and the application operation of the indigofera stachyodes extract are simple, the method is suitable for mass production, the indigofera stachyodes extract is coordinated with the cigarette holder rod aroma after being added, no odor feeling exists, and a certain health effect is provided.
Description
Technical field
The invention belongs to the tobacco spice Synthesis and applications field in cigarette technology, especially a kind of preparation method and application thereof avenging conopsea extraction.
Background technology
Realize the today improved constantly consumer health, human consumer trends towards the many aspects such as low evil, safety, health more for the demand of cigarette product.In a sense, a main object of " reducing tar and reducing harm " is exactly to develop the low tar less harmful product meeting consumer demand, meet psychology and the psychological need of human consumer, try one's best and reduce cigarette to healthy the caused hazardness of human consumer.But " fall Jiao " or " double-edged sword ", it, while effectively reducing the objectionable constituent in cigarette smoke, also can make the aspect such as original suction taste, mouthfeel, physiological strength of cigarette follow corresponding reduction.So this carries out part with regard to needing make up by adding other spices, one of effect of perfuming be reduce cigarette endanger while, make up the loss of fragrance, provide satisfied product to human consumer.
In the history of cigarette material development, filter tip is the innovation of revolution, and the development situation of Tobacco Control campaign has been complied with in its appearance, also makes the objectionable constituent optionally reducing or remove in cigarette become possibility; Burnt part aroma quality and perfume quantity of inevitably losing cigarette fall in Harm reduction techniques, taste is easily made to lose original style, this carries out part with regard to needing make up by adding other spices, one of effect of perfuming is reducing cigarette harm while, make up the loss of fragrance, provide satisfied product to human consumer.
Summary of the invention
The object of the present invention is to provide a kind of simple to operate, be applicable to scale operation, add rear and mouth rod smell coordination, be as good as sense of taste, and there is preparation method and the application thereof of the snow conopsea extraction of certain health-care effect.
For reaching this object, the present invention by the following technical solutions:
Avenge a preparation method for conopsea extraction, comprise the following steps:
1) first snow ginseng is pulverized, add the ethanol of 5 ~ 20 quality multiples, 60 ~ 100 DEG C of heating extractions 1 ~ 3 time, each 1 ~ 3h;
2) after extracting liquid filtering, merging is concentrated, and when being condensed into raw materials quality 2 ~ 5 times, the esters solvent adding lotion quality 3 ~ 10 dissolves;
3) mixed solution is filtered, namely obtain avenging conopsea extraction.
Further, in step 2) in, described esters solvent comprises single product and two or more the allotment product of sweet oil, soybean oil, salad oil, plam oil, rapeseed oil and tea-seed oil.
Another technical problem that the present invention will solve is for providing a kind of application avenging conopsea extraction:
Snow conopsea extraction is used for mouth rod perfuming.
Further, selected organic solvent to be massfraction be 30% ~ 95% ethanol.
Further, described mouth rod perfuming 0.05 ~ 0.8% is added in mouth sticklac capsule in mass ratio by snow conopsea extraction, is processed into perfuming mouth rod and is applied to cigarette.
In Guangxi, Yunnan, Guizhou edible snow ginseng among the people is with a long history, thinks that snow joins the effect having anti-inflammatory, relieve inflammation or internal heat, protect liver, improving eyesight and sober up, without any toxicity.This invention is condensed into cream, dissolves with esters solvent after being extracted by snow ginseng organic solvent, and the snow conopsea extraction obtained after filtration is for mouth rod perfuming.Effectively can promote the perfume quantity of cigarette, improve the cigarette taste bad situation that punching waits the measure of mouth rod reducing tar and reducing harm to cause.
Beneficial effect of the present invention is: first by having anti-inflammatory, relieve inflammation or internal heat, protect liver, improving eyesight and the Chinese medicine snow ginseng of effect of sobering up is used for mouth rod perfuming, preparation technology is simple, snow conopsea extraction has the delicate fragrance of its uniqueness, add rear and mouth rod smell coordination, the cigarette that can promote cigarette is fragrant, the suction quality of cigarette can be improved again, certain health-care effect can also be played.
Embodiment
Embodiment 1
Snow ginseng adds the ethanol of 5 quality multiples after pulverizing, 60 DEG C of heating extractions 3 times, and each 1 hour; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 2 times, the sweet oil adding lotion quality 3 times dissolves; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Embodiment 2
Snow ginseng adds the ethanol of 8 quality multiples after pulverizing, 65 DEG C of heating extractions 3 times, and each 1.5 hours; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 3 times, the soybean oil adding lotion quality 4 times is dissolved; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Embodiment 3
Snow ginseng adds the ethanol of 10 quality multiples after pulverizing, 70 DEG C of heating extractions 2 times, and each 2 hours; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 4 times, the salad oil adding lotion quality 5 times dissolves; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Embodiment 4
Snow ginseng adds the ethanol of 12 quality multiples after pulverizing, 75 DEG C of heating extractions 1 time, and each 2.5 hours; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 5 times, the plam oil adding lotion quality 6 times dissolves; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Embodiment 5
Snow ginseng adds the ethanol of 15 quality multiples after pulverizing, 80 DEG C of heating extractions 2 times, and each 3 hours; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 4 times, the rapeseed oil adding lotion quality 7 times dissolves; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Embodiment 6
Snow ginseng adds the ethanol of 18 quality multiples after pulverizing, 90 DEG C of heating extractions 3 times, and each 3 hours; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 3 times, the tea-seed oil adding lotion quality 8 times dissolves; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Embodiment 7
Snow ginseng adds the ethanol of 20 quality multiples after pulverizing, 100 DEG C of heating extractions 2 times, and each 2 hours; Merge concentrated after extracting liquid filtering, when being condensed into raw materials quality 2 times, the allotment product adding the sweet oil of lotion quality 10 times, soybean oil, salad oil, plam oil, rapeseed oil and tea-seed oil dissolve; Mixed solution is filtered, namely obtains avenging conopsea extraction.
Cigarette filter tip perfuming
The snow conopsea extraction 1,2,3,4,5,6 and 7 that above-mentioned example is obtained, after being evenly injected into 7 parts of mouth sticklac capsules by 0.05%, 0.1%, 0.2%, 0.3%, 0.4%, 0.6%, 0.8% respectively, carry out contrast with blank to smoke panel test, the overall organoleptic's test-results obtained represents as follows.
Snow conopsea extraction cigarette filter tip perfuming sensory evaluating smoking result
| Example | Smoking result (compared with the control) |
| 1 | The fragrant mildness flavouring of cigarette, has fresh and sweet perfume (or spice) |
| 2 | Pleasant impression is comparatively clean, and flue gas conglobation property is good |
| 3 | Fresh and sweet perfume (or spice) is obvious, perfume quantity foot |
| 4 | Comfortableness promotes obviously, perfume quantity foot |
| 5 | Flue gas is clear bright, and the property sent out is good thoroughly |
| 6 | Slightly aobvious pressure is fragrant, good after-taste |
| 7 | Pressure perfume (or spice) is slightly heavy, perfume quantity foot |
Beneficial effect of the present invention: first by having anti-inflammatory, relieve inflammation or internal heat, protect liver, improving eyesight and the Chinese medicine snow ginseng of effect of sobering up is used for mouth rod perfuming, preparation technology is simple, snow conopsea extraction has the delicate fragrance of its uniqueness, add rear and mouth rod smell coordination, the cigarette that can promote cigarette is fragrant, the suction quality of cigarette can be improved again, certain health-care effect can also be played.
Below the present invention be described in detail, the above, be only the preferred embodiment of the present invention, when not limiting the scope of the present invention, namely allly does impartial change according to the application's scope and modify, all should still belong in covering scope of the present invention.
Claims (5)
1. avenge a preparation method for conopsea extraction, it is characterized in that: comprise the following steps:
1) first snow ginseng is pulverized, add the ethanol of 5 ~ 20 quality multiples, 60 ~ 100 DEG C of heating extractions 1 ~ 3 time, each 1 ~ 3h;
2) after extracting liquid filtering, merging is concentrated, and when being condensed into raw materials quality 2 ~ 5 times, the esters solvent adding lotion quality 3 ~ 10 dissolves;
3) mixed solution is filtered, namely obtain avenging conopsea extraction.
2. a kind of preparation method avenging conopsea extraction as claimed in claim 1, it is characterized in that: in step 2) in, described esters solvent comprises single product and two or more the allotment product of sweet oil, soybean oil, salad oil, plam oil, rapeseed oil and tea-seed oil.
3. an application for snow conopsea extraction as claimed in claim 1, is characterized in that: snow conopsea extraction is used for mouth rod perfuming.
4. a kind of application avenging conopsea extraction as claimed in claim 3, is characterized in that: selected organic solvent to be massfraction be 30% ~ 95% ethanol.
5. a kind of application avenging conopsea extraction as claimed in claim 3, is characterized in that: described mouth rod perfuming 0.05 ~ 0.8% is added in mouth sticklac capsule in mass ratio by snow conopsea extraction, is processed into perfuming mouth rod and is applied to cigarette.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510097843.2A CN104818114A (en) | 2015-03-05 | 2015-03-05 | Preparation method and applications of indigofera stachyodes extract |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201510097843.2A CN104818114A (en) | 2015-03-05 | 2015-03-05 | Preparation method and applications of indigofera stachyodes extract |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104818114A true CN104818114A (en) | 2015-08-05 |
Family
ID=53728598
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201510097843.2A Pending CN104818114A (en) | 2015-03-05 | 2015-03-05 | Preparation method and applications of indigofera stachyodes extract |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104818114A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105249531A (en) * | 2015-08-06 | 2016-01-20 | 云南中烟工业有限责任公司 | Method for preparing phoebe zhennan extracts and application thereof |
| CN106539124A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | A kind of cigarette filter tip additive and preparation method thereof |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1360858A (en) * | 2000-12-25 | 2002-07-31 | 颐中烟草(集团)有限公司青州卷烟厂 | Health cigarette |
| CN101317690A (en) * | 2008-07-03 | 2008-12-10 | 广西中烟工业公司 | Additive agent for osmanthus fragrance type cigarette, preparation and application thereof |
| CN101570716A (en) * | 2009-06-01 | 2009-11-04 | 无锡华海香料有限公司 | Method for extracting natural Chinese medicinal herb fragrance component and application of extract thereof |
| CN101843364A (en) * | 2010-02-26 | 2010-09-29 | 湖北中烟工业有限责任公司 | Spice additive for natural cigarettes and preparation method thereof |
| CN101974367A (en) * | 2009-06-23 | 2011-02-16 | 湖北中烟工业有限责任公司 | Novel flavor-enhancing and harm-reducing natural spice for tobacco and use thereof |
| CN103361173A (en) * | 2013-07-26 | 2013-10-23 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
-
2015
- 2015-03-05 CN CN201510097843.2A patent/CN104818114A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1360858A (en) * | 2000-12-25 | 2002-07-31 | 颐中烟草(集团)有限公司青州卷烟厂 | Health cigarette |
| CN101317690A (en) * | 2008-07-03 | 2008-12-10 | 广西中烟工业公司 | Additive agent for osmanthus fragrance type cigarette, preparation and application thereof |
| CN101570716A (en) * | 2009-06-01 | 2009-11-04 | 无锡华海香料有限公司 | Method for extracting natural Chinese medicinal herb fragrance component and application of extract thereof |
| CN101974367A (en) * | 2009-06-23 | 2011-02-16 | 湖北中烟工业有限责任公司 | Novel flavor-enhancing and harm-reducing natural spice for tobacco and use thereof |
| CN101843364A (en) * | 2010-02-26 | 2010-09-29 | 湖北中烟工业有限责任公司 | Spice additive for natural cigarettes and preparation method thereof |
| CN103361173A (en) * | 2013-07-26 | 2013-10-23 | 上海华宝生物科技有限公司 | Preparation method of controllable-releasing and warm-wet-environment-resistance vegetable glue compound cigarette capsule, product obtained and applications thereof |
Non-Patent Citations (1)
| Title |
|---|
| 张忠诚等: ""中国雪参化学成份的研究----人参甙的分离和鉴定"", 《人参研究》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105249531A (en) * | 2015-08-06 | 2016-01-20 | 云南中烟工业有限责任公司 | Method for preparing phoebe zhennan extracts and application thereof |
| CN106539124A (en) * | 2016-10-20 | 2017-03-29 | 云南中烟工业有限责任公司 | A kind of cigarette filter tip additive and preparation method thereof |
| CN106539124B (en) * | 2016-10-20 | 2018-05-29 | 云南中烟工业有限责任公司 | A kind of preparation method of cigarette filter tip additive |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103989245B (en) | The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity | |
| CN104388192A (en) | Rose-type essence for cigarettes for women and application of flavor | |
| CN110699183A (en) | Tobacco essence with spicy fragrance | |
| CN111671134A (en) | Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid | |
| CN104327950A (en) | Green tea extract containing Maillard reaction reactant, its preparation method and its application | |
| CN106418669A (en) | High-sweet-returning-feeling spice for cigarettes and preparation method and application of high-sweet-returning-feeling spice | |
| CN105542958A (en) | Additive and method for supplementing sweetness and fragrance of cigarette | |
| CN101569438A (en) | Method for preparing mulberry cigarette flavor | |
| CN106433990B (en) | A kind of Siraitia grosvenorii essence, preparation method and its application in cigarette | |
| CN100593565C (en) | Petroleum extracted sophora flower extractum and its application in perfuming cigarette | |
| CN101637303A (en) | Lemon extract, preparation method thereof and application thereof in cigarette flavoring | |
| CN104818114A (en) | Preparation method and applications of indigofera stachyodes extract | |
| CN101822418A (en) | Tea stem extract of oolong tea and preparation method and application thereof | |
| CN106305939A (en) | Roughage Chinese medicine biscuit and production method thereof | |
| CN103828962A (en) | Preparation technology of honeysuckle and black tea compound tea beverage | |
| CN103469680A (en) | Lining paper coated with oolong tea extract-containing composition | |
| CN103497834A (en) | Method for preparing dandelion absolute oil and application of dandelion absolute oil in cigarettes | |
| CN103351951B (en) | Cigarette essence capable of improving quality of cigarettes | |
| CN110771944A (en) | Apocynum venetum health-care cigarette and preparation method thereof | |
| KR20120111114A (en) | Method for making onion juice | |
| CN102499433B (en) | Application of suberenol extract in cigarette flavoring additive | |
| CN109022151A (en) | A kind of cigarette of Siraitia grosvenorii flavor quick-fried pearl liquid and preparation method thereof | |
| KR101842842B1 (en) | Method of preparing seasoning compositions | |
| CN109864328A (en) | One grows tea and Maca composition, preparation method and applications | |
| CN105249531A (en) | Method for preparing phoebe zhennan extracts and application thereof |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| EXSB | Decision made by sipo to initiate substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20150805 |
|
| WD01 | Invention patent application deemed withdrawn after publication |