CN103880402A - Preparation method for high-emissivity far-infrared health-care purple-sand porcelain slice - Google Patents
Preparation method for high-emissivity far-infrared health-care purple-sand porcelain slice Download PDFInfo
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- CN103880402A CN103880402A CN201210552300.1A CN201210552300A CN103880402A CN 103880402 A CN103880402 A CN 103880402A CN 201210552300 A CN201210552300 A CN 201210552300A CN 103880402 A CN103880402 A CN 103880402A
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Abstract
A preparation method for a high-emissivity far-infrared health-care purple-sand porcelain slice is disclosed, and mainly solves the problems that conventional purple-sand products are excessively traditional and monotonous, and functional products are less. The preparation method comprises the following steps: material preparing, grinding, granulating, compaction molding, drying and sintering. The raw materials comprises in parts by weight: 100 parts of a purple-sand raw material, 10-20 parts of Chinese medical stone, 45-60 parts of a disperse medium water and 0.45-0.75 part of a dispersant water glass. The preparation method comprises the advantages that by utilizing the far-infrared emission function of purple sand and adding a proper amount of Chinese medical stone, the prepared purple-sand porcelain is applied to summer sleeping mats or heating blankets, and gives play to effects of improving sleep quality, promoting and improving blood circulation, enhancing metabolism, improving immunity and adjusting body metabolism, and delaying organ failure process, thereby reaching the health-care effects of delaying aging, prolonging life span and the like.
Description
Technical field
The invention belongs to ceramic material field, be specifically related to a kind of preparation method of high emissivity far infrared health care boccaro ceramics.
Background technology
The special construction having due to boccaro makes its goods have very high enjoying value and use value.Dark-red enameled pottery can keep the color of tea, not perishable spoiling and turning sour; Boccaro flowerpot is grown flowers and is difficult for rotten, the features such as favourable plant-growth.Although red stoneware product has above-mentioned advantage, it is few that traditional product exists kind, function singleness, and technology content is not high, can not meet the more demand of people.
Summary of the invention
Too tradition is dull to the object of the invention is to make up existing red stoneware product, and the deficiency that functional product is few, utilizes boccaro can launch far function, and a kind of preparation method of high emissivity far infrared health care boccaro ceramics is provided.
For achieving the above object, the present invention adopts following technical proposals: a kind of preparation method of high emissivity far infrared health care boccaro ceramics, this preparation method comprises batching, grinding, granulation, compression moulding, dry and sintering, and aforesaid method is realized by following processing step:
(1) batching and grinding technics: weight share takes 100 parts of boccaro raw materials; 10~20 parts of medical stones; 45~60 parts, dispersion medium water; 0.45~0.75 part of dispersion agent water glass.
By above-mentioned boccaro raw material, medical stone, dispersion agent and water, put into quick mill (in grinding pot the quality of ball be siccative quality 1.5-2 doubly) in grind after 2 minutes, obtain the slurry of good fluidity.
(2) granulation and compression moulding technique: by slurry granulation in spray-drying tower, adopt pressure forming machine to be pressed into the shape (as circle, rhombus, hexagon etc.) of requirement by different moulds.
(3) dry and sintering process: print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on the resistance furnace (SX that is rapidly heated
3-10-14) middle 1100-1160 DEG C of sintering, soaking time 30 minutes, is prepared into boccaro ceramics.
(4) water-intake rate detects: the boccaro ceramics preparing is dried 2 hours in 120 DEG C of baking ovens, weigh quality and record m
1, be put in boiling water and boil 2 hours 30 minutes, wait after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture (to surperficial anhydrous light), take its quality m
2, utilize formula 1. to calculate water-intake rate.Require water-intake rate to be less than 0.5%.
Water-intake rate a=(m
2-m
1)/m
1× 100% .... 1.
In formula: a---water-intake rate, %;
M
1---the quality of the boccaro ceramics after oven dry, g;
M
2---the quality of the boccaro ceramics after water suction, g.
Advantage of the present invention: the far-infrared transmitting function that utilizes boccaro, add suitable medical stone, be prepared into boccaro ceramics and be applied to summer sleeping mat or electric blanket, play and improve sleep quality, promotion and improve blood circulation, strengthen metabolism, improve immunizing power and regulate organism metabolism, delay organ failure process, and then reach the health-care effecies such as the object that delays senility, promotes longevity.
Be mainly reflected in:
(1) far infrared function.Boccaro and medical stone all have very strong far-infrared transmitting function, can activate the macromolecular activity such as biotinylated nucleic acid protein, regulate the movable function such as organism metabolism, immunity, are conducive to the restore peace weighing apparatus of body function, reach the object of preventing and curing diseases; Promote and improve blood circulation, strengthen metabolism, improve immunologic function; There is anti-inflammatory and detumescence, analgesia, the microcirculatory effect of improvement; Reduce the viscosity of blood, increase volume of blood flow, expansion capillary blood vessel, in minimizing blood vessel, the quantity of blood fat, makes vessel wall smooth, reduces arteriosclerosis.The most important thing is that far infrared can accelerate blood circulation, make metabolism more vigorous, improve body tissue organ dysfunction, delay organ failure process, often in good running status, reach the object that human body delays senility, promotes longevity.
(2) give human body trace element supplement.Contain the mineral elements such as a large amount of iron, calcium, potassium, sodium, zinc due to boccaro.Boccaro ceramics and skin contact, these trace elements are penetrated in body by pore, can be used as the warehouse of needed by human body trace element, supplement in time the trace element of needed by human body, regulate organism balance.
(3) good adsorption function.Because medical stone has good adsorption function, in the time of medical stone and skin contact, superoxide rubbish harmful in human body is had to very strong adsorption function, thereby promote the excretion of pore endoperoxide rubbish, dredging capillary vessel, make capillary vessel keep normal metabolism and physiological function, play the effect for the treatment of and prevention multiple dermatosis.
Embodiment
Due to the difference of various places Red Stone Ware performance, the present invention is taking the boccaro in boccaro ore deposit, Fuxin as example, and this Red Stone Ware performance is as follows,
Table 1 chemical composition analysis
Element | SiO 2 | Al 2O 3 | Fe 2O 3 | TiO 2 | CaO | MgO | K 2O | N 2O |
Boccaro | 66.11 | 15.76 | 5.63 | 0.8 | 0.54 | 1.29 | 4.07 | 0.98 |
Embodiment 1
Take 400g boccaro raw material, 40g medical stone, 1.8ml water glass and 240ml water, put in quick mill (in grinding pot, the quality of ball is 1.5 times of siccative quality) and grind 2 minutes, obtain slurry.By slurry granulation in spray-drying tower, be pressed into the shape (as circle, rhombus, hexagon etc.) of requirement by pressure forming machine.Print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on the resistance furnace (SX that is rapidly heated
3-10-14) in 1160 DEG C of sintering, soaking time 30 minutes, is prepared into boccaro ceramics.
The boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture (to surperficial anhydrous light), take its quality, calculating water-intake rate is 0.029%.
Embodiment 2
Take 400g boccaro raw material, 40g medical stone, 1.8ml water glass and 240ml water, put in quick mill (in grinding pot, the quality of ball is 1.5 times of siccative quality) and grind 2 minutes, obtain slurry.By slurry granulation in spray-drying tower, be pressed into the shape (as circle, rhombus, hexagon etc.) of requirement by pressure forming machine.Print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on the resistance furnace (SX that is rapidly heated
3-10-14) in 1120 DEG C of sintering, soaking time 30 minutes, is prepared into boccaro ceramics.
The boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture (to surperficial anhydrous light), take its quality, calculating water-intake rate is 0.34%.
Embodiment 3
Take 400g boccaro raw material, 80g medical stone, 3ml water glass and 180ml water, put in quick mill (in grinding pot, the quality of ball is 1.5 times of siccative quality) and grind 2 minutes, obtain slurry.By slurry granulation in spray-drying tower, be pressed into the shape (as circle, rhombus, hexagon etc.) of requirement by press-forming machine.Print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on the resistance furnace (SX that is rapidly heated
3-10-14) in 1100 DEG C of sintering, soaking time 30 minutes, is prepared into boccaro ceramics.
The boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture (to surperficial anhydrous light), take its quality, calculating water-intake rate is 0.18%.
Embodiment 4
Take 400g boccaro raw material, 60g medical stone, 2ml water glass and 220ml water, put in quick mill (in grinding pot, the quality of ball is 2 times of siccative quality) and grind 2 minutes, obtain slurry.By slurry granulation in spray-drying tower, be pressed into the shape (as circle, rhombus, hexagon etc.) of requirement by pressure forming machine.Print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on the resistance furnace (SX that is rapidly heated
3-10-14) in 1100 DEG C of sintering, soaking time 30 minutes, is prepared into boccaro ceramics.
The boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture (to surperficial anhydrous light), take its quality, calculating water-intake rate is 0.22%.
Claims (7)
1. a preparation method for high emissivity far infrared health care boccaro ceramics, this preparation method comprises batching, grinding, granulation, compression moulding, dry and sintering, aforesaid method is realized by following processing step:
(1) batching and grinding technics: weight share takes 100 parts of boccaro raw materials; 10~20 parts of medical stones; 45~60 parts, dispersion medium water; 0.45~0.75 part of dispersion agent water glass;
By above-mentioned boccaro raw material, medical stone, dispersion agent and water, put in quick mill and grind after 2 minutes, obtain the slurry of good fluidity;
(2) granulation and compression moulding technique: by slurry granulation in spray-drying tower, adopt pressure forming machine to be pressed into the shape of requirement by different moulds;
(3) dry and sintering process: print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C, be then placed on 1100-1160 DEG C of sintering in the resistance furnace that is rapidly heated, soaking time 30 minutes, is prepared into boccaro ceramics;
(4) water-intake rate detects: the boccaro ceramics preparing is dried 2 hours in 120 DEG C of baking ovens, weigh quality record, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture, take its quality, utilize formula to calculate water-intake rate, require water-intake rate to be less than 0.5%.
2. the preparation method of a kind of high emissivity far infrared health care boccaro ceramics as claimed in claim 1, in the method, in the grinding pot of described quick mill the quality of ball be siccative quality 1.5-2 doubly.
3. the preparation method of a kind of high emissivity far infrared health care boccaro ceramics as claimed in claim 1, in the method, described in be pressed into requirement be shaped as circle, rhombus or hexagon.
4. the preparation method of a kind of high emissivity far infrared health care boccaro ceramics as claimed in claim 1, the concrete steps of the method:
Take 400g boccaro raw material, 40g medical stone, 1.8ml water glass and 240ml water, put in quick mill and grind 2 minutes, in grinding pot, the quality of ball is 1.5 times of siccative quality, obtain slurry, by slurry granulation in spray-drying tower, be pressed into the shape of requirement by pressure forming machine, print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C, then be placed on 1160 DEG C of sintering in the resistance furnace that is rapidly heated, soaking time 30 minutes, be prepared into boccaro ceramics, the boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture, take its quality, calculating water-intake rate is 0.029%.
5. the preparation method of a kind of high emissivity far infrared health care boccaro ceramics as claimed in claim 1, the concrete steps of the method:
Take 400g boccaro raw material, 40g medical stone, 1.8ml water glass and 240ml water, put in quick mill and grind 2 minutes, in grinding pot, the quality of ball is 1.5 times of siccative quality, obtain slurry, by slurry granulation in spray-drying tower, be pressed into the shape of requirement by pressure forming machine, print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on 1120 DEG C of sintering in the resistance furnace that is rapidly heated, soaking time 30 minutes, be prepared into boccaro ceramics, the boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture, take its quality, calculating water-intake rate is 0.34%.
6. the preparation method of a kind of high emissivity far infrared health care boccaro ceramics as claimed in claim 1, the concrete steps of the method:
Take 400g boccaro raw material, 80g medical stone, 3ml water glass and 180ml water, put in quick mill and grind 2 minutes, in grinding pot, the quality of ball is 1.5 times of siccative quality, obtain slurry, by slurry granulation in spray-drying tower, be pressed into the shape of requirement by press-forming machine, print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C, then be placed on 1100 DEG C of sintering in the resistance furnace that is rapidly heated, soaking time 30 minutes, be prepared into boccaro ceramics, the boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture, take its quality, calculating water-intake rate is 0.18%.
7. the preparation method of a kind of high emissivity far infrared health care boccaro ceramics as claimed in claim 1, the concrete steps of the method:
Take 400g boccaro raw material, 60g medical stone, 2ml water glass and 220ml water, put in quick mill and grind 2 minutes, in grinding pot, the quality of ball is 2 times of siccative quality, obtain slurry, by slurry granulation in spray-drying tower, be pressed into the shape of requirement by pressure forming machine, print is dried 2 hours at 40 DEG C, thoroughly dry 5 hours at 100 DEG C.Then be placed on 1100 DEG C of sintering in the resistance furnace that is rapidly heated, soaking time 30 minutes, be prepared into boccaro ceramics, the boccaro ceramics preparing is dried 2 hours at 120 DEG C, take quality, be put in boiling water and boil 2 hours 30 minutes, after water naturally cooling, pull ceramics out, on the deerskin soaking, wipe excessive moisture, take its quality, calculating water-intake rate is 0.22%.
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN105753462A (en) * | 2016-02-04 | 2016-07-13 | 浙江醒缘生物科技有限公司 | Turtle type activated energy magnet therapy plate and preparation method thereof |
CN106490903A (en) * | 2016-10-21 | 2017-03-15 | 青岛首创嘉业工贸有限公司 | A kind of active summer sleeping mat and preparation method thereof |
CN106617538A (en) * | 2016-10-21 | 2017-05-10 | 青岛首创嘉业工贸有限公司 | Active pendant and preparation method thereof |
CN110655382A (en) * | 2019-08-02 | 2020-01-07 | 景德镇御腾瓷器有限公司 | Preparation method of health-care ball with high far infrared radiance |
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Publication number | Priority date | Publication date | Assignee | Title |
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CN1603277A (en) * | 2004-10-15 | 2005-04-06 | 徐顺伟 | Eating utensils prepared by mixing medical stone and purple sand mud and production method thereof |
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- 2012-12-19 CN CN201210552300.1A patent/CN103880402B/en active Active
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Publication number | Priority date | Publication date | Assignee | Title |
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CN1603277A (en) * | 2004-10-15 | 2005-04-06 | 徐顺伟 | Eating utensils prepared by mixing medical stone and purple sand mud and production method thereof |
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN105753462A (en) * | 2016-02-04 | 2016-07-13 | 浙江醒缘生物科技有限公司 | Turtle type activated energy magnet therapy plate and preparation method thereof |
CN106490903A (en) * | 2016-10-21 | 2017-03-15 | 青岛首创嘉业工贸有限公司 | A kind of active summer sleeping mat and preparation method thereof |
CN106617538A (en) * | 2016-10-21 | 2017-05-10 | 青岛首创嘉业工贸有限公司 | Active pendant and preparation method thereof |
CN110655382A (en) * | 2019-08-02 | 2020-01-07 | 景德镇御腾瓷器有限公司 | Preparation method of health-care ball with high far infrared radiance |
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Effective date of registration: 20211201 Address after: 110142 No. 3 Chongshan Road, Huanggu District, Shenyang City, Liaoning Province Patentee after: LIAONING LIGHT INDUSTRY SCIENCE RESEARCH INSTITUTE Co.,Ltd. Address before: 110400 Faku Economic Development Zone, Shenyang, Liaoning Patentee before: LIAONING FAKU CERAMIC ENGINEERING TECHNOLOGY RESEARCH CENTER |