CN102212415A - 用毛叶山桐子油制备生物柴油及其制法 - Google Patents
用毛叶山桐子油制备生物柴油及其制法 Download PDFInfo
- Publication number
- CN102212415A CN102212415A CN2011101040746A CN201110104074A CN102212415A CN 102212415 A CN102212415 A CN 102212415A CN 2011101040746 A CN2011101040746 A CN 2011101040746A CN 201110104074 A CN201110104074 A CN 201110104074A CN 102212415 A CN102212415 A CN 102212415A
- Authority
- CN
- China
- Prior art keywords
- oil
- idesia polycarpa
- solid acid
- biofuel
- var
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003225 biodiesel Substances 0.000 title abstract description 8
- 241000538126 Idesia polycarpa var. vestita Species 0.000 title abstract 6
- 238000002360 preparation method Methods 0.000 title description 7
- 239000011973 solid acid Substances 0.000 claims abstract description 27
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 19
- 238000009874 alkali refining Methods 0.000 claims abstract description 19
- 238000006243 chemical reaction Methods 0.000 claims abstract description 16
- 239000003054 catalyst Substances 0.000 claims abstract description 10
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 7
- 239000002551 biofuel Substances 0.000 claims description 36
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 30
- 241001299699 Idesia Species 0.000 claims description 29
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 12
- 238000007171 acid catalysis Methods 0.000 claims description 12
- 230000036571 hydration Effects 0.000 claims description 12
- 238000006703 hydration reaction Methods 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 238000001035 drying Methods 0.000 claims description 6
- 235000011187 glycerol Nutrition 0.000 claims description 6
- 230000004913 activation Effects 0.000 claims description 5
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 claims description 3
- 238000012545 processing Methods 0.000 claims description 3
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- 239000011259 mixed solution Substances 0.000 claims 1
- 235000017550 sodium carbonate Nutrition 0.000 claims 1
- 238000000034 method Methods 0.000 abstract description 15
- 238000011161 development Methods 0.000 abstract description 14
- 238000006555 catalytic reaction Methods 0.000 abstract description 4
- 239000002994 raw material Substances 0.000 abstract description 4
- 239000002253 acid Substances 0.000 abstract description 3
- 230000007797 corrosion Effects 0.000 abstract description 2
- 238000005260 corrosion Methods 0.000 abstract description 2
- 230000035484 reaction time Effects 0.000 abstract description 2
- 238000011084 recovery Methods 0.000 abstract description 2
- 238000003912 environmental pollution Methods 0.000 abstract 1
- 125000004185 ester group Chemical group 0.000 abstract 1
- 230000000887 hydrating effect Effects 0.000 abstract 1
- 239000003921 oil Substances 0.000 description 60
- 235000019198 oils Nutrition 0.000 description 60
- 238000004519 manufacturing process Methods 0.000 description 6
- 238000004821 distillation Methods 0.000 description 4
- 239000000706 filtrate Substances 0.000 description 4
- 239000002283 diesel fuel Substances 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000011160 research Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 244000036905 Benincasa cerifera Species 0.000 description 2
- 235000011274 Benincasa cerifera Nutrition 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 239000010503 gourd oil Substances 0.000 description 2
- 230000001737 promoting effect Effects 0.000 description 2
- 238000012827 research and development Methods 0.000 description 2
- 239000011949 solid catalyst Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 239000002028 Biomass Substances 0.000 description 1
- 244000247747 Coptis groenlandica Species 0.000 description 1
- 235000002991 Coptis groenlandica Nutrition 0.000 description 1
- 240000006766 Cornus mas Species 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 229920000263 Rubber seed oil Polymers 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 240000001866 Vernicia fordii Species 0.000 description 1
- 244000089698 Zanthoxylum simulans Species 0.000 description 1
- 235000009932 Zanthoxylum simulans Nutrition 0.000 description 1
- -1 Zr (SO4) 24H2O Chemical compound 0.000 description 1
- 230000003213 activating effect Effects 0.000 description 1
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000005815 base catalysis Methods 0.000 description 1
- 208000012839 conversion disease Diseases 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000032050 esterification Effects 0.000 description 1
- 238000005886 esterification reaction Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000003208 petroleum Substances 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- 235000013311 vegetables Nutrition 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Fats And Perfumes (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (2)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2011101040746A CN102212415B (zh) | 2011-04-26 | 2011-04-26 | 用毛叶山桐子油制备生物柴油及其制法 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN2011101040746A CN102212415B (zh) | 2011-04-26 | 2011-04-26 | 用毛叶山桐子油制备生物柴油及其制法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN102212415A true CN102212415A (zh) | 2011-10-12 |
CN102212415B CN102212415B (zh) | 2013-08-14 |
Family
ID=44743960
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN2011101040746A Expired - Fee Related CN102212415B (zh) | 2011-04-26 | 2011-04-26 | 用毛叶山桐子油制备生物柴油及其制法 |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN102212415B (zh) |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106867682A (zh) * | 2017-03-10 | 2017-06-20 | 四川森迪科技发展股份有限公司 | 一种用毛叶山桐子油制备生物柴油的方法 |
CN109554218A (zh) * | 2018-10-12 | 2019-04-02 | 贵州航天乌江机电设备有限责任公司 | 一种超临界流体萃取山桐子中脂溶性化合物的工艺 |
CN113736562A (zh) * | 2021-09-02 | 2021-12-03 | 重庆大学 | 一种以小桐子油为原料的植物绝缘油脱酸工艺方法 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1687314A (zh) * | 2005-04-27 | 2005-10-26 | 莫春礼 | 用高酸值废弃动植物油生产生物柴油的工艺 |
CN101358141A (zh) * | 2008-09-28 | 2009-02-04 | 四川省国政生物质能源科技发展股份有限公司 | 用固体碱催化毛叶山桐子油制备生物柴油的方法 |
-
2011
- 2011-04-26 CN CN2011101040746A patent/CN102212415B/zh not_active Expired - Fee Related
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1687314A (zh) * | 2005-04-27 | 2005-10-26 | 莫春礼 | 用高酸值废弃动植物油生产生物柴油的工艺 |
CN101358141A (zh) * | 2008-09-28 | 2009-02-04 | 四川省国政生物质能源科技发展股份有限公司 | 用固体碱催化毛叶山桐子油制备生物柴油的方法 |
Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN106867682A (zh) * | 2017-03-10 | 2017-06-20 | 四川森迪科技发展股份有限公司 | 一种用毛叶山桐子油制备生物柴油的方法 |
CN109554218A (zh) * | 2018-10-12 | 2019-04-02 | 贵州航天乌江机电设备有限责任公司 | 一种超临界流体萃取山桐子中脂溶性化合物的工艺 |
CN113736562A (zh) * | 2021-09-02 | 2021-12-03 | 重庆大学 | 一种以小桐子油为原料的植物绝缘油脱酸工艺方法 |
Also Published As
Publication number | Publication date |
---|---|
CN102212415B (zh) | 2013-08-14 |
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Owner name: SICHUAN ZHIYU BIOLOGICAL ENERGY TECHNOLOGY CO., LT Free format text: FORMER OWNER: LIU CHANGGEN Effective date: 20120918 |
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Free format text: CORRECT: ADDRESS; FROM: 610041 CHENGDU, SICHUAN PROVINCE TO: 621000 MIANYANG, SICHUAN PROVINCE |
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Effective date of registration: 20120918 Address after: 621000, No. 6, building 1, 2, north section of torch West Street, Mianyang hi tech Zone, Sichuan, 2 Applicant after: SICHUAN ZHIYU BIO-ENERGY SOURCE TECHNOLOGY Co.,Ltd. Address before: 610041 No. 13 East Yulin street, Chengdu, Sichuan, Wuhou District Applicant before: Liu Changgen |
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Application publication date: 20111012 Assignee: Sichuan Wantong Li Yuan Agricultural Development Co.,Ltd. Assignor: SICHUAN ZHIYU BIO-ENERGY SOURCE TECHNOLOGY Co.,Ltd. Contract record no.: 2014510000158 Denomination of invention: Biodiesel prepared from Idesia polycarpa var.vestita Diels oil and preparation method thereof Granted publication date: 20130814 License type: Exclusive License Record date: 20140928 |
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Owner name: GUANGDONG DINGRONG ECOLOGICAL AGRICULTURE DEVELOPM Free format text: FORMER OWNER: SICHUAN ZHIYU BIOLOGICAL ENERGY TECHNOLOGY CO., LTD. Effective date: 20150724 |
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C41 | Transfer of patent application or patent right or utility model | ||
TR01 | Transfer of patent right |
Effective date of registration: 20150724 Address after: Guangning County, Guangdong province 526334 Zhaoqing city Jiangtun town (formerly radio station and alliance building) Patentee after: Guangdong Ding Rong Ecological Agriculture Development Co.,Ltd. Address before: 621000, No. 6, building 1, 2, north section of torch West Street, Mianyang hi tech Zone, Sichuan, 2 Patentee before: SICHUAN ZHIYU BIO-ENERGY SOURCE TECHNOLOGY Co.,Ltd. |
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C56 | Change in the name or address of the patentee | ||
CP01 | Change in the name or title of a patent holder |
Address after: Guangning County, Guangdong province 526334 Zhaoqing city Jiangtun town (formerly radio station and alliance building) Patentee after: GUANGDONG DINGFENG ECOLOGICAL AGRICULTURE DEVELOPMENT Co.,Ltd. Address before: Guangning County, Guangdong province 526334 Zhaoqing city Jiangtun town (formerly radio station and alliance building) Patentee before: Guangdong Ding Rong Ecological Agriculture Development Co.,Ltd. |
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CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130814 |
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