CN100372556C - 植物多酚类物质的提取方法 - Google Patents
植物多酚类物质的提取方法 Download PDFInfo
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- CN100372556C CN100372556C CNB2005100224200A CN200510022420A CN100372556C CN 100372556 C CN100372556 C CN 100372556C CN B2005100224200 A CNB2005100224200 A CN B2005100224200A CN 200510022420 A CN200510022420 A CN 200510022420A CN 100372556 C CN100372556 C CN 100372556C
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- plant polyphenol
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- polyphenol
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- 235000013824 polyphenols Nutrition 0.000 title claims abstract description 68
- 150000008442 polyphenolic compounds Chemical class 0.000 title claims abstract description 65
- 238000000605 extraction Methods 0.000 title abstract description 7
- 239000000126 substance Substances 0.000 title abstract 4
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 23
- 239000001301 oxygen Substances 0.000 claims abstract description 23
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 21
- 229910052756 noble gas Inorganic materials 0.000 claims abstract description 20
- 239000007787 solid Substances 0.000 claims abstract description 20
- 238000005303 weighing Methods 0.000 claims abstract description 20
- 239000002994 raw material Substances 0.000 claims abstract description 7
- 239000011261 inert gas Substances 0.000 claims abstract description 6
- 241000196324 Embryophyta Species 0.000 claims description 43
- 238000000034 method Methods 0.000 claims description 22
- 239000007788 liquid Substances 0.000 claims description 19
- 241000219095 Vitis Species 0.000 claims description 9
- 235000009392 Vitis Nutrition 0.000 claims description 9
- 238000000874 microwave-assisted extraction Methods 0.000 claims description 9
- 210000000582 semen Anatomy 0.000 claims description 9
- 239000005445 natural material Substances 0.000 claims description 6
- 244000089265 zong er cha Species 0.000 claims description 6
- PFTAWBLQPZVEMU-DZGCQCFKSA-N (+)-catechin Chemical compound C1([C@H]2OC3=CC(O)=CC(O)=C3C[C@@H]2O)=CC=C(O)C(O)=C1 PFTAWBLQPZVEMU-DZGCQCFKSA-N 0.000 claims description 5
- VYQNWZOUAUKGHI-UHFFFAOYSA-N monobenzone Chemical compound C1=CC(O)=CC=C1OCC1=CC=CC=C1 VYQNWZOUAUKGHI-UHFFFAOYSA-N 0.000 claims description 5
- 238000010298 pulverizing process Methods 0.000 claims description 5
- 235000003143 Panax notoginseng Nutrition 0.000 claims description 4
- 241000180649 Panax notoginseng Species 0.000 claims description 4
- 238000002604 ultrasonography Methods 0.000 claims description 4
- 238000001816 cooling Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 238000009413 insulation Methods 0.000 abstract 1
- 239000008213 purified water Substances 0.000 abstract 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 45
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 30
- 229910052786 argon Inorganic materials 0.000 description 15
- 229910001873 dinitrogen Inorganic materials 0.000 description 15
- 239000000428 dust Substances 0.000 description 15
- 239000001307 helium Substances 0.000 description 15
- 229910052734 helium Inorganic materials 0.000 description 15
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 15
- 229910052757 nitrogen Inorganic materials 0.000 description 15
- 239000000843 powder Substances 0.000 description 13
- 238000002137 ultrasound extraction Methods 0.000 description 11
- 238000005516 engineering process Methods 0.000 description 7
- 244000269722 Thea sinensis Species 0.000 description 6
- 230000000694 effects Effects 0.000 description 6
- 229940087559 grape seed Drugs 0.000 description 6
- 230000008569 process Effects 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 238000010792 warming Methods 0.000 description 5
- 238000002386 leaching Methods 0.000 description 4
- -1 chebulic acid polyphenol Chemical class 0.000 description 3
- 239000003814 drug Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 238000007254 oxidation reaction Methods 0.000 description 3
- COZMWVAACFYLBI-UHFFFAOYSA-N Chebulic acid Natural products OC1=C(O)C(O)=C2C(C(CC(=O)O)C(O)=O)C(C(O)=O)OC(=O)C2=C1 COZMWVAACFYLBI-UHFFFAOYSA-N 0.000 description 2
- 229920002361 Chebulic acid Polymers 0.000 description 2
- 206010028980 Neoplasm Diseases 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 244000025254 Cannabis sativa Species 0.000 description 1
- 208000024172 Cardiovascular disease Diseases 0.000 description 1
- 241000208152 Geranium Species 0.000 description 1
- 241001415959 Grus japonensis Species 0.000 description 1
- 208000008589 Obesity Diseases 0.000 description 1
- 240000005001 Paeonia suffruticosa Species 0.000 description 1
- 235000003889 Paeonia suffruticosa Nutrition 0.000 description 1
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000003181 Panax pseudoginseng Nutrition 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 230000003178 anti-diabetic effect Effects 0.000 description 1
- 230000003579 anti-obesity Effects 0.000 description 1
- 230000003064 anti-oxidating effect Effects 0.000 description 1
- 230000000840 anti-viral effect Effects 0.000 description 1
- 230000002155 anti-virotic effect Effects 0.000 description 1
- 239000003472 antidiabetic agent Substances 0.000 description 1
- 239000002246 antineoplastic agent Substances 0.000 description 1
- 229940041181 antineoplastic drug Drugs 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 235000013361 beverage Nutrition 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 201000011510 cancer Diseases 0.000 description 1
- 230000036996 cardiovascular health Effects 0.000 description 1
- 230000008859 change Effects 0.000 description 1
- COZMWVAACFYLBI-XJEVXTIOSA-N chebulic acid Chemical compound OC1=C(O)C(O)=C2[C@H]([C@H](CC(=O)O)C(O)=O)[C@@H](C(O)=O)OC(=O)C2=C1 COZMWVAACFYLBI-XJEVXTIOSA-N 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- JEIPFZHSYJVQDO-UHFFFAOYSA-N ferric oxide Chemical compound O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 230000036541 health Effects 0.000 description 1
- 230000006872 improvement Effects 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000012054 meals Nutrition 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229930014626 natural product Natural products 0.000 description 1
- 231100000252 nontoxic Toxicity 0.000 description 1
- 230000003000 nontoxic effect Effects 0.000 description 1
- 235000020824 obesity Nutrition 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 150000003254 radicals Chemical class 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
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CNB2005100224200A CN100372556C (zh) | 2005-12-29 | 2005-12-29 | 植物多酚类物质的提取方法 |
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CNB2005100224200A CN100372556C (zh) | 2005-12-29 | 2005-12-29 | 植物多酚类物质的提取方法 |
Publications (2)
Publication Number | Publication Date |
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CN1824084A CN1824084A (zh) | 2006-08-30 |
CN100372556C true CN100372556C (zh) | 2008-03-05 |
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CNB2005100224200A Active CN100372556C (zh) | 2005-12-29 | 2005-12-29 | 植物多酚类物质的提取方法 |
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Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1970015B (zh) * | 2006-12-12 | 2010-09-22 | 中国人民解放军第三军医大学 | 木瓜多酚类物质的酶解提取方法 |
FR2926190B1 (fr) * | 2008-01-14 | 2013-07-05 | Thiomed | Procede de preparation d'extraits vegetaux permettant l'obtention d'une nouvelle forme galenique |
CN101294048B (zh) * | 2008-06-19 | 2010-06-23 | 晋城市柿宝科技发展有限公司 | 一种柿子栲胶的制备方法 |
CN101444562B (zh) * | 2008-12-24 | 2012-10-03 | 中国人民解放军第三军医大学 | 木瓜抗氧化精华素及其制备方法 |
CN101773589B (zh) * | 2010-01-12 | 2011-08-17 | 海南大学 | 一种椰子多酚提取物的生产方法 |
CN103622135A (zh) * | 2013-11-26 | 2014-03-12 | 山东鲁花集团有限公司 | 一种从花生红衣中提取多酚类物质的方法 |
CN105146590B (zh) * | 2015-09-08 | 2019-04-12 | 浙江省海洋开发研究院 | 一种金枪鱼罐头的制备方法 |
CN105237589A (zh) * | 2015-11-04 | 2016-01-13 | 中国科学院过程工程研究所 | 一种同时提取葡萄籽中多酚及半纤维素的方法 |
CN105535029B (zh) * | 2015-12-28 | 2020-02-21 | 江苏大学 | 一种蜂胶提取物的逆流超声制备方法 |
CN105853475A (zh) * | 2016-01-05 | 2016-08-17 | 浙江海洋学院 | 一种水芫花提取物制备方法 |
CN105779588A (zh) * | 2016-01-28 | 2016-07-20 | 云南农业大学 | 一种烟草多酚类物质诱导植物免疫反应的检测方法 |
CN109054014B (zh) * | 2018-07-24 | 2020-06-26 | 上海中医药大学 | 一种多酚聚合物及其用途 |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1565697A (zh) * | 2003-07-07 | 2005-01-19 | 珠海经济特区新科应用研究所 | 新型无氧化低温提取浓缩喷雾干燥生产线 |
CN1197857C (zh) * | 2003-06-25 | 2005-04-20 | 张守政 | 茶多酚与茶色素的提取方法 |
-
2005
- 2005-12-29 CN CNB2005100224200A patent/CN100372556C/zh active Active
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1197857C (zh) * | 2003-06-25 | 2005-04-20 | 张守政 | 茶多酚与茶色素的提取方法 |
CN1565697A (zh) * | 2003-07-07 | 2005-01-19 | 珠海经济特区新科应用研究所 | 新型无氧化低温提取浓缩喷雾干燥生产线 |
Non-Patent Citations (3)
Title |
---|
植物多酚提取技术及其开发应用现状. 韩丙军,彭黎旭.华南热带农业大学学报,第11卷第1期. 2005 * |
绿茶中茶多酚的提取工艺研究. 郑尚珍,孟军才,王定勇,沈序维.西北师范大学学报,第32卷第3期. 1996 * |
苹果渣多酚超声波提取工艺及其抗氧化性研究. 李志西,李元瑞,葛蕾,司翔宇.西北农林科技大学学报,第33卷第8期. 2005 * |
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CN1824084A (zh) | 2006-08-30 |
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C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Guangzhou Xipu Bio-Feed Co.,Ltd. Assignor: Xie Jun Contract fulfillment period: 2009.6.30 to 2015.6.29 Contract record no.: 2009440001295 Denomination of invention: Active component extraction method of plant polyphenol kind substance Granted publication date: 20080305 License type: Exclusive license Record date: 20090820 |
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LIC | Patent licence contract for exploitation submitted for record |
Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2009.6.30 TO 2015.6.29; CHANGE OF CONTRACT Name of requester: GUANGZHOU CITY XIPU BIOLOGY FEED CO., LTD. Effective date: 20090820 |
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Owner name: CHENGDU WEIHUI BIOTCCHNOLOGY CO., LTD. Free format text: FORMER OWNER: XIE JUN Effective date: 20091127 |
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Effective date of registration: 20091127 Address after: Prosperous road, Heshan Town, Pujiang County, Sichuan Patentee after: CHENGDU WEIHUI BIOTECHNOLOGY Co.,Ltd. Address before: Room 253, No. 708 Cha Shan Road, Guangzhou, Guangdong, Tianhe District Patentee before: Xie Jun |
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Owner name: XIE JUN Free format text: FORMER OWNER: CHENGDU WEIHUI BIOLOGICAL TECHNOLOGY CO., LTD. Effective date: 20150109 |
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Free format text: CORRECT: ADDRESS; FROM: 611630 CHENGDU, SICHUAN PROVINCE TO: 510640 GUANGZHOU, GUANGDONG PROVINCE |
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TR01 | Transfer of patent right |
Effective date of registration: 20150109 Address after: 510640, room 253, 708 Cha Shan Road, Guangzhou, Tianhe District, Guangdong Patentee after: Xie Jun Address before: 611630 prosperous road, Heshan Town, Pujiang County, Sichuan Patentee before: CHENGDU WEIHUI BIOTECHNOLOGY Co.,Ltd. |
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Effective date of registration: 20240723 Address after: Room 321, Building 18, Mount Taishan District, South China Agricultural University, No. 483, Wushan Road, Tianhe District, Guangzhou, Guangdong 510000 Patentee after: Yujiaofu (Guangzhou) Biotechnology Co.,Ltd. Country or region after: China Address before: 510640, room 253, 708 Cha Shan Road, Guangzhou, Tianhe District, Guangdong Patentee before: Xie Jun Country or region before: China |